Fabrication of films and coatings used to activate shear thickening, impact resistant electrolytes

Armstrong, Beth L.; Veith, Gabriel M.; Kalnaus, Sergiy; Wang, Hsin; Browning, Katie L.; Cooley, Kevin M.

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Title: Fabrication of films and coatings used to activate shear thickening, impact resistant electrolytes

Abstract

A method of making a passively impact resistant composite electrolyte and separator layer includes providing a suspension composition including electrically non-conducting particles that enable shear thickening. The particles can have a polydispersity index of no greater than 0.1, an average particle size in a range of from 50 nm to 1 um, and an absolute zeta potential of greater than ±40 mV. A particle suspension solvent is provided for suspending the particles. The suspension composition is applied to a porous separator material. A portion of the particles and suspension solvent penetrate the pores and the remainder of the particles in the suspension composition are distributed across the surface of the separator material. The suspension solvent is evaporated from the separator material to provide a shear thickening particle loaded separator. A separator assembly and a passivated battery are also disclosed.

Inventors:: Armstrong, Beth L.; Veith, Gabriel M.; Kalnaus, Sergiy; Wang, Hsin; Browning, Katie L.; Cooley, Kevin M.

Issue Date:: Tue Apr 28 00:00:00 EDT 2020

Research Org.:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1650837

Patent Number(s):: 10637100

Application Number:: 15/958,446

Assignee:: UT-Battelle, LLC (Oak Ridge, TN)

Patent Classifications (CPCs):: C - CHEMISTRY C04 - CEMENTS C04B - LIME, MAGNESIA

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY

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C - CHEMISTRY C04 - CEMENTS C04B - LIME, MAGNESIA
C04B41/88 - Metals

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M10/052 - Li-accumulators
H01M10/0567 - characterised by the additives
H01M10/0568 - characterised by the solutes
H01M10/0569 - characterised by the solvents
H01M2300/0028 - characterised by the solvent
H01M2300/0045 - Room temperature molten salts comprising at least one organic ion
H01M2300/0085 - Immobilising or gelification of electrolyte
H01M2300/0094 - in the form of layered products, e.g. coatings

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/10 - Energy storage

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DOE Contract Number:: AC05-00OR22725

Resource Type:: Patent

Resource Relation:: Patent File Date: 04/20/2018

Country of Publication:: United States

Language:: English

Subject:: 25 ENERGY STORAGE; 36 MATERIALS SCIENCE; 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY

Citation Formats


                    Armstrong, Beth L., Veith, Gabriel M., Kalnaus, Sergiy, Wang, Hsin, Browning, Katie L., and Cooley, Kevin M. Fabrication of films and coatings used to activate shear thickening, impact resistant electrolytes.  United States: N. p., 2020. 
        Web.

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                    Armstrong, Beth L., Veith, Gabriel M., Kalnaus, Sergiy, Wang, Hsin, Browning, Katie L., & Cooley, Kevin M. Fabrication of films and coatings used to activate shear thickening, impact resistant electrolytes.  United States.

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                    Armstrong, Beth L., Veith, Gabriel M., Kalnaus, Sergiy, Wang, Hsin, Browning, Katie L., and Cooley, Kevin M. Tue .  
        "Fabrication of films and coatings used to activate shear thickening, impact resistant electrolytes".  United States.  https://www.osti.gov/servlets/purl/1650837.

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@article{osti_1650837,

  title        = {Fabrication of films and coatings used to activate shear thickening, impact resistant electrolytes},

  author       = {Armstrong, Beth L. and Veith, Gabriel M. and Kalnaus, Sergiy and Wang, Hsin and Browning, Katie L. and Cooley, Kevin M.},

  abstractNote = {A method of making a passively impact resistant composite electrolyte and separator layer includes providing a suspension composition including electrically non-conducting particles that enable shear thickening. The particles can have a polydispersity index of no greater than 0.1, an average particle size in a range of from 50 nm to 1 um, and an absolute zeta potential of greater than ±40 mV. A particle suspension solvent is provided for suspending the particles. The suspension composition is applied to a porous separator material. A portion of the particles and suspension solvent penetrate the pores and the remainder of the particles in the suspension composition are distributed across the surface of the separator material. The suspension solvent is evaporated from the separator material to provide a shear thickening particle loaded separator. A separator assembly and a passivated battery are also disclosed.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Apr 28 00:00:00 EDT 2020},

  month        = {Tue Apr 28 00:00:00 EDT 2020}

}

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Title: Fabrication of films and coatings used to activate shear thickening, impact resistant electrolytes

Abstract

Citation Formats

Membranes f0r Electrochemical Cells patent-application, January 2016

Shear-thickening solutions with hydroxypropyl cellulose patent, March 1992

Method of making a laminated lithium-ion rechargeable battery cell patent, November 1995

Electrochemical Cell, Related Material, Process for Production and Use Thereof patent-application, July 2014

Electrolyte comprising non-ionic surfactant and lithium ion battery using the same patent, November 2005

Chemical Battery patent-application, October 2015

Shear Thickening Fluid Containment in Polymer Composites patent-application, October 2006

Micro-Porous Hybris Film Having Electro-Chemical Stability and Method for Preparing the Same patent-application, November 2015

Current collector for battery and battery using same patent-application, November 2015

Separator and Rechargeable Lithium Battery Including the Same patent-application, September 2014

Electrospinning for Integrated Separator for Lithium-Ion Batteries patent-application, December 2015

Integral bi-layer separator-electrode construction for lithium-ion batteries patent-application, February 2016

Lithium rechargeable battery including a porous membrane separator formed of ceramic secondary particles and a binder patent, February 2010

Polymer brushes patent, January 2013

Lubricant-impregnated surfaces for electrochemical applications, and devices and systems using same patent-application, December 2015

Advanced body armor utilizing shear thickening fluids patent, March 2009

Ceramic electrolyte coating methods patent, October 2004

Emulsification of Concentrated Dispersions of Colloidal and Nanoparticles patent-application, December 2007

Shear Activated Impact Resistant Electrolyte patent-application, April 2017

Lithium ion battery electrodes patent-application, August 2004

Radiation shield using electrical insulating materials and the spacecharge fields therein patent, November 2002

Integrated Composite Separator for Lithium-ion Batteries patent-application, September 2011

Lithium battery with surfactant Coated electrode patent-application, January 2007

Battery Separator patent, November 1942

Graphite-Carbon Composite Electrode for Supercapacitors patent-application, March 2009

Low electrolyte electrochemical cells patent-application, March 2012

Aqueous processing of composite lithium ion electrode material patent, February 2015

Separators for a Lithium Ion Battery patent-application, December 2012

Advanced body armor patent, November 2010

LITHIUM ION BATTERIES COMPRISING NANOFIBERS patent-application, April 2015

Prototyping graphical user interfaces patent, September 2009

Impact resistant electrolytes patent, March 2017

Non-Aqueous Liquid Electrolyte and Non-Aqueous Liquid Electrolyte Secondary Battery patent-application, September 2007

Ceramic electrolyte coating and methods patent, August 2007

Conformable Ballistic Resistant and Protective Composite Materials Composed of Shear Thickening Fluids Reinforced by Short Fibers patent-application, January 2009

Binder for batteries, and electrode compositions and batteries incorporating same patent, January 1998

Electrochemical Cells with Glass Containing Separators patent-application, December 2014

Multi-layered apparatus for stopping projectiles patent-application, August 2007

Electrolyte for high voltage lithium rechargeable battery and high voltage lithium rechargeable battery employing the same patent, February 2010

Electrode for All Solid-State Secondary Battery and Method for Producing Same patent-application, March 2015

Nonaqueous liquid electrolyte and nonaqueous liquid electrolyte secondary battery patent, March 2009

Separator for Non-Aqueous Electrolyte Secondary Battery and Non-Aqueous Electrolyte Secondary Battery patent-application, April 2015

Impact Resistant Electrolytes patent-application, March 2016

Electrolyte, lithium battery and lithium metal battery including the same, and method of preparing the electrolyte patent-application, January 2016

Shear-activated viscoelastic surfactant fluid and method patent, October 2013

Separator for Electrochemical Cell and Method for Its Manufacture patent-application, June 2009

Nonaqueous liquid electrolyte and nonaqueous liquid electrolyte secondary battery patent, June 2007

Electronic Component Separator and Method for Producing the Same patent-application, September 2005

Membranes f0r Electrochemical Cells
patent-application, January 2016

Shear-thickening solutions with hydroxypropyl cellulose
patent, March 1992

Method of making a laminated lithium-ion rechargeable battery cell
patent, November 1995

Electrochemical Cell, Related Material, Process for Production and Use Thereof
patent-application, July 2014

Electrolyte comprising non-ionic surfactant and lithium ion battery using the same
patent, November 2005

Chemical Battery
patent-application, October 2015

Shear Thickening Fluid Containment in Polymer Composites
patent-application, October 2006

Micro-Porous Hybris Film Having Electro-Chemical Stability and Method for Preparing the Same
patent-application, November 2015

Current collector for battery and battery using same
patent-application, November 2015

Separator and Rechargeable Lithium Battery Including the Same
patent-application, September 2014

Electrospinning for Integrated Separator for Lithium-Ion Batteries
patent-application, December 2015

Integral bi-layer separator-electrode construction for lithium-ion batteries
patent-application, February 2016

Lithium rechargeable battery including a porous membrane separator formed of ceramic secondary particles and a binder
patent, February 2010

Polymer brushes
patent, January 2013

Lubricant-impregnated surfaces for electrochemical applications, and devices and systems using same
patent-application, December 2015

Advanced body armor utilizing shear thickening fluids
patent, March 2009

Ceramic electrolyte coating methods
patent, October 2004

Emulsification of Concentrated Dispersions of Colloidal and Nanoparticles
patent-application, December 2007

Shear Activated Impact Resistant Electrolyte
patent-application, April 2017

Lithium ion battery electrodes
patent-application, August 2004

Radiation shield using electrical insulating materials and the spacecharge fields therein
patent, November 2002

Integrated Composite Separator for Lithium-ion Batteries
patent-application, September 2011

Lithium battery with surfactant Coated electrode
patent-application, January 2007

Battery Separator
patent, November 1942

Graphite-Carbon Composite Electrode for Supercapacitors
patent-application, March 2009

Low electrolyte electrochemical cells
patent-application, March 2012

Aqueous processing of composite lithium ion electrode material
patent, February 2015

Separators for a Lithium Ion Battery
patent-application, December 2012

Advanced body armor
patent, November 2010

LITHIUM ION BATTERIES COMPRISING NANOFIBERS
patent-application, April 2015

Prototyping graphical user interfaces
patent, September 2009

Impact resistant electrolytes
patent, March 2017

Non-Aqueous Liquid Electrolyte and Non-Aqueous Liquid Electrolyte Secondary Battery
patent-application, September 2007

Ceramic electrolyte coating and methods
patent, August 2007

Conformable Ballistic Resistant and Protective Composite Materials Composed of Shear Thickening Fluids Reinforced by Short Fibers
patent-application, January 2009

Binder for batteries, and electrode compositions and batteries incorporating same
patent, January 1998

Electrochemical Cells with Glass Containing Separators
patent-application, December 2014

Multi-layered apparatus for stopping projectiles
patent-application, August 2007

Electrolyte for high voltage lithium rechargeable battery and high voltage lithium rechargeable battery employing the same
patent, February 2010

Electrode for All Solid-State Secondary Battery and Method for Producing Same
patent-application, March 2015

Nonaqueous liquid electrolyte and nonaqueous liquid electrolyte secondary battery
patent, March 2009

Separator for Non-Aqueous Electrolyte Secondary Battery and Non-Aqueous Electrolyte Secondary Battery
patent-application, April 2015

Impact Resistant Electrolytes
patent-application, March 2016

Electrolyte, lithium battery and lithium metal battery including the same, and method of preparing the electrolyte
patent-application, January 2016

Shear-activated viscoelastic surfactant fluid and method
patent, October 2013

Separator for Electrochemical Cell and Method for Its Manufacture
patent-application, June 2009

Nonaqueous liquid electrolyte and nonaqueous liquid electrolyte secondary battery
patent, June 2007

Electronic Component Separator and Method for Producing the Same
patent-application, September 2005