Atmospheric-pressure ionization and fragmentation of molecules for structural elucidation
Abstract
A solution-cathode glow discharge (SCGD) spectrometry apparatus may comprise an SCGD source and a mass or ion mobility spectrometer. A method for ionizing a molecular analyte may comprise contacting the molecular analyte with a plasma discharge to form ions and separating the ions in a mass spectrometer or ion mobility spectrometer. The contacting step may occur under atmospheric pressure and/or ambient conditions. The molecular analyte may be fragmented by the plasma discharge.
- Inventors:
- Issue Date:
- Research Org.:
- Indiana Univ., Indianapolis, IN (United States); Kent State Univ., Kent, OH (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1735298
- Patent Number(s):
- 10784097
- Application Number:
- 15/756,011
- Assignee:
- Indiana University Research and Technology Corporation (Indianapolis, IN); Kent State University (Kent, OH)
- Patent Classifications (CPCs):
-
H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01J - ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- DOE Contract Number:
- FG02-98ER14890
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 08/28/2016
- Country of Publication:
- United States
- Language:
- English
Citation Formats
Shelley, Jacob T., Williams, Kelsey L., Hieftje, Gary M., and Schwartz, Andrew J. Atmospheric-pressure ionization and fragmentation of molecules for structural elucidation. United States: N. p., 2020.
Web.
Shelley, Jacob T., Williams, Kelsey L., Hieftje, Gary M., & Schwartz, Andrew J. Atmospheric-pressure ionization and fragmentation of molecules for structural elucidation. United States.
Shelley, Jacob T., Williams, Kelsey L., Hieftje, Gary M., and Schwartz, Andrew J. Tue .
"Atmospheric-pressure ionization and fragmentation of molecules for structural elucidation". United States. https://www.osti.gov/servlets/purl/1735298.
@article{osti_1735298,
title = {Atmospheric-pressure ionization and fragmentation of molecules for structural elucidation},
author = {Shelley, Jacob T. and Williams, Kelsey L. and Hieftje, Gary M. and Schwartz, Andrew J.},
abstractNote = {A solution-cathode glow discharge (SCGD) spectrometry apparatus may comprise an SCGD source and a mass or ion mobility spectrometer. A method for ionizing a molecular analyte may comprise contacting the molecular analyte with a plasma discharge to form ions and separating the ions in a mass spectrometer or ion mobility spectrometer. The contacting step may occur under atmospheric pressure and/or ambient conditions. The molecular analyte may be fragmented by the plasma discharge.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2020},
month = {9}
}
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Works referenced in this record:
Spectroscopic characterization of ion and electron populations in a solution-cathode glow discharge
journal, January 2006
- Webb, Michael R.; Chan, George C. -Y.; Andrade, Francisco J.
- Journal of Analytical Atomic Spectrometry, Vol. 21, Issue 5