Barrier film, method of making the barrier film, and articles including the barrier film

Spagnola, Joseph C.; Roehrig, Mark A.; Klun, Thomas P.; Nachtigal, Alan K.; Schnobrich, Jennifer K.; Joly, Guy D.

Title: Barrier film, method of making the barrier film, and articles including the barrier film

Abstract

A barrier film that includes a substrate, a first polymer layer on a major surface of the substrate, an oxide layer on the first polymer layer, and a second polymer layer on the oxide layer. At least one of the first or second polymer layers includes a siloxane reaction product of a secondary or tertiary amino-functional silane having at least two silane groups. A method of making the barrier film and articles and a barrier assembly including the barrier film are also disclosed.

Inventors:: Spagnola, Joseph C.; Roehrig, Mark A.; Klun, Thomas P.; Nachtigal, Alan K.; Schnobrich, Jennifer K.; Joly, Guy D.

Issue Date:: 2020-04-28

Research Org.:: 3M Innovative Properties Company

Sponsoring Org.:: USDOE

OSTI Identifier:: 1650831

Patent Number(s):: 10636920

Application Number:: 14/420,060

Assignee:: 3M Innovative Properties Company (St. Paul, MN)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B05 - SPRAYING OR ATOMISING IN GENERAL B05D - PROCESSES FOR APPLYING LIQUIDS OR OTHER FLUENT MATERIALS TO SURFACES, IN GENERAL

B - PERFORMING OPERATIONS B32 - LAYERED PRODUCTS B32B - LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM

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B - PERFORMING OPERATIONS B05 - SPRAYING OR ATOMISING IN GENERAL B05D - PROCESSES FOR APPLYING LIQUIDS OR OTHER FLUENT MATERIALS TO SURFACES, IN GENERAL
B05D1/60 - {Deposition of organic layers from vapour phase
B05D7/04 - to surfaces of films or sheets
B05D7/56 - {Three layers or more}

B - PERFORMING OPERATIONS B32 - LAYERED PRODUCTS B32B - LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
B32B2307/554 - Wear resistance
B32B2307/558 - Impact strength, toughness
B32B2307/584 - Scratch resistance
B32B2307/712 - Weather resistant
B32B2307/7244 - Oxygen barrier
B32B2307/7246 - Water vapor barrier
B32B2307/7248 - Odour barrier
B32B2457/00 - Electrical equipment
B32B2457/12 - Photovoltaic modules
B32B2457/20 - Displays, e.g. liquid crystal displays, plasma displays
B32B27/08 - of synthetic resin {
B32B27/281 - {comprising polyimides}
B32B27/283 - {comprising polysiloxanes}
B32B27/286 - {comprising polysulphones
B32B27/288 - {comprising polyketones}
B32B27/30 - comprising vinyl {
B32B27/308 - {comprising acrylic
B32B27/36 - comprising polyesters
B32B33/00 - Layered products characterised by particular properties or particular surface features, e.g. particular surface coatings
B32B7/12 - using interposed adhesives or interposed materials with bonding properties

C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08J - WORKING-UP
C08J2367/02 - Polyesters derived from dicarboxylic acids and dihydroxy compounds
C08J2433/14 - of esters containing halogen, nitrogen, sulfur, or oxygen atoms in addition to the carboxy oxygen
C08J2483/04 - Polysiloxanes
C08J7/0423 - {with at least one layer of inorganic material and at least one layer of a composition containing a polymer binder}
C08J7/043 - Improving the adhesiveness of the coatings per se, e.g. forming primers
C08J7/048 - Forming gas barrier coatings

C - CHEMISTRY C09 - DYES C09D - COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS
C09D183/04 - Polysiloxanes

G - PHYSICS G02 - OPTICS G02F - DEVICES OR ARRANGEMENTS, THE OPTICAL OPERATION OF WHICH IS MODIFIED BY CHANGING THE OPTICAL PROPERTIES OF THE MEDIUM OF THE DEVICES OR ARRANGEMENTS FOR THE CONTROL OF THE INTENSITY, COLOUR, PHASE, POLARISATION OR DIRECTION OF LIGHT, e.g. SWITCHING, GATING, MODULATING OR DEMODULATING
G02F1/133305 - {Flexible substrates, e.g. plastics, organic film}

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01L - SEMICONDUCTOR DEVICES
H01L31/02167 - {for solar cells}

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
Y10T428/3154 - Of fluorinated addition polymer from unsaturated monomers
Y10T428/31544 - Addition polymer is perhalogenated
Y10T428/31547 - Of polyisocyanurate
Y10T428/31663 - As siloxane, silicone or silane

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DOE Contract Number:: EE0004739

Resource Type:: Patent

Resource Relation:: Patent File Date: 08/08/2013

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY

Citation Formats


                    Spagnola, Joseph C., Roehrig, Mark A., Klun, Thomas P., Nachtigal, Alan K., Schnobrich, Jennifer K., and Joly, Guy D.. Barrier film, method of making the barrier film, and articles including the barrier film.  United States: N. p., 2020. 
        Web.

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                    Spagnola, Joseph C., Roehrig, Mark A., Klun, Thomas P., Nachtigal, Alan K., Schnobrich, Jennifer K., & Joly, Guy D.. Barrier film, method of making the barrier film, and articles including the barrier film.  United States.

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                    Spagnola, Joseph C., Roehrig, Mark A., Klun, Thomas P., Nachtigal, Alan K., Schnobrich, Jennifer K., and Joly, Guy D.. Tue .  
        "Barrier film, method of making the barrier film, and articles including the barrier film".  United States.  https://www.osti.gov/servlets/purl/1650831.

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@article{osti_1650831,

  title        = {Barrier film, method of making the barrier film, and articles including the barrier film},

  author       = {Spagnola, Joseph C. and Roehrig, Mark A. and Klun, Thomas P. and Nachtigal, Alan K. and Schnobrich, Jennifer K. and Joly, Guy D.},

  abstractNote = {A barrier film that includes a substrate, a first polymer layer on a major surface of the substrate, an oxide layer on the first polymer layer, and a second polymer layer on the oxide layer. At least one of the first or second polymer layers includes a siloxane reaction product of a secondary or tertiary amino-functional silane having at least two silane groups. A method of making the barrier film and articles and a barrier assembly including the barrier film are also disclosed.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2020},

  month        = {4}

}

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Title: Barrier film, method of making the barrier film, and articles including the barrier film

Abstract

Citation Formats

Solar Control Film patent, November 1973

Multilayer Surface Covering with Barrier Layer patent-application, May 2012

Miniaturized monolithic multi-layer capacitor and apparatus and method for making patent, May 1991

Flexible encapsulating film systems patent, September 2014

Acrylate coating material patent, August 1995

Flexible high-temperature ultrabarrier patent, March 2006

Photovoltaic module and method for producing same patent, April 2002

All-polymeric ultraviolet light reflecting film patent, July 1996

Diffusion barrier coatings having graded compositions and devices incorporating the same patent, March 2006

Acrylate composite barrier coating patent, May 2001

Moisture barrier coatings for organic light emitting diode devices patent-application, August 2008

Method of making a multi-layered article patent, July 1991

Barrier Assembly with Encapsulant and Photovoltaic Cell patent-application, January 2012

Ultrabarrier substrates patent, July 2002

High speed process for coating substrates patent, June 1989

Barrier film patent, January 2014

Weatherable multilayer articles and method for their preparation patent-application, December 2004

Method for producing photovoltaic thin film module patent-application, February 2003

High speed apparatus for forming capacitors patent, March 1992

Fast-Curing Modified Siloxane patent-application, March 2006

Moisture Resistant Coating for Barrier Films patent-application, January 2012

Method of forming a hybrid polymer film patent, April 2001

Semiconductor System with Surface Modification patent-application, December 2007

Organically-modified, radiation-curable siloxane resin and method of making the same patent, November 1998

Vapor-Deposited Coating for Barrier Films and Methods of Making and Using the Same patent-application, November 2013

Flash evaporation of monomer fluids patent, September 1990

Multilayer Laminates Comprising Twisted Nematic Liquid Crystals patent-application, July 2007

Method for forming a multicolor interference coating patent, January 2000

Silicone/multifunctional acrylate barrier coatings patent, February 2004

Silane Coating Compositions, Coating Systems, and Methods patent-application, June 2007

Dielectric ceramic composition and package made of the same composition for packaging semiconductor patent, August 1996

Vapor coating method patent, April 2000

Coated Substrates and Methods for Their Preparation patent-application, May 2009

Barrier Coatings for Polymeric Substrates patent-application, May 2011

Moisture barrier coatings patent-application, January 2007

O2 and H2O barrier material patent, July 2006

Multicolor interference coating patent, March 1999

Barrier Assembly patent-application, January 2012

Jet plasma process for deposition of coatings patent, February 2002

Monomer atomizer for vaporization patent, September 1987

Laminated Plastic Substrate, and a Production Method for the Same patent-application, November 2011

Atomizing device for vaporization patent, February 1988

Coatings for Barrier Films and Methods of Making and Using the Same patent-application, December 2013

Flexible Assembly And Method Of Making And Using The Same patent-application, September 2012

Low refractive index fluoropolymer coating compositions for use in antireflective polymer films patent, January 2008

Jet plasma process and apparatus patent, November 1995

Protected Organic Electronic Devices and Methods for Making the Same patent-application, February 2004

Barrier composite films and a method for producing the same patent, June 1998

Miniaturized monolithic multi-layer capacitor and apparatus and method for making same patent, June 1992

Moisture resistant coating for barrier films patent, February 2016

Composition for Producing a Barrier Layer for Gases patent-application, May 2007

Barrier Laminate and Gas Barrier Film Using the Same patent-application, March 2011

Azasilanes and Methods for Making and Using the Same patent-application, April 2004

Solar Control Film
patent, November 1973

Multilayer Surface Covering with Barrier Layer
patent-application, May 2012

Miniaturized monolithic multi-layer capacitor and apparatus and method for making
patent, May 1991

Flexible encapsulating film systems
patent, September 2014

Acrylate coating material
patent, August 1995

Flexible high-temperature ultrabarrier
patent, March 2006

Photovoltaic module and method for producing same
patent, April 2002

All-polymeric ultraviolet light reflecting film
patent, July 1996

Diffusion barrier coatings having graded compositions and devices incorporating the same
patent, March 2006

Acrylate composite barrier coating
patent, May 2001

Moisture barrier coatings for organic light emitting diode devices
patent-application, August 2008

Method of making a multi-layered article
patent, July 1991

Barrier Assembly with Encapsulant and Photovoltaic Cell
patent-application, January 2012

Ultrabarrier substrates
patent, July 2002

High speed process for coating substrates
patent, June 1989

Barrier film
patent, January 2014

Weatherable multilayer articles and method for their preparation
patent-application, December 2004

Method for producing photovoltaic thin film module
patent-application, February 2003

High speed apparatus for forming capacitors
patent, March 1992

Fast-Curing Modified Siloxane
patent-application, March 2006

Moisture Resistant Coating for Barrier Films
patent-application, January 2012

Method of forming a hybrid polymer film
patent, April 2001

Semiconductor System with Surface Modification
patent-application, December 2007

Organically-modified, radiation-curable siloxane resin and method of making the same
patent, November 1998

Vapor-Deposited Coating for Barrier Films and Methods of Making and Using the Same
patent-application, November 2013

Flash evaporation of monomer fluids
patent, September 1990

Multilayer Laminates Comprising Twisted Nematic Liquid Crystals
patent-application, July 2007

Method for forming a multicolor interference coating
patent, January 2000

Silicone/multifunctional acrylate barrier coatings
patent, February 2004

Silane Coating Compositions, Coating Systems, and Methods
patent-application, June 2007

Dielectric ceramic composition and package made of the same composition for packaging semiconductor
patent, August 1996

Vapor coating method
patent, April 2000

Coated Substrates and Methods for Their Preparation
patent-application, May 2009

Barrier Coatings for Polymeric Substrates
patent-application, May 2011

Moisture barrier coatings
patent-application, January 2007

O2 and H2O barrier material
patent, July 2006

Multicolor interference coating
patent, March 1999

Barrier Assembly
patent-application, January 2012

Jet plasma process for deposition of coatings
patent, February 2002

Monomer atomizer for vaporization
patent, September 1987

Laminated Plastic Substrate, and a Production Method for the Same
patent-application, November 2011

Atomizing device for vaporization
patent, February 1988

Coatings for Barrier Films and Methods of Making and Using the Same
patent-application, December 2013

Flexible Assembly And Method Of Making And Using The Same
patent-application, September 2012

Low refractive index fluoropolymer coating compositions for use in antireflective polymer films
patent, January 2008

Jet plasma process and apparatus
patent, November 1995

Protected Organic Electronic Devices and Methods for Making the Same
patent-application, February 2004

Barrier composite films and a method for producing the same
patent, June 1998

Miniaturized monolithic multi-layer capacitor and apparatus and method for making same
patent, June 1992

Moisture resistant coating for barrier films
patent, February 2016

Composition for Producing a Barrier Layer for Gases
patent-application, May 2007

Barrier Laminate and Gas Barrier Film Using the Same
patent-application, March 2011

Azasilanes and Methods for Making and Using the Same
patent-application, April 2004