Title: Direct synthesis of high-aspect ratio zeolite nanosheets

Abstract

An example material includes a planar layer of MFI zeolite. The planar layer has a thickness in a range between 4 nm and 10 nm for at least 70% of a basal area of the planar layer. In one embodiment, the planar layer includes an embedded particle of an MFI zeolite.

Inventors:

Tsapatsis, Michael; Jeon, Mi Young; Lee, Pyung-Soo; Kim, Donghun; Kumar, Prashant; Mkhoyan, K. Andre; Siepmann, Joern Ilja

Issue Date:

Tue Jul 20 00:00:00 EDT 2021

Research Org.:

Univ. of Minnesota, Minneapolis, MN (United States)

Sponsoring Org.:

USDOE

OSTI Identifier:

1840271

Patent Number(s):

11066309

Application Number:

15/791,876

Assignee:

Regents of the University of Minnesota (Minneapolis, MN)

Patent Classifications (CPCs):

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY

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B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION

B01D2256/24 - Hydrocarbons
B01D2257/7022 - Aliphatic hydrocarbons
B01D2257/7027 - Aromatic hydrocarbons
B01D2323/36 - Introduction of specific chemical groups
B01D2325/02 - Details relating to pores or pososity of the membranes
B01D53/228 - {characterised by specific membranes}
B01D61/362 - {Pervaporation}
B01D67/0051 - {by controlled crystallisation, e,.g. hydrothermal growth}
B01D67/0086 - {Mechanical after-treatment}
B01D69/02 - characterised by their properties
B01D69/06 - Flat membranes
B01D71/028 - {Molecular sieves, e.g. zeolites, silicalite

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY

B01J20/18 - Synthetic zeolitic molecular sieves
B01J20/28033 - {Membrane, sheet, cloth, pad, lamellar or mat}
B01J29/40 - of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

C01B39/026 - {After-treatment}
C01B39/04 - using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
C01B39/38 - Type ZSM-5
C01B39/40 - using at least one organic template directing agent
C01B39/48 - using at least one organic template directing agent

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS

C01P2002/90 - Other crystal-structural characteristics not specified above
C01P2004/24 - Nanoplates, i.e. plate-like particles with a thickness from 1-100 nanometer
C01P2004/90 - Other morphology not specified above
C01P2006/16 - Pore diameter

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DOE Contract Number:  

AR0000338

Resource Type:

Patent

Resource Relation:

Patent File Date: 10/24/2017

Country of Publication:

United States

Language:

English