Methods of producing metal sulfides, metal selenides, and metal sulfides/selenides having controlled architectures using kinetic control

Owen, Jonathan S.; Hendricks, Mark P.; Campos, Michael P.; Cleveland, Gregory T.; Plante, Ilan Jen-La; Hamachi, Leslie Sachiyo

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Title: Methods of producing metal sulfides, metal selenides, and metal sulfides/selenides having controlled architectures using kinetic control

Abstract

The present invention is directed to methods of preparing metal sulfide, metal selenide, or metal sulfide/selenide nanoparticles and the products derived therefrom. In various embodiments, the nanoparticles are derived from the reaction between precursor metal salts and certain sulfur- and/or selenium-containing precursors each independently having a structure of Formula (I), (II), or (III), or an isomer, salt, or tautomer thereof, where Q1, Q2, Q3, R1, R2, R3, R5, and X are defined within the specification.

Inventors:: Owen, Jonathan S.; Hendricks, Mark P.; Campos, Michael P.; Cleveland, Gregory T.; Plante, Ilan Jen-La; Hamachi, Leslie Sachiyo

Issue Date:: 2020-09-08

Research Org.:: Columbia Univ., New York, NY (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1735228

Patent Number(s):: 10767112

Application Number:: 15/541,937

Assignee:: The Trustees of Columbia University in the City of New York (New York, NY)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

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B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
B82Y20/00 - Nanooptics, e.g. quantum optics or photonic crystals
B82Y30/00 - Nanotechnology for materials or surface science, e.g. nanocomposites
B82Y40/00 - Manufacture or treatment of nanostructures

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B19/007 - {Tellurides or selenides of metals
C01B19/04 - Binary compounds {including binary selenium-tellurium compounds

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
C01G1/12 - Sulfides
C01G11/02 - Sulfides
C01G19/00 - Compounds of tin
C01G19/006 - {Compounds containing, besides tin, two or more other elements, with the exception of oxygen or hydrogen}
C01G21/21 - Sulfides
C01G3/12 - Sulfides
C01G53/11 - Sulfides
C01G9/08 - Sulfides

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
C01P2002/72 - by d-values or two theta-values, e.g. as X-ray diagram
C01P2002/84 - by UV- or VIS- data
C01P2004/04 - obtained by TEM, STEM, STM or AFM
C01P2004/16 - Nanowires or nanorods, i.e. solid nanofibres with two nearly equal dimensions between 1-100 nanometer
C01P2004/24 - Nanoplates, i.e. plate-like particles with a thickness from 1-100 nanometer
C01P2004/32 - Spheres
C01P2004/64 - Nanometer sized, i.e. from 1-100 nanometer
C01P2004/80 - Particles consisting of a mixture of two or more inorganic phases

C - CHEMISTRY C09 - DYES C09K - MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
C09K11/565 - {with zinc cadmium}
C09K11/582 - {Chalcogenides}
C09K11/602 - {Chalcogenides}
C09K11/661 - {Chalcogenides}
C09K11/881 - {Chalcogenides}
C09K11/883 - {with zinc or cadmium}

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01L - SEMICONDUCTOR DEVICES
H01L33/04 - with a quantum effect structure or superlattice, e.g. tunnel junction

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10S - TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
Y10S977/774 - Exhibiting three-dimensional carrier confinement, e.g. quantum dots
Y10S977/824 - Group II-VI nonoxide compounds, e.g. CdxMnyTe
Y10S977/825 - Heterojunction formed between semiconductor materials that differ in that they belong to different periodic table groups
Y10S977/892 - Liquid phase deposition
Y10S977/896 - Chemical synthesis, e.g. chemical bonding or breaking
Y10S977/95 - Electromagnetic energy

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DOE Contract Number:: SC0001085; SC0006410

Resource Type:: Patent

Resource Relation:: Patent File Date: 01/15/2016

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; 77 NANOSCIENCE AND NANOTECHNOLOGY

Citation Formats


                    Owen, Jonathan S., Hendricks, Mark P., Campos, Michael P., Cleveland, Gregory T., Plante, Ilan Jen-La, and Hamachi, Leslie Sachiyo. Methods of producing metal sulfides, metal selenides, and metal sulfides/selenides having controlled architectures using kinetic control.  United States: N. p., 2020. 
        Web.

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                    Owen, Jonathan S., Hendricks, Mark P., Campos, Michael P., Cleveland, Gregory T., Plante, Ilan Jen-La, & Hamachi, Leslie Sachiyo. Methods of producing metal sulfides, metal selenides, and metal sulfides/selenides having controlled architectures using kinetic control.  United States.

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                    Owen, Jonathan S., Hendricks, Mark P., Campos, Michael P., Cleveland, Gregory T., Plante, Ilan Jen-La, and Hamachi, Leslie Sachiyo. Tue .  
        "Methods of producing metal sulfides, metal selenides, and metal sulfides/selenides having controlled architectures using kinetic control".  United States.  https://www.osti.gov/servlets/purl/1735228.

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@article{osti_1735228,

  title        = {Methods of producing metal sulfides, metal selenides, and metal sulfides/selenides having controlled architectures using kinetic control},

  author       = {Owen, Jonathan S. and Hendricks, Mark P. and Campos, Michael P. and Cleveland, Gregory T. and Plante, Ilan Jen-La and Hamachi, Leslie Sachiyo},

  abstractNote = {The present invention is directed to methods of preparing metal sulfide, metal selenide, or metal sulfide/selenide nanoparticles and the products derived therefrom. In various embodiments, the nanoparticles are derived from the reaction between precursor metal salts and certain sulfur- and/or selenium-containing precursors each independently having a structure of Formula (I), (II), or (III), or an isomer, salt, or tautomer thereof, where Q1, Q2, Q3, R1, R2, R3, R5, and X are defined within the specification.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2020},

  month        = {9}

}

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Works referenced in this record:

Method for Preparing Nanoparticles Using Carbene Derivatives
patent-application, November 2009

Jang, Eun Joo; Son, Seung Uk
US Patent Application 12/329058; 20090289233
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Aqueous process for producing crystalline copper chalcogenide nanoparticles, the nanoparticles so-produced, and inks and coated substrates incorporating the nanoparticles
patent, June 2013

Radu, Daniela Rodica; Johnson, Lynda Kaye; Lai, Cheng-Yu
US Patent Document 8,470,636
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Passive Q-Switch Laser
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Galun, Ehud; Lifshitz, Efrat; Sirota, Marina
US Patent Application 11/132037; 20050254528
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Method of Producing Sulfide Compound Semiconductor by Use of Solvothermal Method and Rod-Like Crystal of Sulfide Compound Semiconductor
patent-application, April 2014

Kamiya, Sumio; Kishita, Keisuke; Yanagisawa, Kazumichi
US Patent Application 14/124156; 20140110640
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Method for Synthesizing Nanoparticles of Metal Sulfides
patent-application, February 2005

Hyeon, Taegwhan
US Patent Application 10/641394; 20050036938
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Synthesis and Use of [Cd(Detu) ₂ (OOCCH ₃ ) ₂ ]·H ₂ O as Single Molecule Precursor for Cds Nanoparticles
journal, January 2013

Ajibade, Peter A.
The Scientific World Journal, Vol. 2013
https://doi.org/10.1155/2013/907562

A tunable library of substituted thiourea precursors to metal sulfide nanocrystals
journal, June 2015

Hendricks, M. P.; Campos, M. P.; Cleveland, G. T.
Science, Vol. 348, Issue 6240
https://doi.org/10.1126/science.aaa2951

Synthesis of PB Alloy and Core/Shell Nanowires
patent-application, January 2011

Mokari, Taleb; Zhang, Minjuan; Yang, Peidong
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Use of sulfur and selenium compounds as precursors to nanostructured materials
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Owen, Jonathan S.; Hendricks, Mark P.; Campos, Michael P.
US Patent Document 10,253,256
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Synthesis of High-Quality Metal Sulfide Nanoparticles from Alkyl Xanthate Single Precursors in Alkylamine Solvents
journal, December 2003

Pradhan, Narayan; Katz, Beni; Efrima, Shlomo
The Journal of Physical Chemistry B, Vol. 107, Issue 50
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Control of the Morphology and Size of PbS Nanowires Using Gold Nanoparticles
journal, December 2006

Yong, Ken-Tye; Sahoo, Yudhisthira; Choudhury, Kaushik Roy
Chemistry of Materials, Vol. 18, Issue 25
https://doi.org/10.1021/cm061771q

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Similar Records

Title: Methods of producing metal sulfides, metal selenides, and metal sulfides/selenides having controlled architectures using kinetic control

Abstract

Citation Formats

Method for Preparing Nanoparticles Using Carbene Derivatives patent-application, November 2009

Aqueous process for producing crystalline copper chalcogenide nanoparticles, the nanoparticles so-produced, and inks and coated substrates incorporating the nanoparticles patent, June 2013

Passive Q-Switch Laser patent-application, November 2005

Method of Producing Sulfide Compound Semiconductor by Use of Solvothermal Method and Rod-Like Crystal of Sulfide Compound Semiconductor patent-application, April 2014

Method for Synthesizing Nanoparticles of Metal Sulfides patent-application, February 2005

Synthesis and Use of [Cd(Detu) 2 (OOCCH 3 ) 2 ]·H 2 O as Single Molecule Precursor for Cds Nanoparticles journal, January 2013

A tunable library of substituted thiourea precursors to metal sulfide nanocrystals journal, June 2015

Synthesis of PB Alloy and Core/Shell Nanowires patent-application, January 2011

Use of sulfur and selenium compounds as precursors to nanostructured materials patent, April 2019

Synthesis of High-Quality Metal Sulfide Nanoparticles from Alkyl Xanthate Single Precursors in Alkylamine Solvents journal, December 2003

Control of the Morphology and Size of PbS Nanowires Using Gold Nanoparticles journal, December 2006

Method for Preparing Nanoparticles Using Carbene Derivatives
patent-application, November 2009

Aqueous process for producing crystalline copper chalcogenide nanoparticles, the nanoparticles so-produced, and inks and coated substrates incorporating the nanoparticles
patent, June 2013

Passive Q-Switch Laser
patent-application, November 2005

Method of Producing Sulfide Compound Semiconductor by Use of Solvothermal Method and Rod-Like Crystal of Sulfide Compound Semiconductor
patent-application, April 2014

Method for Synthesizing Nanoparticles of Metal Sulfides
patent-application, February 2005

Synthesis and Use of [Cd(Detu) ₂ (OOCCH ₃ ) ₂ ]·H ₂ O as Single Molecule Precursor for Cds Nanoparticles
journal, January 2013

A tunable library of substituted thiourea precursors to metal sulfide nanocrystals
journal, June 2015

Synthesis of PB Alloy and Core/Shell Nanowires
patent-application, January 2011

Use of sulfur and selenium compounds as precursors to nanostructured materials
patent, April 2019

Synthesis of High-Quality Metal Sulfide Nanoparticles from Alkyl Xanthate Single Precursors in Alkylamine Solvents
journal, December 2003

Control of the Morphology and Size of PbS Nanowires Using Gold Nanoparticles
journal, December 2006