Catalyst comprising Pt, Ni, and Cr

Steinbach, Andrew J. L.; Hester, Amy E.; Haug, Andrew T.; Lewinski, Krzysztof A.; Luopa, Sean M.; Thoma, Grant M.

Title: Catalyst comprising Pt, Ni, and Cr

Abstract

Catalysts comprising nanostructured elements comprising microstructured whiskers having an outer surface at least partially covered by a catalyst material comprising at least 90 atomic percent collectively Pt, Ni, and Cr, wherein the Pt is present in a range from 32.4 to 35.8 atomic percent, the Ni is present in a range from 57.7 to 63.7 atomic percent, and the Cr is present in a range from 0.5 to 10.0 atomic percent, and wherein the total atomic percent of Pt, Ni, and Cr equals 100. Catalyst described herein are useful, for example, in fuel cell membrane electrode assemblies.

Inventors:: Steinbach, Andrew J. L.; Hester, Amy E.; Haug, Andrew T.; Lewinski, Krzysztof A.; Luopa, Sean M.; Thoma, Grant M.

Issue Date:: 2022-08-02

Research Org.:: 3M Innovative Properties Company

Sponsoring Org.:: USDOE

OSTI Identifier:: 1924951

Patent Number(s):: 11404702

Application Number:: 15/733,645

Assignee:: 3M Innovative Properties Company (St. Paul, MN)

Patent Classifications (CPCs):: H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION

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H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M2008/1095 - {Fuel cells with polymeric electrolytes}
H01M4/8657 - {layered}
H01M4/8825 - {Methods for deposition of the catalytic active composition}
H01M4/8889 - {Cosintering or cofiring of a catalytic active layer with another type of layer}
H01M4/9041 - {Metals or alloys
H01M4/9075 - {Catalytic material supported on carriers, e.g. powder carriers
H01M4/921 - {Alloys or mixtures with metallic elements}
H01M8/1004 - characterised by membrane-electrode assemblies [MEA]

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/50 - Fuel cells

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DOE Contract Number:: EE0007270

Resource Type:: Patent

Resource Relation:: Patent File Date: 03/27/2019

Country of Publication:: United States

Language:: English

Citation Formats


                    Steinbach, Andrew J. L., Hester, Amy E., Haug, Andrew T., Lewinski, Krzysztof A., Luopa, Sean M., and Thoma, Grant M. Catalyst comprising Pt, Ni, and Cr.  United States: N. p., 2022. 
        Web.

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                    Steinbach, Andrew J. L., Hester, Amy E., Haug, Andrew T., Lewinski, Krzysztof A., Luopa, Sean M., & Thoma, Grant M. Catalyst comprising Pt, Ni, and Cr.  United States.

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                    Steinbach, Andrew J. L., Hester, Amy E., Haug, Andrew T., Lewinski, Krzysztof A., Luopa, Sean M., and Thoma, Grant M. Tue .  
        "Catalyst comprising Pt, Ni, and Cr".  United States.  https://www.osti.gov/servlets/purl/1924951.

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@article{osti_1924951,

  title        = {Catalyst comprising Pt, Ni, and Cr},

  author       = {Steinbach, Andrew J. L. and Hester, Amy E. and Haug, Andrew T. and Lewinski, Krzysztof A. and Luopa, Sean M. and Thoma, Grant M.},

  abstractNote = {Catalysts comprising nanostructured elements comprising microstructured whiskers having an outer surface at least partially covered by a catalyst material comprising at least 90 atomic percent collectively Pt, Ni, and Cr, wherein the Pt is present in a range from 32.4 to 35.8 atomic percent, the Ni is present in a range from 57.7 to 63.7 atomic percent, and the Cr is present in a range from 0.5 to 10.0 atomic percent, and wherein the total atomic percent of Pt, Ni, and Cr equals 100. Catalyst described herein are useful, for example, in fuel cell membrane electrode assemblies.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2022},

  month        = {8}

}

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US Patent Application 14/652275; 20150311536
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20150311536

Ternary Pt-Ru-Ni catalytic layers for methanol electrooxidation prepared by electrodeposition and galvanic replacement
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Papaderakis, Athanasios; Pliatsikas, Nikolaos; Prochaska, Chara
Frontiers in Chemistry, Vol. 2
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Fuel Cell Oxidation Reduction Reaction Catalyst
patent-application, March 2018

Gath, Kerrie K.; Yang, Jun; Xu, Chunchuan
US Patent Application 15/248,270; 2018/0062181 Al
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20180062181

RDE Measurements of ORR Activity of Pt[sub 1−x]Ir[sub x] (0<x<0.3) on High Surface Area NSTF-Coated Glassy Carbon Disks
journal, January 2010

Liu, Gary Chih-Kang; Sanderson, R. J.; Vernstrom, George
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https://doi.org/10.1149/1.3262522

Carbon Nanotubes Supported Pt-Ru-Ni as Methanol Electro-Oxidation Catalyst for Direct Methanol Fuel Cells
journal, June 2007

Ye, Fei; Chen, Shengzhou; Dong, Xinfa
Journal of Natural Gas Chemistry, Vol. 16, Issue 2
https://doi.org/10.1016/S1003-9953(07)60042-5

Methanol Oxidation on Pt/Ru, Pt/Ni, and Pt/Ru/Ni Anode Electrocatalysts at Different Temperatures for DMFCs
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Choi, Jong-Ho; Park, Kyung-Won; Kwon, Boo-Kil
Journal of The Electrochemical Society, Vol. 150, Issue 7
https://doi.org/10.1149/1.1581011

Development of plurimetallic electrocatalysts prepared by decomposition of polymeric precursors for EtOH/O2 fuel cell
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Palma, Lívia M.; Almeida, Thiago S.; Andrade, Adalgisa R. de
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Suboxide Fuel Cell Catalyst for Enhanced Reformate Tolerance
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Haugen, Gregory M.; Debe, Mark K.; Thomas III, John H.
US Patent Application 09/745,501; 2002/0004453 Al
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20020004453

Development of Ternary and Quaternary Catalysts for the Electrooxidation of Glycerol
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Artem, L. M.; Santos, D. M.; De Andrade, A. R.
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Title: Catalyst comprising Pt, Ni, and Cr

Abstract

Citation Formats

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Enhanced catalyst interface for membrane electrode assembly patent, March 2011

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Method of producing a microstructured surface and the article produced thereby patent, July 1982

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Mesostructured thin films as electrocatalysts with tunable composition and surface morphology
journal, November 2012

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journal, October 2013

Structurally ordered intermetallic platinum–cobalt core–shell nanoparticles with enhanced activity and stability as oxygen reduction electrocatalysts
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journal, January 2006

An advantageous method for methanol oxidation: Design and fabrication of a nanoporous PtRuNi trimetallic electrocatalyst
journal, November 2011

Microtextured catalyst transfer substrate
patent, October 2000

Method to Prepare Ternary Methanol Electro-Oxidation Catalysts for Direct Methanol Fuel Cell Applications
journal, January 2017

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patent, May 1984

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journal, January 2009

Method for producing a nanoporous layer
patent, March 2014

A core–shell Pd ₁ Ru ₁ Ni ₂ @Pt/C catalyst with a ternary alloy core and Pt monolayer: enhanced activity and stability towards the oxygen reduction reaction by the addition of Ni
journal, January 2016

Methanol oxidation catalyst
patent, July 2012

A facile and surfactant-free route for nanomanufacturing of tailored ternary nanoalloys as superior oxygen reduction reaction electrocatalysts
journal, January 2017

TiC supported Pt–Ir electrocatalyst prepared by a plasma process for the oxygen electrode in unitized regenerative fuel cells
journal, July 2011

Ethanol Electrooxidation by Plurimetallic Pt-Based Electrocatalysts Prepared by Microwave Assisted Heating
journal, January 2014

Electrochemical characterization of Pt–Ru–Ni/C anode electrocatalyst for methanol electrooxidation in membraneless fuel cells
journal, January 2015

Platinum-chromium-copper/nickel fuel cell catalyst
patent-application, November 2006

Fuel cell cathode catalyst
patent, September 2008

Effects of Nitrogen, Methane, and Oxygen on Structure and Electrical Properties of Thin Tantalum Films
journal, February 1964

One step NaBH 4 reduction of Pt-Ru-Ni catalysts on different types of carbon supports for direct ethanol fuel cells: Synthesis and characterization
journal, May 2017

Nanostructured electrode membranes
patent, August 1994

Effect of gravity on copper phthalocyanine thin films III: Microstructure comparisons of copper phthalocyanine thin films grown in microgravity and unit gravity
journal, May 1990

Catalyst for membrane electrode assembly and method of making
patent, March 2000

Effect of Ni on PtRu/C Catalyst Performance for Ethanol Electrooxidation in Acidic Medium
journal, April 2008

Membrane electrode assembly
patent, March 1999

Annealed nanostructured thin film catalyst
patent, June 2014

Fabrication of biologically based microstructure composites for vacuum field emission
journal, October 1992

Catalyst for membrane electrode assembly and method of making
patent, March 1999

Truncated octahedral platinum–nickel–iridium ternary electro-catalyst for oxygen reduction reaction
journal, September 2015

Low Platinum Fuel Cell Catalysts and Method for Preparing the Same
patent-application, March 2005

Combinatorial screening of fuel cell cathode catalyst compositions
journal, November 2007

Evaluation of the Performance of Carbon Supported Pt-Ru-Ni-P as Anode Catalyst for Methanol Electrooxidation
journal, June 2010

Preparation of Surface Organometallic Catalysts by Gas-Phase Ligand Stripping and Reactive Landing of Mass-Selected Ions
journal, November 2010

Evolution of Nanoporous Pt-Fe Alloy Nanowires by Dealloying and their Catalytic Property for Oxygen Reduction Reaction
journal, July 2011

Preparation of Pt-Ru-Ni ternary nanoparticles by microemulsion and electrocatalytic activity for methanol oxidation
journal, February 2007

Effect of a Carbon Support Containing Large Mesopores on the Performance of a Pt−Ru−Ni/C Catalyst for Direct Methanol Fuel Cells
journal, November 2009

Electrochemical impedance studies on carbon supported PtRuNi and PtRu anode catalysts in acid medium for direct methanol fuel cell
journal, February 2007

Atomic layer deposition of ultrathin platinum films on tungsten atomic layer deposition adhesion layers: Application to high surface area substrates
journal, January 2015

Dealloyed binary PtM3 (M=Cu, Co, Ni) and ternary PtNi3M (M=Cu, Co, Fe, Cr) electrocatalysts for the oxygen reduction reaction: Performance in polymer electrolyte membrane fuel cells
journal, January 2011

Co-tolerant catalyst for PAFC
patent-application, December 2015

Preparation and Electrochemical Research of Anode Catalyst PtRuNi/C for Direct Methanol Fuel Cell
journal, August 2013

Summary Abstract: Dramatic variation of the physical microstructure of a vapor deposited organic thin film
journal, July 1987

Synthesis and Structure−Activity Relationship Exploration of Carbon-Supported PtRuNi Nanocomposite as a CO-Tolerant Electrocatalyst for Proton Exchange Membrane Fuel Cells
journal, March 2006

Fuel Cell Nanocatalyst with Voltage Reversal Tolerance
patent-application, February 2010

Membrane electrode assembly
patent, November 2001

Article having surface layer of uniformly oriented, crystalline, organic microstructures
patent, March 1989

Ta-doped Anatase TiO ₂ Epitaxial Film as Transparent Conducting Oxide
journal, August 2005

Method and Apparatus for Forming High Surface Area Material Films and Membranes
patent-application, March 2004

Electrodeposition of Pt–Ru and Pt–Ru–Ni nanoclusters on multi-walled carbon nanotubes for direct methanol fuel cell
journal, March 2014

NSTF Advances for PEM Electrolysis - the Effect of Alloying on Activity of NSTF Electrolyzer Catalysts and Performance of NSTF Based PEM Electrolyzers
journal, September 2015

Effects of morphology on NO2 detection in air at room temperature with phthalocyanine thin films
journal, December 1990

Platinum-Iridium Alloys as Oxygen Reduction Electrocatalysts for Polymer Electrolyte Fuel Cells
journal, January 2005

Article with reduced friction polymer sheet support
patent, February 1986

Enhanced activity and stability of core–shell structured PtRuNi electrocatalysts for direct methanol fuel cells
journal, January 2016

Catalyst material
patent, June 1998

Porous platinum-based catalysts for oxygen reduction
patent, November 2014

Method for preparing an article having surface layer of uniformly oriented, crystalline, organic microstructures
patent, August 1991

Method of forming nanoporous membranes
patent, October 2004

Evolution of nanoporosity in dealloying
journal, March 2001

Electrocatalytic characteristics of Pt–Ru–Co and Pt–Ru–Ni based on covalently cross-linked sulfonated poly(ether ether ketone)/heteropolyacids composite membranes for water electrolysis
journal, September 2010

Basic materials physics of transparent conducting oxides
journal, January 2004

Effect of Ni addition over PtRu/C based electrocatalysts for fuel cell applications
journal, December 2006

Chemical and Electronic Effects of Ni in Pt/Ni and Pt/Ru/Ni Alloy Nanoparticles in Methanol Electrooxidation
journal, February 2002

High dispersion and electrocatalytic properties of platinum on well-aligned carbon nanotube arrays
journal, January 2004

Methanol oxidation on carbon-supported Pt–Ru–Ni ternary nanoparticle electrocatalysts
journal, January 2008

Enhanced catalyst interface for membrane electrode assembly
patent, March 2011

In Situ Reactivity and TOF-SIMS Analysis of Surfaces Prepared by Soft and Reactive Landing of Mass-Selected Ions
journal, June 2010

Catalyst electrodes, and methods of making and using the same
patent-application, September 2014

Paramagnetic Susceptibility, Electrical Resistivity, and Lattice Parameters of Nickel‐Rich Nickel‐Tantalum Alloys
journal, August 1964

Method of producing a microstructured surface and the article produced thereby
patent, July 1982

Catalyst material
patent, November 1991

Platinum based oxygen reaction reduction catalyst
patent-application, April 2015

Carbon monoxide tolerant platinum-tantalum alloyed catalyst
patent, February 1993

Ternary nanocatalyst and method of making
patent-application, April 2007

Vacuum vapor deposited thin films of a perylene dicarboximide derivative: Microstructure versus deposition parameters
journal, May 1988

Electrical Properties of Amorphous Titanium Oxide Thin Films for Bolometric Application
journal, January 2013

Synthesis of the ceramic-metal catalysts (PtRuNi-TiO2) by the combustion method
journal, June 2007

Comparison study of few-layered graphene supported platinum and platinum alloys for methanol and ethanol electro-oxidation
journal, March 2015

Catalyst electrodes and method of making it
patent-application, March 2016

Nanostructured whisker article
patent-application, October 2015