DOE Patents title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Methods for producing metal carbide materials

Abstract

Methods of producing silicon carbide, and other metal carbide materials. The method comprises reacting a carbon material (e.g., fibers, or nanoparticles, such as powder, platelet, foam, nanofiber, nanorod, nanotube, whisker, graphene (e.g., graphite), fullerene, or hydrocarbon) and a metal or metal oxide source material (e.g., in gaseous form) in a reaction chamber at an elevated temperature ranging up to approximately 2400° C. or more, depending on the particular metal or metal oxide, and the desired metal carbide being produced. A partial pressure of oxygen in the reaction chamber is maintained at less than approximately 1.01×102 Pascal, and overall pressure is maintained at approximately 1 atm.

Inventors:
;
Issue Date:
Research Org.:
Idaho National Lab. (INL), Idaho Falls, ID (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1805650
Patent Number(s):
10954167
Application Number:
16/261,246
Assignee:
Advanced Ceramic Fibers, LLC (Idaho Falls, ID)
DOE Contract Number:  
AC07-05ID14517
Resource Type:
Patent
Resource Relation:
Patent File Date: 01/29/2019
Country of Publication:
United States
Language:
English

Citation Formats

Garnier, John E., and Griffith, George W. Methods for producing metal carbide materials. United States: N. p., 2021. Web.
Garnier, John E., & Griffith, George W. Methods for producing metal carbide materials. United States.
Garnier, John E., and Griffith, George W. Tue . "Methods for producing metal carbide materials". United States. https://www.osti.gov/servlets/purl/1805650.
@article{osti_1805650,
title = {Methods for producing metal carbide materials},
author = {Garnier, John E. and Griffith, George W.},
abstractNote = {Methods of producing silicon carbide, and other metal carbide materials. The method comprises reacting a carbon material (e.g., fibers, or nanoparticles, such as powder, platelet, foam, nanofiber, nanorod, nanotube, whisker, graphene (e.g., graphite), fullerene, or hydrocarbon) and a metal or metal oxide source material (e.g., in gaseous form) in a reaction chamber at an elevated temperature ranging up to approximately 2400° C. or more, depending on the particular metal or metal oxide, and the desired metal carbide being produced. A partial pressure of oxygen in the reaction chamber is maintained at less than approximately 1.01×102 Pascal, and overall pressure is maintained at approximately 1 atm.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2021},
month = {3}
}

Works referenced in this record:

Method of coating carbon fibers with a carbide
patent, August 1993


Process for producing silicon carbide fibers essentially devoid of whiskers
patent, August 2006


Composite articles comprising metal carbide fibers
patent, October 2019


Coated carbonaceous articles and method for making same
patent, July 1994


Method of Preparing Fibrous Silicon Carbide
patent, April 1966


Nuclear fuel element having a metal liner and a diffusion barrier
patent, May 1977


Manufacture of hexagonal boron nitride
patent, August 1978


Method of making metal carbide and nitride powders
patent, November 1988


Surface-Treated Lamination Structures
patent, April 1974


Process for making silicon carbide ceramic fibers
patent, October 1994


Electrostatic Spray Device
patent, February 1969


Non-oxide sintered ceramic fibers
patent, March 1990


Porous ceramic seals and method of making same
patent, June 1980


High yield manufacturing process for silicon carbide
patent, March 1993


Nuclear fuel element
patent, December 1975


Methods for producing silicon carbide architectural preforms
patent, March 2010


Oxidation resistant carbon and method for making same
patent, November 1994


Silicon carbide fibers and articles including same
patent, January 2015


Silicon carbide fibre and production thereof
patent, November 1991


Abrasive/abradable gas path seal system
patent, January 1986


Method for forming metal matrix composites having variable filler loadings and products produced thereby
patent, June 1991


Process for the production of tungsten carbide or mixed metal carbides
patent, February 1977


Nuclear fuel element having a composite coating
patent, September 1984


Process for coating carbon fibers with a carbide
patent, May 1990


Carbon fiber-reinforced light metal composites
patent, March 1988


Composite containing coated fibrous material
patent, December 1989


Hexagonal silicon carbide platelets and preforms and methods for making and using same
patent, July 1988


Oxidation resistant carbon and method for making same
patent, April 1994


Composite bodies and methods for making same
patent, September 2000


Article Containing Silicon Carbon Fibers
patent, June 1968


Process for coating carbon fibers with a carbide, and carbon fibers thus coated
patent, August 1989


Process for preparing silicon carbide by carbothermal reduction
patent, August 1994


Method of thermochemically treating silicon carbide fibers derived from polymers
patent, July 1993


Method of producing silicon carbide fibers
patent, October 1997


Process for Making Nuclear Fuel Element
patent, January 1965


Wear resistant coating for fuel cladding
patent, December 1993


Oxidation-resistant interfacial coating for fiber-reinforced ceramic
patent, November 2001


Process for the Formation of Metal Carbide and Metal Carbide Plus Carbon Microspheres
patent, October 1973


Whisker reinforced composites for cutting tools with improved performance
patent, October 1993


Incandescent light energy conversion with reduced infrared emission
patent, September 1998


Inorganic fibrous material as reinforcement for composite materials and process for production thereof
patent, September 1988


Non-oxide sintered ceramic fibers
patent, August 1992


Preparation of carbide nanorods
patent, December 1999


Manufacture of Silicon Carbide Fibers
patent, June 1969


Process for producing boron nitride
patent, March 2008


Continuous atmospheric pressure CVD coating of fibers
patent, November 1994


Preparation of hollow ceramic fibers
patent, August 1990


Boron Carbide Fiber Production
patent, July 1974


Single crystal whisker electric light filament
patent, September 1989


Process for producing silicon carbide fibers
patent, July 1999


Silicon carbide composite with coated fiber reinforcement
patent, September 1996


Silicon carbide fibers essentially devoid of whiskers and products made therefrom
patent, May 2006


Process for Producing Boron Nitride
patent-application, June 2006


High strength ceramic fibers and methods of fabrication
patent, August 2018


Protective coating with reactive interlayer on reinforcement in silicon carbide composite
patent, March 1994


Methods of producing continuous boron carbide fibers
patent, December 2015


Boron Carbide Fiber Production
patent, April 1973


Method for making hexagonal silicon carbide platelets with the addition of a growth additive
patent, April 1993


Precursor formulation of a silicon carbide material
patent, April 2010


Manufacture of Silicon Carbide
patent, July 1970


Preparation of SiC whiskers
patent, August 1981


Process for producing boron nitride
patent, June 1988


Boron nitride/silicon-containing ceramic materials
patent, November 1991


Methods for producing silicon carbide fibers
patent, March 2016


Process to produce silicon carbide fibers using a controlled concentration of boron oxide vapor
patent, July 2001


Filamentary silicon carbide crystals by VLS growth in molten iron
patent, March 1977


Process and Composition for the Production of Cemented Metal Carbides
patent, January 1970


Metal carbide, nitride, or carbonitride whiskers coated with metal carbides, nitrides, carbonitrides, or oxides
patent, January 1991


Process for producing silicon carbide
patent, February 2000


Process for coating a part with an oxidation-protective coating
patent, October 2016


Article and method for making complex shaped preform and silicon carbide composite by melt infiltration
patent, February 2000


Method of producing single-crystal silicon carbide
patent, August 2000


Method for preparing a boron nitride composite
patent, February 1997


Submicron Silicon Carbide
patent, March 1965


Method for making fuel cladding having zirconium barrier layers and inner liners
patent, January 1995


Process for Producing Coatings on Carbon and Graphite Filaments
patent, February 1968


Gas turbine engine and composite parts
patent, December 1986


Method for providing a silicon carbide matrix in carbon-fiber reinforced composites
patent, November 1991


Polycrystalline silicon carbide fibers
patent, November 1994


Amorphous boron-carbon alloy in bulk form and methods of making the same
patent, September 1980


Continuous atomspheric pressure CVD coating of fibers
patent, August 1996


Process for producing silicon carbide material
patent, April 1997


Process for producing reinforcing SiC fiber for SiC composite material
patent, October 2006


Hexagonal boron nitride powder having excellent sinterability and a method for the preparation thereof
patent, November 1988


Coating fibers with a layer of silicon
patent, November 1990


Ceramic hot gas filter
patent, October 1995


Activated carbon fiber composite material and method of making
patent, February 2000


Ceramic fiber-reinforced composite articles and their production
patent, July 1995


Method for forming nuclear fuel containers of a composite construction and the product thereof
patent, May 1984


Nuclear Fuel Elements
patent, February 1969


Dispersions of silica in carbon and a method of making such dispersions
patent, October 1990


Methods of making composite ceramic articles having embedded filler
patent, July 1989


Nuclear fuel elements having a composite cladding
patent, September 1983


Method of Producing Crystalline Silicon Carbide Whiskers
patent, May 1974


Process for producing silicon carbide fiber
patent, November 2001


Ultra-refractory material that is stable in a wet environment, and process for manufacturing same
patent, May 2016


Method of making carbon fiber-carbon matrix reinforced ceramic composites
patent, November 2007


Process for producing silicon carbide and metal carbides
patent, August 1990


Hydride damage resistant fuel elements
patent, July 1995