Method for producing nanoparticles and the nanoparticles produced therefrom

Manuel, Michele Viola; Henderson, Hunter B.; Rios, Orlando; Ludtka, Gerard M.

Title: Method for producing nanoparticles and the nanoparticles produced therefrom

Abstract

Disclosed herein is a method comprising disposing a container containing a metal and/or ferromagnetic solid and abrasive particles in a static magnetic field; where the container is surrounded by an induction coil; activating the induction coil with an electrical current, to heat up the metallic or ferromagnetic solid to form a fluid; generating sonic energy to produce acoustic cavitation and abrasion between the abrasive particles and the container; and producing nanoparticles that comprise elements from the container, the metal and/or the ferromagnetic solid and the abrasive particles. Disclosed herein too is a composition comprising first metal or a first ceramic; and particles comprising carbides and/or nitrides dispersed therein. Disclosed herein too is a composition comprising nanoparticles comprising chromium carbide, iron carbide, nickel carbide, y.-Fe and magnesium nitride.

Inventors:: Manuel, Michele Viola; Henderson, Hunter B.; Rios, Orlando; Ludtka, Gerard M.

Issue Date:: 2019-07-09

Research Org.:: National Energy Technology Laboratory (NETL), Pittsburgh, PA, Morgantown, WV, and Albany, OR (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1568564

Patent Number(s):: 10343219

Application Number:: 15/123,172

Assignee:: University of Florida Research Foundation, Inc. (Gainesville, FL); UT-Battelle, LLC (Oak Ridge, TN)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25D - PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS

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B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER
B22F2302/20 - Nitride

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25D - PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS
C25D1/00 - Electroforming

B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER
B22F2302/10 - Carbide
B22F9/06 - starting from liquid material
B22F1/00 - Special treatment of metallic powder, e.g. to facilitate working, to improve properties {

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01F - MAGNETS
H01F1/442 - {the magnetic component being a metal or alloy, e.g. Fe

B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER
B22F2202/05 - Use of magnetic field
B22F9/04 - starting from solid material, e.g. by crushing, grinding or milling
B22F1/0044 - {Nanometer size structures}
B22F2009/045 - {by other means than ball or jet milling}

C - CHEMISTRY C22 - METALLURGY C22C - ALLOYS
C22C1/1084 - {by mechanical alloying

B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER
B22F2202/07 - by induction
B22F2009/042 - {using a particular milling fluid}
B22F2998/10 - Processes characterised by the sequence of their steps
B22F2301/058 - Magnesium

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25D - PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS
C25D15/00 - Electrolytic or electrophoretic production of coatings containing embedded materials, e.g. particles, whiskers, wires

B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER
B22F2999/00 - Aspects linked to processes or compositions used in powder metallurgy

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01F - MAGNETS
H01F1/0036 - {showing low dimensional magnetism, i.e. spin rearrangements due to a restriction of dimensions, e.g. showing giant magnetoresistivity,

B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER
B22F1/0018 - {Nanometer sized particles}

H - ELECTRICITY H05 - ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR H05B - ELECTRIC HEATING
H05B6/367 - {for melting furnaces}

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01F - MAGNETS
H01F1/047 - Alloys characterised by their composition

B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER
B22F2202/01 - Use of vibrations

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DOE Contract Number:: AC05-00OR22725; DMR0845868

Resource Type:: Patent

Resource Relation:: Patent File Date: 03/04/2015

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; 77 NANOSCIENCE AND NANOTECHNOLOGY

Citation Formats


                    Manuel, Michele Viola, Henderson, Hunter B., Rios, Orlando, and Ludtka, Gerard M. Method for producing nanoparticles and the nanoparticles produced therefrom.  United States: N. p., 2019. 
        Web.

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                    Manuel, Michele Viola, Henderson, Hunter B., Rios, Orlando, & Ludtka, Gerard M. Method for producing nanoparticles and the nanoparticles produced therefrom.  United States.

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                    Manuel, Michele Viola, Henderson, Hunter B., Rios, Orlando, and Ludtka, Gerard M. Tue .  
        "Method for producing nanoparticles and the nanoparticles produced therefrom".  United States.  https://www.osti.gov/servlets/purl/1568564.

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@article{osti_1568564,

  title        = {Method for producing nanoparticles and the nanoparticles produced therefrom},

  author       = {Manuel, Michele Viola and Henderson, Hunter B. and Rios, Orlando and Ludtka, Gerard M.},

  abstractNote = {Disclosed herein is a method comprising disposing a container containing a metal and/or ferromagnetic solid and abrasive particles in a static magnetic field; where the container is surrounded by an induction coil; activating the induction coil with an electrical current, to heat up the metallic or ferromagnetic solid to form a fluid; generating sonic energy to produce acoustic cavitation and abrasion between the abrasive particles and the container; and producing nanoparticles that comprise elements from the container, the metal and/or the ferromagnetic solid and the abrasive particles. Disclosed herein too is a composition comprising first metal or a first ceramic; and particles comprising carbides and/or nitrides dispersed therein. Disclosed herein too is a composition comprising nanoparticles comprising chromium carbide, iron carbide, nickel carbide, y.-Fe and magnesium nitride.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2019},

  month        = {7}

}

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Works referenced in this record:

Process for forming metal-ceramic composites
patent, December 1987

Brupbacher, John M.; Christodoulou, Leontios; Nagle, Dennis C.
US Patent Document 4,710,348
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Semi-solid forming of metal-matrix nanocomposites
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Turng, Lih-Sheng; De Cicco, Michael Peter; Li, Xiaochun
US Patent Document 7,509,993
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Johnson, D. Lynn; Dravid, Vinayak P.; Teng, Mao-Hua
US Patent Document 5,665,277
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Composite materials having a matrix of magnesium or magnesium alloy reinforced with discontinuous silicon carbide particles
patent, April 1987

Wada, Tsuguyasu; Eldis, George T.; Albright, Darryl L.
US Patent Document 4,657,065
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Preparation of composites
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US Patent Document 4,749,545
URL: http://patft.uspto.gov/netacgi/nph-Parser?patentnumber=4749545

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Title: Method for producing nanoparticles and the nanoparticles produced therefrom

Abstract

Citation Formats

Process for forming metal-ceramic composites patent, December 1987

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Nanoparticle synthesis apparatus and method patent, September 1997

Composite materials having a matrix of magnesium or magnesium alloy reinforced with discontinuous silicon carbide particles patent, April 1987

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patent, December 1987

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patent, September 1997

Composite materials having a matrix of magnesium or magnesium alloy reinforced with discontinuous silicon carbide particles
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