Extreme synthesis of crystalline aerogel materials from amorphous aerogel precursors
Abstract
A method includes positioning a porous structure in a pressure cell; injecting an inert pressure medium within the pressure cell; and pressurizing the pressure cell to a pressure that thermodynamically favors a crystalline phase of the porous structure over an amorphous phase of the porous structure to transition the amorphous phase of the porous structure into the crystalline phase of the porous structure.
- Inventors:
- Issue Date:
- Research Org.:
- Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1600291
- Patent Number(s):
- 10479933
- Application Number:
- 15/595,706
- Assignee:
- Lawrence Livermore National Security, LLC (Livermore, CA)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- DOE Contract Number:
- AC52-07NA27344
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 05/15/2017
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS
Citation Formats
Pauzauskie, Peter J., Crowhurst, Jonathan C., Worsley, Marcus A., and Satcher, Jr., Joe H. Extreme synthesis of crystalline aerogel materials from amorphous aerogel precursors. United States: N. p., 2019.
Web.
Pauzauskie, Peter J., Crowhurst, Jonathan C., Worsley, Marcus A., & Satcher, Jr., Joe H. Extreme synthesis of crystalline aerogel materials from amorphous aerogel precursors. United States.
Pauzauskie, Peter J., Crowhurst, Jonathan C., Worsley, Marcus A., and Satcher, Jr., Joe H. Tue .
"Extreme synthesis of crystalline aerogel materials from amorphous aerogel precursors". United States. https://www.osti.gov/servlets/purl/1600291.
@article{osti_1600291,
title = {Extreme synthesis of crystalline aerogel materials from amorphous aerogel precursors},
author = {Pauzauskie, Peter J. and Crowhurst, Jonathan C. and Worsley, Marcus A. and Satcher, Jr., Joe H.},
abstractNote = {A method includes positioning a porous structure in a pressure cell; injecting an inert pressure medium within the pressure cell; and pressurizing the pressure cell to a pressure that thermodynamically favors a crystalline phase of the porous structure over an amorphous phase of the porous structure to transition the amorphous phase of the porous structure into the crystalline phase of the porous structure.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2019},
month = {11}
}
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