Stable catalyst layers for hydrogen permeable composite membranes

Way, J. Douglas; Wolden, Colin A.

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Title: Stable catalyst layers for hydrogen permeable composite membranes

Abstract

The present invention provides a hydrogen separation membrane based on nanoporous, composite metal carbide or metal sulfide coated membranes capable of high flux and permselectivity for hydrogen without platinum group metals. The present invention is capable of being operated over a broad temperature range, including at elevated temperatures, while maintaining hydrogen selectivity.

Inventors:: Way, J. Douglas; Wolden, Colin A.

Issue Date:: 2014-01-07

Research Org.:: Colorado School of Mines, Golden, CO (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1531891

Patent Number(s):: 8623121

Application Number:: 13/069,050

Assignee:: Colorado School of Mines (Golden, CO)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

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B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D2325/10 - Catalysts being present on the surface of the membrane or in the pores
B01D65/102 - {Detection of leaks in membranes}
B01D65/108 - {Repairing membranes}
B01D67/0072 - {by deposition from the gaseous phase, e.g. sputtering, CVD, PVD}
B01D69/10 - Supported membranes
B01D71/02 - Inorganic material
B01D71/022 - {Metals}

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B2203/0405 - Purification by membrane separation
C01B3/503 - {characterised by the membrane}

C - CHEMISTRY C23 - COATING METALLIC MATERIAL C23C - COATING METALLIC MATERIAL
C23C14/0635 - {Carbides}

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DOE Contract Number:: FE0001009

Resource Type:: Patent

Resource Relation:: Patent File Date: 2011-03-22

Country of Publication:: United States

Language:: English

Citation Formats


                    Way, J. Douglas, and Wolden, Colin A. Stable catalyst layers for hydrogen permeable composite membranes.  United States: N. p., 2014. 
        Web.

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                    Way, J. Douglas, & Wolden, Colin A. Stable catalyst layers for hydrogen permeable composite membranes.  United States.

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                    Way, J. Douglas, and Wolden, Colin A. Tue .  
        "Stable catalyst layers for hydrogen permeable composite membranes".  United States.  https://www.osti.gov/servlets/purl/1531891.

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@article{osti_1531891,

  title        = {Stable catalyst layers for hydrogen permeable composite membranes},

  author       = {Way, J. Douglas and Wolden, Colin A.},

  abstractNote = {The present invention provides a hydrogen separation membrane based on nanoporous, composite metal carbide or metal sulfide coated membranes capable of high flux and permselectivity for hydrogen without platinum group metals. The present invention is capable of being operated over a broad temperature range, including at elevated temperatures, while maintaining hydrogen selectivity.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2014},

  month        = {1}

}

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Works referenced in this record:

Membrane for hydrogen recovery from streams containing hydrogen sulfide
patent, January 2007

Agarwal, Pradeep
US Patent Document 7,163,670
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7163670

Composite hydrogen separation metal membrane
patent, February 1995

Edlund, David J.
US Patent Document 5,393,325
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5393325

Molybdenum carbide catalysts for water–gas shift
journal, April 2000

Patt, Jeremy; Moon, Dong Ju; Phillips, Cory
Catalysis Letters, Vol. 65, Issue 4, p. 193-195
https://doi.org/10.1023/A:1019098112056

Porous membrane for use in reaction process
patent, September 1989

Abe, Fumio
US Patent Document 4,865,630
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Gas Separation Membrane System and Method of Making Thereof Using Nanoscale Metal Material
patent-application, July 2003

Saukaitis, John Charles; Del Paggio, Alan Anthony
US Patent Application 11/932223; 20080174040
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20080174040

Hydrogen Separation Using Dense Composite Membranes: Part 1 Fundamentals
book, January 2009

Mundschau, Michael V.
Inorganic Membranes for Energy and Environmental Applications
https://doi.org/10.1007/978-0-387-34526-0_8

Improvement in high temperature stability of Pd coating on Nb by Nb2C intermediate layer
journal, April 2007

Hatano, Yuji; Ishiyama, Keita; Homma, Hirofumi
International Journal of Hydrogen Energy, Vol. 32, Issue 5
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Molybdenum carbide catalysts I. Synthesis of unsupported powders
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Lee, J.
Journal of Catalysis, Vol. 106, Issue 1
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Preparation and catalytic properties of transition metal carbides and nitrides
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Oyama, S. T.
Catalysis Today, Vol. 15, Issue 2
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Synthetic approaches to the molybdenum sulfide materials
journal, January 2008

Afanasiev, Pavel
Comptes Rendus Chimie, Vol. 11, Issue 1-2
https://doi.org/10.1016/j.crci.2007.04.009

Composition and operation of hydrogen-selective amorphous alloy membranes
journal, November 2006

Dolan, M. D.; Dave, N. C.; Ilyushechkin, A. Y.
Journal of Membrane Science, Vol. 285, Issue 1-2, p. 30-55
https://doi.org/10.1016/j.memsci.2006.09.014

Composite metal membrane
patent, April 1998

Peachey, Nathaniel; Dye, Robert C.; Snow, Ronny C.
US Patent Document 5,738,708
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5738708

Composite metal membrane for hydrogen extraction
patent, June 1993

Buxbaum, Robert E.
US Patent Document 5,215,729
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5215729

V–Ni alloy membranes for hydrogen purification
journal, January 2002

Nishimura, C.; Komaki, M.; Hwang, S.
Journal of Alloys and Compounds, Vol. 330-332
https://doi.org/10.1016/S0925-8388(01)01648-6

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Similar Records

Title: Stable catalyst layers for hydrogen permeable composite membranes

Abstract

Citation Formats

Membrane for hydrogen recovery from streams containing hydrogen sulfide patent, January 2007

Composite hydrogen separation metal membrane patent, February 1995

Molybdenum carbide catalysts for water–gas shift journal, April 2000

Porous membrane for use in reaction process patent, September 1989

Gas Separation Membrane System and Method of Making Thereof Using Nanoscale Metal Material patent-application, July 2003

Hydrogen Separation Using Dense Composite Membranes: Part 1 Fundamentals book, January 2009

Improvement in high temperature stability of Pd coating on Nb by Nb2C intermediate layer journal, April 2007

Molybdenum carbide catalysts I. Synthesis of unsupported powders journal, July 1987

Preparation and catalytic properties of transition metal carbides and nitrides journal, June 1992

Synthetic approaches to the molybdenum sulfide materials journal, January 2008

Composition and operation of hydrogen-selective amorphous alloy membranes journal, November 2006

Composite metal membrane patent, April 1998

Composite metal membrane for hydrogen extraction patent, June 1993

V–Ni alloy membranes for hydrogen purification journal, January 2002

Membrane for hydrogen recovery from streams containing hydrogen sulfide
patent, January 2007

Composite hydrogen separation metal membrane
patent, February 1995

Molybdenum carbide catalysts for water–gas shift
journal, April 2000

Porous membrane for use in reaction process
patent, September 1989

Gas Separation Membrane System and Method of Making Thereof Using Nanoscale Metal Material
patent-application, July 2003

Hydrogen Separation Using Dense Composite Membranes: Part 1 Fundamentals
book, January 2009

Improvement in high temperature stability of Pd coating on Nb by Nb2C intermediate layer
journal, April 2007

Molybdenum carbide catalysts I. Synthesis of unsupported powders
journal, July 1987

Preparation and catalytic properties of transition metal carbides and nitrides
journal, June 1992

Synthetic approaches to the molybdenum sulfide materials
journal, January 2008

Composition and operation of hydrogen-selective amorphous alloy membranes
journal, November 2006

Composite metal membrane
patent, April 1998

Composite metal membrane for hydrogen extraction
patent, June 1993

V–Ni alloy membranes for hydrogen purification
journal, January 2002