Production of chemical products using electrochemical flow systems and slug flow and associated methods

Voskian, Sahag; Murray, Alexander; Hatton, Trevor Alan; Surendranath, Yogesh

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A - human necessities
A01 - agriculture
A21 - baking
A22 - butchering
A23 - foods or foodstuffs
A24 - tobacco
A41 - wearing apparel
A42 - headwear
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A44 - haberdashery
A45 - hand or travelling articles
A46 - brushware
A47 - furniture
A61 - medical or veterinary science
A62 - life-saving
A63 - sports
A99 - subject matter not otherwise provided for in this section
B - performing operations
B01 - physical or chemical processes or apparatus in general
B02 - crushing, pulverising, or disintegrating
B03 - separation of solid materials using liquids or using pneumatic tables or jigs
B04 - centrifugal apparatus or machines for carrying-out physical or chemical processes
B05 - spraying or atomising in general
B06 - generating or transmitting mechanical vibrations in general
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B44 - decorative arts
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B62 - land vehicles for travelling otherwise than on rails
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B68 - saddlery
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C22 - metallurgy
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C25 - electrolytic or electrophoretic processes
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D01 - natural or man-made threads or fibres
D02 - yarns
D03 - weaving
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D05 - sewing
D06 - treatment of textiles or the like
D07 - ropes
D10 - indexing scheme associated with sublasses of section d, relating to textiles
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F03 - machines or engines for liquids
F04 - positive - displacement machines for liquids
F05 - indexing schemes relating to engines or pumps in various subclasses of classes f01-f04
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F17 - storing or distributing gases or liquids
F21 - lighting
F22 - steam generation
F23 - combustion apparatus
F24 - heating
F25 - refrigeration or cooling
F26 - drying
F27 - furnaces
F28 - heat exchange in general
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F42 - ammunition
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G - physics
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G02 - optics
G03 - photography
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Title: Production of chemical products using electrochemical flow systems and slug flow and associated methods

Abstract

Systems and methods for electrochemically producing chemical products are provided. In certain cases, the systems and methods described herein are capable of producing chemical products such as hydrogen peroxide in solutions with relatively low concentrations of electrolyte or other dissolved species at high efficiencies and/or low energetic cost. In some cases, redox mediators are used to temporally decouple direct electrochemical processes from the production of the chemical product.

Inventors:: Voskian, Sahag; Murray, Alexander; Hatton, Trevor Alan; Surendranath, Yogesh

Issue Date:: 2022-02-01

Research Org.:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1892578

Patent Number(s):: 11236429

Application Number:: 16/450,859

Assignee:: Massachusetts Institute of Technology (Cambridge, MA)

Patent Classifications (CPCs):: C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25B - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS

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C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25B - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS
C25B1/13 - of ozone
C25B1/30 - Peroxides
C25B15/08 - Supplying or removing reactants or electrolytes

Show less

DOE Contract Number:: AC05-76RL01830

Resource Type:: Patent

Resource Relation:: Patent File Date: 06/24/2019

Country of Publication:: United States

Language:: English

Citation Formats


                    Voskian, Sahag, Murray, Alexander, Hatton, Trevor Alan, and Surendranath, Yogesh. Production of chemical products using electrochemical flow systems and slug flow and associated methods.  United States: N. p., 2022. 
        Web.

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                    Voskian, Sahag, Murray, Alexander, Hatton, Trevor Alan, & Surendranath, Yogesh. Production of chemical products using electrochemical flow systems and slug flow and associated methods.  United States.

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                    Voskian, Sahag, Murray, Alexander, Hatton, Trevor Alan, and Surendranath, Yogesh. Tue .  
        "Production of chemical products using electrochemical flow systems and slug flow and associated methods".  United States.  https://www.osti.gov/servlets/purl/1892578.

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@article{osti_1892578,

  title        = {Production of chemical products using electrochemical flow systems and slug flow and associated methods},

  author       = {Voskian, Sahag and Murray, Alexander and Hatton, Trevor Alan and Surendranath, Yogesh},

  abstractNote = {Systems and methods for electrochemically producing chemical products are provided. In certain cases, the systems and methods described herein are capable of producing chemical products such as hydrogen peroxide in solutions with relatively low concentrations of electrolyte or other dissolved species at high efficiencies and/or low energetic cost. In some cases, redox mediators are used to temporally decouple direct electrochemical processes from the production of the chemical product.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2022},

  month        = {2}

}

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Works referenced in this record:

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Yang, Sungeun; Verdaguer-Casadevall, Arnau; Arnarson, Logi
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Alkaline Quinone Flow Battery with Long Lifetime at pH 12
journal, September 2018

Kwabi, David G.; Lin, Kaixiang; Ji, Yunlong
Joule, Vol. 2, Issue 9
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High-Yield Electrosynthesis of Hydrogen Peroxide from Oxygen Reduction by Hierarchically Porous Carbon
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Electrosynthesis of Hydrogen Peroxide by Phase-Transfer Catalysis
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Similar Records

Title: Production of chemical products using electrochemical flow systems and slug flow and associated methods

Abstract

Citation Formats

Process for on-site production of ultra-high-purity hydrogen peroxide for the electronics industry patent, August 2001

Applications of Transition-Metal Catalysts to Textile and Wood-Pulp Bleaching journal, January 2006

Chemical Process patent-application, January 2007

Production of Chemical Products Using Electrochemical Flow Systems and Mediators and Associated Methods patent-application, February 2020

Erratum: Enabling direct H2O2 production through rational electrocatalyst design journal, January 2014

Method of making hydrogen peroxide patent, January 1978

Electrochemical oxygen reduction catalysed by Ni3(hexaiminotriphenylene)2 journal, March 2016

Decoupling hydrogen and oxygen evolution during electrolytic water splitting using an electron-coupled-proton buffer journal, April 2013

Polyanthraquinone as a Reliable Organic Electrode for Stable and Fast Lithium Storage journal, September 2015

Toward the Decentralized Electrochemical Production of H 2 O 2 : A Focus on the Catalysis journal, March 2018

Alkaline Quinone Flow Battery with Long Lifetime at pH 12 journal, September 2018

High-Yield Electrosynthesis of Hydrogen Peroxide from Oxygen Reduction by Hierarchically Porous Carbon journal, April 2015

Electrosynthesis of Hydrogen Peroxide by Phase-Transfer Catalysis journal, December 2019

Recovering zinc from a material containing zinc and iron patent, November 1978

Cooperative Electrocatalytic O 2 Reduction Involving Co(salophen) with p- Hydroquinone as an Electron–Proton Transfer Mediator journal, December 2017

Alloy Catalyst Metal patent-application, March 2016

Electrochemical process for gas separation patent-application, April 2017

Molecular Catalysis of Electrochemical Reactions. Mechanistic Aspects journal, July 2008

Redox catalysis in organic electrosynthesis: basic principles and recent developments journal, January 2014

Development of a reactor with carbon catalysts for modular-scale, low-cost electrochemical generation of H 2 O 2 journal, January 2017

A Bio-Inspired, Small Molecule Electron-Coupled-Proton Buffer for Decoupling the Half-Reactions of Electrolytic Water Splitting journal, September 2013

Chemical and Technical Aspects of Propene Oxide Production via Hydrogen Peroxide (HPPO Process) journal, January 2013

A metal-free organic–inorganic aqueous flow battery journal, January 2014

A Model of a Phase Transfer Catalyst Liquid/Liquid Electrochemical Membrane Reactor book, January 1995

Advances in the direct synthesis of hydrogen peroxide from hydrogen and oxygen journal, June 2015

Manufacture of Hydrogen Peroxide patent, March 1941

Poly(anthraquinone)s Having a .pi.-Conjugation System along the Main Chain. Synthesis by Organometallic Polycondensation, Redox Behavior, and Optical Properties journal, April 1995

A practical, organic-mediated, hybrid electrolyser that decouples hydrogen production at high current densities journal, January 2018

Regenerative fuel cell with catholyte comprising a polyoxometalate and a vanadium (IV) - compound patent-application, January 2014

Process for on-site production of ultra-high-purity hydrogen peroxide for the electronics industry
patent, August 2001

Applications of Transition-Metal Catalysts to Textile and Wood-Pulp Bleaching
journal, January 2006

Chemical Process
patent-application, January 2007

Production of Chemical Products Using Electrochemical Flow Systems and Mediators and Associated Methods
patent-application, February 2020

Erratum: Enabling direct H2O2 production through rational electrocatalyst design
journal, January 2014

Method of making hydrogen peroxide
patent, January 1978

Electrochemical oxygen reduction catalysed by Ni3(hexaiminotriphenylene)2
journal, March 2016

Decoupling hydrogen and oxygen evolution during electrolytic water splitting using an electron-coupled-proton buffer
journal, April 2013

Polyanthraquinone as a Reliable Organic Electrode for Stable and Fast Lithium Storage
journal, September 2015

Toward the Decentralized Electrochemical Production of H ₂ O ₂ : A Focus on the Catalysis
journal, March 2018

Alkaline Quinone Flow Battery with Long Lifetime at pH 12
journal, September 2018

High-Yield Electrosynthesis of Hydrogen Peroxide from Oxygen Reduction by Hierarchically Porous Carbon
journal, April 2015

Electrosynthesis of Hydrogen Peroxide by Phase-Transfer Catalysis
journal, December 2019

Recovering zinc from a material containing zinc and iron
patent, November 1978

Cooperative Electrocatalytic O ₂ Reduction Involving Co(salophen) with p- Hydroquinone as an Electron–Proton Transfer Mediator
journal, December 2017

Alloy Catalyst Metal
patent-application, March 2016

Electrochemical process for gas separation
patent-application, April 2017

Molecular Catalysis of Electrochemical Reactions. Mechanistic Aspects
journal, July 2008

Redox catalysis in organic electrosynthesis: basic principles and recent developments
journal, January 2014

Development of a reactor with carbon catalysts for modular-scale, low-cost electrochemical generation of H ₂ O ₂
journal, January 2017

A Bio-Inspired, Small Molecule Electron-Coupled-Proton Buffer for Decoupling the Half-Reactions of Electrolytic Water Splitting
journal, September 2013

Chemical and Technical Aspects of Propene Oxide Production via Hydrogen Peroxide (HPPO Process)
journal, January 2013

A metal-free organic–inorganic aqueous flow battery
journal, January 2014

A Model of a Phase Transfer Catalyst Liquid/Liquid Electrochemical Membrane Reactor
book, January 1995

Advances in the direct synthesis of hydrogen peroxide from hydrogen and oxygen
journal, June 2015

Manufacture of Hydrogen Peroxide
patent, March 1941

Poly(anthraquinone)s Having a .pi.-Conjugation System along the Main Chain. Synthesis by Organometallic Polycondensation, Redox Behavior, and Optical Properties
journal, April 1995

A practical, organic-mediated, hybrid electrolyser that decouples hydrogen production at high current densities
journal, January 2018

Regenerative fuel cell with catholyte comprising a polyoxometalate and a vanadium (IV) - compound
patent-application, January 2014