Lithium metal recovery and synthesis

Ignacio de Leon, Patricia Anne; Hryn, John N.; Tang, Li; Barry, Edward F.; Arenas, Daniel Yoav

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Title: Lithium metal recovery and synthesis

Abstract

A process and system for creating a lithium ion anolyte from lithium alloys. Metal and lithium alloys are processed to remove the metal with lithium from the alloy remaining. A lithium ion anolyte formed may be used in a process to form lithium metal. Alternatively, a process and system for recovering lithium from sources such as lithium alloys and lithium metal oxides and other feedstock such as recycled batteries into a thin lithium metal film via electrodeposition in an organic electrolyte contacting both anode (holder for lithium source) and cathode (substrate for lithium deposition) in a single-compartment electrolysis cell.

Inventors:: Ignacio de Leon, Patricia Anne; Hryn, John N.; Tang, Li; Barry, Edward F.; Arenas, Daniel Yoav

Issue Date:: 2022-04-05

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1892805

Patent Number(s):: 11296354

Application Number:: 16/145,364

Assignee:: UChicago Argonne, LLC (Chicago, IL)

Patent Classifications (CPCs):: C - CHEMISTRY C22 - METALLURGY C22B - PRODUCTION AND REFINING OF METALS

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25C - PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS

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C - CHEMISTRY C22 - METALLURGY C22B - PRODUCTION AND REFINING OF METALS
C22B26/12 - Obtaining lithium
C22B3/06 - in inorganic acid solutions {, e.g. with acids generated in situ
C22B3/22 - by physical processes, e.g. by filtration, by magnetic means, {by thermal decomposition}

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25C - PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS
C25C1/02 - of light metals

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M10/052 - Li-accumulators
H01M10/0561 - the electrolyte being constituted of inorganic materials only
H01M10/54 - Reclaiming serviceable parts of waste accumulators
H01M4/0438 - {by electrochemical processing
H01M4/382 - {Lithium
H01M4/622 - {being polymers}

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02P - CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
Y02P10/20 - Process efficiency

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02W - CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
Y02W30/84 - Recycling of batteries

Show less

DOE Contract Number:: AC02-06CH11357

Resource Type:: Patent

Resource Relation:: Patent File Date: 09/28/2018

Country of Publication:: United States

Language:: English

Citation Formats


                    Ignacio de Leon, Patricia Anne, Hryn, John N., Tang, Li, Barry, Edward F., and Arenas, Daniel Yoav. Lithium metal recovery and synthesis.  United States: N. p., 2022. 
        Web.

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                    Ignacio de Leon, Patricia Anne, Hryn, John N., Tang, Li, Barry, Edward F., & Arenas, Daniel Yoav. Lithium metal recovery and synthesis.  United States.

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                    Ignacio de Leon, Patricia Anne, Hryn, John N., Tang, Li, Barry, Edward F., and Arenas, Daniel Yoav. Tue .  
        "Lithium metal recovery and synthesis".  United States.  https://www.osti.gov/servlets/purl/1892805.

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@article{osti_1892805,

  title        = {Lithium metal recovery and synthesis},

  author       = {Ignacio de Leon, Patricia Anne and Hryn, John N. and Tang, Li and Barry, Edward F. and Arenas, Daniel Yoav},

  abstractNote = {A process and system for creating a lithium ion anolyte from lithium alloys. Metal and lithium alloys are processed to remove the metal with lithium from the alloy remaining. A lithium ion anolyte formed may be used in a process to form lithium metal. Alternatively, a process and system for recovering lithium from sources such as lithium alloys and lithium metal oxides and other feedstock such as recycled batteries into a thin lithium metal film via electrodeposition in an organic electrolyte contacting both anode (holder for lithium source) and cathode (substrate for lithium deposition) in a single-compartment electrolysis cell.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2022},

  month        = {4}

}

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Similar Records

Title: Lithium metal recovery and synthesis

Abstract

Citation Formats

Ion Conducting Hybrid Membranes patent-application, September 2016

Dendrite-Free Lithium Deposition with Self-Aligned Nanorod Structure journal, November 2014

Electrolytic process for recovering lithium from aluminum-lithium alloy scrap patent, July 1989

Lithium ion conducting membranes patent-application, March 2020

Atomic Layer Deposition of the Solid Electrolyte Garnet Li 7 La 3 Zr 2 O 12 journal, April 2017

Process and apparatus for producing lithium from aluminum-lithium alloy scrap in a three-layered lithium transport cell patent, November 1990

Processes for Preparing Highly Pure Lithium Carbonate and Other Highly Pure Lithium Containing Compounds patent-application, April 2012

Lithium recovery device using separator reservoir, lithium recovery method and lithium adsorption/desorption system using the same patent, June 2014

Recent Developments in the Synthesis of Supported Catalysts journal, June 2015

Magnetic Nanotube Composite Membranes patent-application, July 2017

Dendrite-free Li deposition using trace-amounts of water as an electrolyte additive journal, July 2015

Lithium primary battery patent, February 2014

Ion Conducting Membrane, Making Method Thereof, Secondary Battery Comprising the Same patent-application, October 2019

Non-aqueous electrolyte secondary battery and process for the preparation thereof patent-application, February 2002

Method of producing electrolytic hydrogen using rare element-deposit electrode patent-application, June 2005

Recycling of Aluminium-Lithium Process Scrap journal, September 1987

Issues and challenges facing rechargeable lithium batteries journal, November 2001

Method for recycling aluminum-lithium-type alloy scrap patent, June 2009

3D printing of electrically conductive hybrid organic–inorganic composite materials journal, February 2018

Inorganic/organic composite porous separator and electrochemical device using the same patent-application, November 2012

Method for Recycling Aluminum-Lithium-Type Alloy Scrap patent-application, March 2007

Improved Lithium Metal Oxide Rich Cathode Materials and Method to Make Them patent-application, June 2016

Polymer Nanofiber-Guided Uniform Lithium Deposition for Battery Electrodes journal, April 2015

Composite Semipermeable Membrane and Method for Manufacturing Same patent-application, November 2020

The use of nanoparticles in polymeric and ceramic membrane structures: Review of manufacturing procedures and performance improvement for water treatment journal, July 2010

Membranes, Separators, Batteries, and Methods patent-application, January 2017

Extraction of metals from municipal solid waste incinerator fly ash by hydrothermal process journal, August 2006

Functionalized inorganic membranes for gas separation patent-application, March 2007

Separation for Alkali Metal Ion Battery patent-application, May 2015

High Purity Lithium and Associated Products and Processes patent-application, December 2016

Polymerized Polymeric Fluid Storage and Purification Method and System patent-application, June 2010

High Energy Lithium Ion Secondary Batteries patent-application, October 2009

Producing Lithium patent-application, January 2015

Electrochemical Cell Used in Production of Hydrogen Using CU-UL Thermochemical Cycle patent-application, September 2014

High-Purity Lithium Metal Films from Aqueous Mineral Solutions journal, January 2018

Method of extracting lithium from aluminum-lithium alloys patent, July 1992

Method for Extracting Lithium from Solution Containing Lithium patent-application, July 2015

Alkali Metal Intercalation Material, as an Electrode in an Electrolytic Cell patent-application, July 2014

Ion Conducting Hybrid Membranes
patent-application, September 2016

Dendrite-Free Lithium Deposition with Self-Aligned Nanorod Structure
journal, November 2014

Electrolytic process for recovering lithium from aluminum-lithium alloy scrap
patent, July 1989

Lithium ion conducting membranes
patent-application, March 2020

Atomic Layer Deposition of the Solid Electrolyte Garnet Li ₇ La ₃ Zr ₂ O ₁₂
journal, April 2017

Process and apparatus for producing lithium from aluminum-lithium alloy scrap in a three-layered lithium transport cell
patent, November 1990

Processes for Preparing Highly Pure Lithium Carbonate and Other Highly Pure Lithium Containing Compounds
patent-application, April 2012

Lithium recovery device using separator reservoir, lithium recovery method and lithium adsorption/desorption system using the same
patent, June 2014

Recent Developments in the Synthesis of Supported Catalysts
journal, June 2015

Magnetic Nanotube Composite Membranes
patent-application, July 2017

Dendrite-free Li deposition using trace-amounts of water as an electrolyte additive
journal, July 2015

Lithium primary battery
patent, February 2014

Ion Conducting Membrane, Making Method Thereof, Secondary Battery Comprising the Same
patent-application, October 2019

Non-aqueous electrolyte secondary battery and process for the preparation thereof
patent-application, February 2002

Method of producing electrolytic hydrogen using rare element-deposit electrode
patent-application, June 2005

Recycling of Aluminium-Lithium Process Scrap
journal, September 1987

Issues and challenges facing rechargeable lithium batteries
journal, November 2001

Method for recycling aluminum-lithium-type alloy scrap
patent, June 2009

3D printing of electrically conductive hybrid organic–inorganic composite materials
journal, February 2018

Inorganic/organic composite porous separator and electrochemical device using the same
patent-application, November 2012

Method for Recycling Aluminum-Lithium-Type Alloy Scrap
patent-application, March 2007

Improved Lithium Metal Oxide Rich Cathode Materials and Method to Make Them
patent-application, June 2016

Polymer Nanofiber-Guided Uniform Lithium Deposition for Battery Electrodes
journal, April 2015

Composite Semipermeable Membrane and Method for Manufacturing Same
patent-application, November 2020

The use of nanoparticles in polymeric and ceramic membrane structures: Review of manufacturing procedures and performance improvement for water treatment
journal, July 2010

Membranes, Separators, Batteries, and Methods
patent-application, January 2017

Extraction of metals from municipal solid waste incinerator fly ash by hydrothermal process
journal, August 2006

Functionalized inorganic membranes for gas separation
patent-application, March 2007

Separation for Alkali Metal Ion Battery
patent-application, May 2015

High Purity Lithium and Associated Products and Processes
patent-application, December 2016

Polymerized Polymeric Fluid Storage and Purification Method and System
patent-application, June 2010

High Energy Lithium Ion Secondary Batteries
patent-application, October 2009

Producing Lithium
patent-application, January 2015

Electrochemical Cell Used in Production of Hydrogen Using CU-UL Thermochemical Cycle
patent-application, September 2014

High-Purity Lithium Metal Films from Aqueous Mineral Solutions
journal, January 2018

Method of extracting lithium from aluminum-lithium alloys
patent, July 1992

Method for Extracting Lithium from Solution Containing Lithium
patent-application, July 2015

Alkali Metal Intercalation Material, as an Electrode in an Electrolytic Cell
patent-application, July 2014