Methods for synthesizing high purity niobium or rhenium powders
Abstract
Methods are provided for synthesizing high purity niobium or rhenium powders by a combustion reaction. The methods can include: forming a combustion synthesis solution by dissolving in water an oxidizer, a fuel, and at least one base-soluble, ammonium salt of niobium or rhenium in amounts that yield a stoichiometric burn when combusted; and heating the combustion synthesis solution to a temperature sufficient to substantially remove the water and to initiate a self-sustaining combustion reaction.
- Inventors:
- Issue Date:
- Research Org.:
- Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1805571
- Patent Number(s):
- 10934605
- Application Number:
- 15/786,289
- Assignee:
- Battelle Memorial Institute (Richland, WA)
- Patent Classifications (CPCs):
-
B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
- DOE Contract Number:
- AC05-76RL01830
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 10/17/2017
- Country of Publication:
- United States
- Language:
- English
Citation Formats
Frye, Jr., John G., Weil, Kenneth Scott, Lavender, Curt A., and Kim, Jin Yong. Methods for synthesizing high purity niobium or rhenium powders. United States: N. p., 2021.
Web.
Frye, Jr., John G., Weil, Kenneth Scott, Lavender, Curt A., & Kim, Jin Yong. Methods for synthesizing high purity niobium or rhenium powders. United States.
Frye, Jr., John G., Weil, Kenneth Scott, Lavender, Curt A., and Kim, Jin Yong. Tue .
"Methods for synthesizing high purity niobium or rhenium powders". United States. https://www.osti.gov/servlets/purl/1805571.
@article{osti_1805571,
title = {Methods for synthesizing high purity niobium or rhenium powders},
author = {Frye, Jr., John G. and Weil, Kenneth Scott and Lavender, Curt A. and Kim, Jin Yong},
abstractNote = {Methods are provided for synthesizing high purity niobium or rhenium powders by a combustion reaction. The methods can include: forming a combustion synthesis solution by dissolving in water an oxidizer, a fuel, and at least one base-soluble, ammonium salt of niobium or rhenium in amounts that yield a stoichiometric burn when combusted; and heating the combustion synthesis solution to a temperature sufficient to substantially remove the water and to initiate a self-sustaining combustion reaction.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2021},
month = {3}
}
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.
Works referenced in this record:
Tungsten alloy high temperature tool materials
patent-application, June 2005
- Ohriner, Evan K.; David, Stan A.
- US Patent Document 10/735974; 20050129565
Scintillator nanoparticles and method of making
patent, November 2008
- Krishna, Kalaga Murali; Loureiro, Sergio Paulo Martins; Manoharan, Mohan
- US Patent Document 7,449,128
Method for Preparation of Rhenium
patent, May 1960
- Campbell, Ivor Eugene; Mees, Danny
- US Patent Document 2,935,399
Tungsten rhenium compounds and composites and methods for forming the same
patent, January 2013
- Liu, Qingyuan; Steel, Russell J.; Packer, Scott M.
- US Patent Document 8,361,178
Scintillator Nanoparticles and Method of Making
patent-application, October 2008
- Krishna, Kalaga Murali; Loureiro, Sergio Paulo Martins; Manoharan, Mohan
- US Patent Application 10/872867; 20080246004
Plasma arc reactor for the production of fine powders
patent-application, May 2003
- Deegan, David Edward; Chapman, Chris David; Johnson, Timothy Paul
- US Patent Application 10/203467; 20030097903
Plasma arc reactor for the production of fine powders
patent, April 2006
- Deegan, David; Chapman, Chris; Johnson, Timothy P.
- US Patent Document 7,022,155
Ceramic precursor mixture and technique for converting the same to ceramic
patent, October 1991
- Aksay, Ilhan A.; Han, Chan; Maupin, Gary D.
- US Patent Document 5,061,682
Solution method for making molybdate and tungstate negative thermal expansion materials and compounds made by the method
patent, February 2001
- Sleight, Arthur W.; Closmann, Claire E.; Haygarth, John C.
- US Patent Document 6,183,716
Refractory Metal Tool for Friction Stir Welding Comprising a Shoulder Made of Tungsten, Molybdenum, Tantalum, Niobium, or Hafnium Alloy and a Coated or Treated Surface
patent-application, November 2010
- Rowe, Charles E. D.; Tuck, Jonathan R.; Staines, David George
- US Patent Document 12/377702; 20100279146
Method of Preparing Lead and Alkaline Earth Titanates and Niobates and Coating Method Using the Same to Form a Capacitor
patent, July 1967
- Pechini, Maggio P.
- US Patent Document 3,330,697
Apparatus and method for friction stir welding of high strength materials, and articles made therefrom
patent, April 2006
- Subramanian, Pazhayannur Ramanathan; Bewlay, Bernard Patrick; Helder, Earl Claude
- US Patent Document 7,032,800
Crystalline multinary metal oxide compositions, process for preparing and processes for using the composition
patent, January 2001
- Bedard, Robert L.; Bogdan, Paula L.; King, Lisa M.
- US Patent Document 6,171,571
Apparatus and method for friction stir welding of high strength materials, and articles made therefrom
patent, March 2008
- Subramanian, Pazhayannur Ramanathan; Bewlay, Bernard Patrick; Helder, Earl Claude
- US Patent Document 7,337,940
Method of making metal oxide ceramic powders by using a combustible amino acid compound
patent, May 1992
- Pederson, Larry R.; Chick, Lawrence A.; Exarhos, Gregory J.
- US Patent Document 5,114,702
Process for preparing fine metal oxide particles
patent-application, August 2006
- Myeong, Wan-Jae; Baik, Jin-Soo; Park, Se-Woong
- US Patent Application 10/521642; 20060182677
Single step process for the synthesis of nanoparticles of ceramic oxide powders
patent, December 2004
- James, Jose; Jose, Rajan; John, Asha Mary
- US Patent Document 6,835,367
Combustion of emulsions: A method and process for producing fine powders
patent, November 1999
- Bickmore, Clint; Galde, Benjamin; Yadav, Tapesh
- US Patent Document 5,984,997
Process for plasma synthesis of rhenium nano and micro powders, and for coatings and near net shape deposits thereof and apparatus therefor
patent-application, September 2005
- Jurewicz, Jerzy W.; Guo, Jiayin
- US Patent Document 11/041870; 20050211018
Ceramic oxide powder, method for producing the ceramic oxide powder, ceramic paste produced using the ceramic oxide powder, and method for producing the ceramic paste
patent, November 2001
- Yun, Sang Kyeong; Kim, Dong-Hoon; Jung, Yeon-kyoung
- US Patent Document 6,319,421
Method of Making Nanocrystalline Tungsten Powder
patent-application, September 2008
- Lunk, Hans-Joachim; Stevens, Henry J.
- US Patent Document 12/036507; 20080223175
High strength and toughness steel structures by friction stir welding
patent-application, June 2010
- Ayer, Raghavan; Fairchild, Douglas Paul; Ford, Steven Jeffrey
- US Patent Document 12/590956; 20100136369
Process for making ultra-fine ceramic particles
patent, November 1995
- Stangle, Gregory C.; Venkatachari, Koththavasal R.; Ostrander, Steven P.
- US Patent Document 5,468,427
Production of Nanocrystalline Metal Powders via Combustion Reaction Synthesis
patent-application, August 2011
- Frye, John G.; Weil, Kenneth Scott; Lavender, Curt A.
- US Patent Document 12/700923; 20110194970
Preparation of tungsten oxide
patent-application, February 2005
- Bulian, Christopher J.; Dye, Robert C.; Son, Steven F.
- US Patent Document 10/629489; 20050025700