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Title: Mechanochemical synthesis of alane

Abstract

In some examples, a method of forming alane (AlH3), the method comprising reacting one of: 1) a MAlH4, wherein M is an alkali metal; 2) alkali-metal hydride, MH; or 3) alkali-metal with one or more aluminum halides (AlX3, where X is a halogen), via a mechanochemical process, to form the alane, wherein the reaction is substantially solvent free and carried out in an environment with a temperature between approximately 250 K and approximately 330 K.

Inventors:
; ; ; ;
Issue Date:
Research Org.:
Ames Laboratory (AMES), Ames, IA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1568256
Patent Number(s):
10,273,156
Application Number:
15/118,788
Assignee:
Iowa State University Research Foundation, Inc. (Ames, IA)
DOE Contract Number:  
AC02-07CH11358
Resource Type:
Patent
Resource Relation:
Patent File Date: 02/12/2015
Country of Publication:
United States
Language:
English
Subject:
08 HYDROGEN; 36 MATERIALS SCIENCE

Citation Formats

Gupta, Shalabh, Pecharsky, Vitalij K., Kobayashi, Takeshi, Pruski, Marek, and Hlova, Ihor. Mechanochemical synthesis of alane. United States: N. p., 2019. Web.
Gupta, Shalabh, Pecharsky, Vitalij K., Kobayashi, Takeshi, Pruski, Marek, & Hlova, Ihor. Mechanochemical synthesis of alane. United States.
Gupta, Shalabh, Pecharsky, Vitalij K., Kobayashi, Takeshi, Pruski, Marek, and Hlova, Ihor. Tue . "Mechanochemical synthesis of alane". United States. https://www.osti.gov/servlets/purl/1568256.
@article{osti_1568256,
title = {Mechanochemical synthesis of alane},
author = {Gupta, Shalabh and Pecharsky, Vitalij K. and Kobayashi, Takeshi and Pruski, Marek and Hlova, Ihor},
abstractNote = {In some examples, a method of forming alane (AlH3), the method comprising reacting one of: 1) a MAlH4, wherein M is an alkali metal; 2) alkali-metal hydride, MH; or 3) alkali-metal with one or more aluminum halides (AlX3, where X is a halogen), via a mechanochemical process, to form the alane, wherein the reaction is substantially solvent free and carried out in an environment with a temperature between approximately 250 K and approximately 330 K.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2019},
month = {4}
}

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