Low temperature electrolytes for solid oxide cells having high ionic conductivity

Budaragin, Leonid V.; Deininger, Mark A.; Pozvonkov, Michael M.; Spears, D. Morgan; Fisher, Paul D.; Pasto, Arvid E.

Title: Low temperature electrolytes for solid oxide cells having high ionic conductivity

Abstract

Methods for forming a metal oxide electrolyte improve ionic conductivity. Some of those methods involve applying a first metal compound to a substrate, converting that metal compound to a metal oxide, applying a different metal compound to the metal oxide, and converting the different metal compound to form a second metal oxide. Electrolytes so formed can be used in solid oxide fuel cells, electrolyzers, and sensors, among other applications.

Inventors:: Budaragin, Leonid V.; Deininger, Mark A.; Pozvonkov, Michael M.; Spears, II, D. Morgan; Fisher, Paul D.; Pasto, Arvid E.

Issue Date:: 2019-07-09

Research Org.:: FCET, Inc., Roswell, GA (United States); UT-Battelle LLC/ORNL, Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1568569

Patent Number(s):: 10344389

Application Number:: 15/597,126

Assignee:: FCET, Inc. (Roswell, GA); UT-Battelle, LLC (Oak Ridge, TN)

Patent Classifications (CPCs):: H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02P - CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS

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H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M8/1246 - the electrolyte consisting of oxides
H01M8/1253 - the electrolyte containing zirconium oxide
H01M2300/0077 - based on zirconium oxide
H01M8/1016 - characterised by the electrolyte material
H01M8/0271 - Sealing or supporting means around electrodes, matrices or membranes
H01M8/1007 - with both reactants being gaseous or vaporised

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02P - CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
Y02P70/50 - Manufacturing or production processes characterised by the final manufactured product

G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N27/4073 - {Composition or fabrication of the solid electrolyte}

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M2300/0091 - in the form of mixtures

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25B - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS
C25B13/04 - characterised by the material

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/50 - Fuel cells

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M2008/1293 - {Fuel cells with solid oxide electrolytes}
H01M8/004 - {Cylindrical, tubular or wound}

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01B - CABLES
H01B1/122 - {Ionic conductors}

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M2300/0071 - Oxides
H01M2300/0074 - Ion conductive at high temperature

G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N27/40 - Semi-permeable membranes or partitions

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M8/243 - Grouping of unit cells of tubular or cylindrical configuration
H01M8/1006 - Corrugated, curved or wave-shaped MEA
H01M8/126 - the electrolyte containing cerium oxide

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Resource Type:: Patent

Resource Relation:: Patent File Date: 05/16/2017

Country of Publication:: United States

Language:: English

Subject:: 30 DIRECT ENERGY CONVERSION; 36 MATERIALS SCIENCE

Citation Formats


                    Budaragin, Leonid V., Deininger, Mark A., Pozvonkov, Michael M., Spears, II, D. Morgan, Fisher, Paul D., and Pasto, Arvid E. Low temperature electrolytes for solid oxide cells having high ionic conductivity.  United States: N. p., 2019. 
        Web.

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                    Budaragin, Leonid V., Deininger, Mark A., Pozvonkov, Michael M., Spears, II, D. Morgan, Fisher, Paul D., & Pasto, Arvid E. Low temperature electrolytes for solid oxide cells having high ionic conductivity.  United States.

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                    Budaragin, Leonid V., Deininger, Mark A., Pozvonkov, Michael M., Spears, II, D. Morgan, Fisher, Paul D., and Pasto, Arvid E. Tue .  
        "Low temperature electrolytes for solid oxide cells having high ionic conductivity".  United States.  https://www.osti.gov/servlets/purl/1568569.

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@article{osti_1568569,

  title        = {Low temperature electrolytes for solid oxide cells having high ionic conductivity},

  author       = {Budaragin, Leonid V. and Deininger, Mark A. and Pozvonkov, Michael M. and Spears, II, D. Morgan and Fisher, Paul D. and Pasto, Arvid E.},

  abstractNote = {Methods for forming a metal oxide electrolyte improve ionic conductivity. Some of those methods involve applying a first metal compound to a substrate, converting that metal compound to a metal oxide, applying a different metal compound to the metal oxide, and converting the different metal compound to form a second metal oxide. Electrolytes so formed can be used in solid oxide fuel cells, electrolyzers, and sensors, among other applications.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2019},

  month        = {7}

}

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Title: Low temperature electrolytes for solid oxide cells having high ionic conductivity

Abstract

Citation Formats

Oxygen sensor and a process for production thereof patent, May 1996

Method of preparing ceramic composite powders and the powders obtained thereby patent, November 1991

Synthesis of layers, coatings or films using precursor layer exerted pressure containment patent, December 2002

Method and apparatus for fabrication of integrated circuit by selective deposition of precursor liquid patent, September 2002

Protective metal oxide films on metal or alloy substrate surfaces susceptible to coking, corrosion or catalytic activity patent, October 1981

Solid electrolyte type fuel cell and method for producing the same patent, August 1994

High temperature epoxy tooling composition of bifunctional epoxy, trifunctional epoxy, anhydride, imidazole and interstitially matched filler patent, May 1990

Metal organic precursors for transparent metal oxide thin films and method of making same patent, February 2004

Electrolyte for solid oxide fuel cells patent, May 2001

Solid electrolytic material and use thereof patent, July 1981

Electrolyte-cathode assembly for a fuel cell patent, February 1979

Dithiolate metal complex compound, production method of the same, and optical information recording medium comprising the same patent, July 1991

Oxide modified air electrode surface for high temperature electrochemical cells patent, April 1992

Solid oxide fuel cells with novel internal geometry patent, February 2006

Method of forming patterned oxide superconducting films patent, June 1991

Coatings for metal casting parts patent, May 2010

Catalyzed diesel exhaust particulate filter patent, March 1992

Thermal cracking process using tubes, pipes, and coils made of novel stainless steel matrix patent, January 2007

Gas sensor, in particular a lambda sensor patent, August 2006

Solid oxide fuel cells, electrolyzers, and sensors, and methods of making and using the same patent, January 2014

Structure and method for compaction of powder-like materials patent, November 1997

Process for making dense thin films patent, July 2005

Processing for forming corrosion and permeation barriers patent, May 1995

Radiation concentrator for a photovoltaic device patent, November 2002

Chemical derivatization of silica coated fullerenes and use of derivatized silica coated fullerenes patent, February 2009

NO.sub.x selective reduction catalyst with broadened active temperature range patent, October 1999

Photovoltaic devices and compositions for use therein patent, May 2003

Hydrogen sensor, hydrogen sensor device and method of detecting hydrogen concentration patent, June 2007

Self-recovering soot detector, particularly to monitor carbon content in diesel engine exhaust gases patent, December 1981

Method of production of a spark plug for internal combustion engines patent, October 1990

Spark plug for use in internal combustion engine patent, August 1989

Coated articles and method for the prevention of fuel thermal degradation deposits patent, September 1998

Composition and method for forming Ba.sub.1-X Sr.sub.x Ti.sub.y O.sub.3 thin films patent, July 1997

Fuel cell electrode comprising conductive zeolite support material patent, September 2000

Spark plug patent, October 1976

Process for derivatizing carbon nanotubes with diazonium species patent, July 2007

Preparation of nickel and chromium substrates for ceramic coating patent, June 1976

Environmentally tolerant anode catalyst for a solid oxide fuel cell patent, August 2007

Non-chromated oxide coating for aluminum substrates patent, September 1996

Method for reducing the internal resistance of rechargeable batteries patent, May 1999

Method for depositing fine-grained alumina coatings on cutting tools patent, October 2000

Method of protecting ceramic bodies against mechanical and thermal action patent, May 1989

Method and system for coating internal surfaces of prefabricated process piping in the field patent, November 2007

Apparatus for the catalytic purification of exhaust gases patent, March 1982

Multilayer nanolaminates containing polycrystalline zirconia patent, December 1995

Potable water supply components patent, July 1999

Electrochemical cell stack assembly patent-application, February 2004

Method for reduction of nitrogen oxides with ammonia using promoted zeolite catalysts patent, October 1990

Gas turbine cooling patent, January 1994

Spark plug for internal combustion engine patent, April 1992

Microwave regenerated diesel particular filter and method of making the same patent, December 2001

Antifoulants for thermal cracking processes patent, August 1987

Carbide nanostructures and methods for making same patent, January 2008

Method for detection of rare earth metal oxide inclusions in titanium and other non-magnetic or metal alloy castings patent, November 2001

Surface on a stainless steel matrix patent, November 2004

Oxygen sensor element patent, February 1998

High temperature epoxy adhesive films patent, September 2003

Spark plug patent, June 1976

Insulator on spark plug electrode coated with zirconium and vanadium oxides patent, May 1981

Method of producing battery and electrolytic cell electrodes patent, November 1982

Method for coating sparkplugs patent, September 1999

Ignition device with lowered ignition temperature patent, November 1990

Methods of making highly dispersed substantially uniform cerium and zirconium mixed-metal-oxide composite supports for exhaust conversion catalysts patent, March 2000

Method for smoothing the surface of a protective coating patent, September 2001

Synthesis of layers, coatings or films using electrostatic fields patent, July 2003

Stabilized zirconia solid electrolyte and process for preparation thereof patent, July 1992

Preparation of an alkaline iron electrode material using sulfur acids patent, March 1976

Process for introducing a functionality patent, July 2002

Composite surface on a stainless steel matrix patent, May 2005

Metal coated phyllosilicate and method patent, September 1988

Antifoulants comprising tin antimony and aluminum for thermal cracking processes patent, August 1987

Reactor for extended duration growth of gallium containing single crystals patent, October 2007

Thermal barrier coating with improved strength and fracture toughness patent, December 2003

Composite ceramic articles and method for making such articles patent, October 1998

Low temperature solid oxide cells patent, February 2018

Four-way diesel exhaust catalyst and method of use patent, July 2000

Catalyzed SCR filter and emission treatment system patent, June 2007

Oxygen sensor and a process for production thereof
patent, May 1996

Method of preparing ceramic composite powders and the powders obtained thereby
patent, November 1991

Synthesis of layers, coatings or films using precursor layer exerted pressure containment
patent, December 2002

Method and apparatus for fabrication of integrated circuit by selective deposition of precursor liquid
patent, September 2002

Protective metal oxide films on metal or alloy substrate surfaces susceptible to coking, corrosion or catalytic activity
patent, October 1981

Solid electrolyte type fuel cell and method for producing the same
patent, August 1994

High temperature epoxy tooling composition of bifunctional epoxy, trifunctional epoxy, anhydride, imidazole and interstitially matched filler
patent, May 1990

Metal organic precursors for transparent metal oxide thin films and method of making same
patent, February 2004

Electrolyte for solid oxide fuel cells
patent, May 2001

Solid electrolytic material and use thereof
patent, July 1981

Electrolyte-cathode assembly for a fuel cell
patent, February 1979

Dithiolate metal complex compound, production method of the same, and optical information recording medium comprising the same
patent, July 1991

Oxide modified air electrode surface for high temperature electrochemical cells
patent, April 1992

Solid oxide fuel cells with novel internal geometry
patent, February 2006

Method of forming patterned oxide superconducting films
patent, June 1991

Coatings for metal casting parts
patent, May 2010

Catalyzed diesel exhaust particulate filter
patent, March 1992

Thermal cracking process using tubes, pipes, and coils made of novel stainless steel matrix
patent, January 2007

Gas sensor, in particular a lambda sensor
patent, August 2006

Solid oxide fuel cells, electrolyzers, and sensors, and methods of making and using the same
patent, January 2014

Structure and method for compaction of powder-like materials
patent, November 1997

Process for making dense thin films
patent, July 2005

Processing for forming corrosion and permeation barriers
patent, May 1995

Radiation concentrator for a photovoltaic device
patent, November 2002

Chemical derivatization of silica coated fullerenes and use of derivatized silica coated fullerenes
patent, February 2009

NO.sub.x selective reduction catalyst with broadened active temperature range
patent, October 1999

Photovoltaic devices and compositions for use therein
patent, May 2003

Hydrogen sensor, hydrogen sensor device and method of detecting hydrogen concentration
patent, June 2007

Self-recovering soot detector, particularly to monitor carbon content in diesel engine exhaust gases
patent, December 1981

Method of production of a spark plug for internal combustion engines
patent, October 1990

Spark plug for use in internal combustion engine
patent, August 1989

Coated articles and method for the prevention of fuel thermal degradation deposits
patent, September 1998

Composition and method for forming Ba.sub.1-X Sr.sub.x Ti.sub.y O.sub.3 thin films
patent, July 1997

Fuel cell electrode comprising conductive zeolite support material
patent, September 2000

Spark plug
patent, October 1976

Process for derivatizing carbon nanotubes with diazonium species
patent, July 2007

Preparation of nickel and chromium substrates for ceramic coating
patent, June 1976

Environmentally tolerant anode catalyst for a solid oxide fuel cell
patent, August 2007

Non-chromated oxide coating for aluminum substrates
patent, September 1996

Method for reducing the internal resistance of rechargeable batteries
patent, May 1999

Method for depositing fine-grained alumina coatings on cutting tools
patent, October 2000

Method of protecting ceramic bodies against mechanical and thermal action
patent, May 1989

Method and system for coating internal surfaces of prefabricated process piping in the field
patent, November 2007

Apparatus for the catalytic purification of exhaust gases
patent, March 1982

Multilayer nanolaminates containing polycrystalline zirconia
patent, December 1995

Potable water supply components
patent, July 1999

Electrochemical cell stack assembly
patent-application, February 2004

Method for reduction of nitrogen oxides with ammonia using promoted zeolite catalysts
patent, October 1990

Gas turbine cooling
patent, January 1994

Spark plug for internal combustion engine
patent, April 1992

Microwave regenerated diesel particular filter and method of making the same
patent, December 2001

Antifoulants for thermal cracking processes
patent, August 1987

Carbide nanostructures and methods for making same
patent, January 2008

Method for detection of rare earth metal oxide inclusions in titanium and other non-magnetic or metal alloy castings
patent, November 2001

Surface on a stainless steel matrix
patent, November 2004

Oxygen sensor element
patent, February 1998

High temperature epoxy adhesive films
patent, September 2003

Spark plug
patent, June 1976

Insulator on spark plug electrode coated with zirconium and vanadium oxides
patent, May 1981

Method of producing battery and electrolytic cell electrodes
patent, November 1982

Method for coating sparkplugs
patent, September 1999

Ignition device with lowered ignition temperature
patent, November 1990

Methods of making highly dispersed substantially uniform cerium and zirconium mixed-metal-oxide composite supports for exhaust conversion catalysts
patent, March 2000

Method for smoothing the surface of a protective coating
patent, September 2001

Synthesis of layers, coatings or films using electrostatic fields
patent, July 2003

Stabilized zirconia solid electrolyte and process for preparation thereof
patent, July 1992

Preparation of an alkaline iron electrode material using sulfur acids
patent, March 1976

Process for introducing a functionality
patent, July 2002

Composite surface on a stainless steel matrix
patent, May 2005

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patent, September 1988

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patent, August 1987

Reactor for extended duration growth of gallium containing single crystals
patent, October 2007

Thermal barrier coating with improved strength and fracture toughness
patent, December 2003

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patent, October 1998

Low temperature solid oxide cells
patent, February 2018

Four-way diesel exhaust catalyst and method of use
patent, July 2000

Catalyzed SCR filter and emission treatment system
patent, June 2007

Manufacturing method and device for electret processed product
patent, November 2005

Acid catalyzed combustion
patent, July 1985

Apparatus and method of production of thin film photovoltaic modules
patent, September 2007