Salts for multivalent ion batteries

Liao, Chen; Dzwiniel, Trevor L.; Pan, Baofei; Han, Sang-Don; Burrell, Anthony K.

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Title: Salts for multivalent ion batteries

Abstract

Methods for preparing electrolyte salts for alkaline earth metal-ion batteries (e.g., calcium and magnesium ion batteries) are described. The electrolyte salts comprise alkaline earth metal (e.g., Mg or Ca) salts of 3,4-dicyano-2-trifluoromethylimidazole (TDI). The methods comprise contacting TDI with an alkaline earth metal bis(trifluoroacetate) salt in trifluoroacetic acid.

Inventors:: Liao, Chen; Dzwiniel, Trevor L.; Pan, Baofei; Han, Sang-Don; Burrell, Anthony K.

Issue Date:: 2020-06-09

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1651010

Patent Number(s):: 10680285

Application Number:: 16/025,676

Assignee:: UChicago Argonne, LLC (Chicago, IL)

Patent Classifications (CPCs):: C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07D - HETEROCYCLIC COMPOUNDS

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C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B21/084 - containing also one or more oxygen atoms, e.g. nitrosyl halides
C01B21/086 - containing one or more sulfur atoms

C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07D - HETEROCYCLIC COMPOUNDS
C07D233/90 - Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
C07D233/93 - with hydrocarbon radicals, substituted by halogen atoms, attached to other ring members

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M10/054 - Accumulators with insertion or intercalation of metals other than lithium, e.g. with magnesium or aluminium
H01M10/0563 - Liquid materials, e.g. for Li-SOCl2 cells
H01M10/0568 - characterised by the solutes
H01M10/0569 - characterised by the solvents

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/10 - Energy storage

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DOE Contract Number:: AC02-06CH11357

Resource Type:: Patent

Resource Relation:: Patent File Date: 07/02/2018

Country of Publication:: United States

Language:: English

Subject:: 25 ENERGY STORAGE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats


                    Liao, Chen, Dzwiniel, Trevor L., Pan, Baofei, Han, Sang-Don, and Burrell, Anthony K. Salts for multivalent ion batteries.  United States: N. p., 2020. 
        Web.

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                    Liao, Chen, Dzwiniel, Trevor L., Pan, Baofei, Han, Sang-Don, & Burrell, Anthony K. Salts for multivalent ion batteries.  United States.

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                    Liao, Chen, Dzwiniel, Trevor L., Pan, Baofei, Han, Sang-Don, and Burrell, Anthony K. Tue .  
        "Salts for multivalent ion batteries".  United States.  https://www.osti.gov/servlets/purl/1651010.

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@article{osti_1651010,

  title        = {Salts for multivalent ion batteries},

  author       = {Liao, Chen and Dzwiniel, Trevor L. and Pan, Baofei and Han, Sang-Don and Burrell, Anthony K.},

  abstractNote = {Methods for preparing electrolyte salts for alkaline earth metal-ion batteries (e.g., calcium and magnesium ion batteries) are described. The electrolyte salts comprise alkaline earth metal (e.g., Mg or Ca) salts of 3,4-dicyano-2-trifluoromethylimidazole (TDI). The methods comprise contacting TDI with an alkaline earth metal bis(trifluoroacetate) salt in trifluoroacetic acid.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2020},

  month        = {6}

}

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Works referenced in this record:

Pentacyclic Anion Salt and Use Thereof as an Electrolyte
patent-application, December 2011

Armand, Michael; Grugeon, Sylvie; Laruelle, Stephane
US Patent Application 13/060,776; 2011/0311884 Al
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20110311884

Method for Producing Disulfonylamine Alkali Metal Salt
patent-application, January 2016

Maekawa, Hideki; Yasuhara, Masamichi; Hayashi, Ken-Ichi
US Patent Application 14/773964; 20160016797
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20160016797

Preparation of Imides Containing a Fluorosulfonyl Group
patent-application, February 2017

Schmidt, Gregory; Audureau, Sophie
US Patent Application 15/304577; 20170047607
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20170047607

Synthesis of bis(fluorosulfonyl)imide
patent, February 2013

Singh, Rajendra; Martin, Jerry L.; Poshusta, Joseph C.
US Patent Document 8,377,406
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8377406

Synthesis of Tetrabutylammonium Bis(fluorosulfonyl)imide and Related Salts
patent-application, May 2014

Johnson, Martin R.
US Patent Application 14/081817; 20140142338
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20140142338

Method for Producing Lithium or Sodium Bis(fluorosulfonyl)imide
patent-application, March 2014

Schmidt, Gregory
US Patent Application 14/115909; 20140075746
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20140075746

Method for preparing bis(fluorosulfonyl)imide acid and salts thereof
patent-application, October 2016

Buisine, Olivier
US Patent Application 15/101149; 20160308247
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20160308247

Method for Producing Imide Salt
patent-application, August 2014

Fukunaga, Atsushi; Inazawa, Shinji; Nitta, Koji
US Patent Application 14/352175; 20140241973
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20140241973

Fluorosulfonyl Imide Salt and Method for Producing Fluorosulfonyl Imide Salt
patent-application, February 2012

Sato, Shimpei; Okumura, Yasunori; Sato, Yuichi
US Patent Application 13/264244; 20120041233
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20120041233

Synthesis of hydrogen bis(fluorosulfonyl)imide
patent, May 2014

Poshusta, Joseph C.; Martin, Jerry L.; Singh, Rajendra
US Patent Document 8,722,005
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8722005

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Methods for preparing electrolyte salts for alkaline earth metal-ion batteries (e.g., calcium and magnesium ion batteries) are described. The electrolyte salts comprise alkaline earth metal (e.g., Mg or Ca) salts of bis(fluorosulfonyl)imide (FSI) and 3,4-dicyano-2-trifluoromethylimidazole (TDI). The methods comprise contacting FSI or TDI with an alkaline earth metal bis(trifluoroacetate) salt in trifluoroacetic acid.
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Similar Records

Title: Salts for multivalent ion batteries

Abstract

Citation Formats

Pentacyclic Anion Salt and Use Thereof as an Electrolyte patent-application, December 2011

Method for Producing Disulfonylamine Alkali Metal Salt patent-application, January 2016

Preparation of Imides Containing a Fluorosulfonyl Group patent-application, February 2017

Synthesis of bis(fluorosulfonyl)imide patent, February 2013

Synthesis of Tetrabutylammonium Bis(fluorosulfonyl)imide and Related Salts patent-application, May 2014

Method for Producing Lithium or Sodium Bis(fluorosulfonyl)imide patent-application, March 2014

Method for preparing bis(fluorosulfonyl)imide acid and salts thereof patent-application, October 2016

Method for Producing Imide Salt patent-application, August 2014

Fluorosulfonyl Imide Salt and Method for Producing Fluorosulfonyl Imide Salt patent-application, February 2012

Synthesis of hydrogen bis(fluorosulfonyl)imide patent, May 2014

Pentacyclic Anion Salt and Use Thereof as an Electrolyte
patent-application, December 2011

Method for Producing Disulfonylamine Alkali Metal Salt
patent-application, January 2016

Preparation of Imides Containing a Fluorosulfonyl Group
patent-application, February 2017

Synthesis of bis(fluorosulfonyl)imide
patent, February 2013

Synthesis of Tetrabutylammonium Bis(fluorosulfonyl)imide and Related Salts
patent-application, May 2014

Method for Producing Lithium or Sodium Bis(fluorosulfonyl)imide
patent-application, March 2014

Method for preparing bis(fluorosulfonyl)imide acid and salts thereof
patent-application, October 2016

Method for Producing Imide Salt
patent-application, August 2014

Fluorosulfonyl Imide Salt and Method for Producing Fluorosulfonyl Imide Salt
patent-application, February 2012

Synthesis of hydrogen bis(fluorosulfonyl)imide
patent, May 2014