Rotational exchange gradient imager for in situ magnetic resonance analyses in ultracentrifuge sedimentation of biological materials and rheology investigations

Gerald, Rex E.; Klingler, Robert J.; Rathke, Jerome W.

Title: Rotational exchange gradient imager for in situ magnetic resonance analyses in ultracentrifuge sedimentation of biological materials and rheology investigations

Abstract

A detecting method and detector expands the capabilities of Nuclear Magnetic Resonance (NMR) analysis. A Rotational Exchange Gradient Imager (REGI) allows for real-time, in situ investigation of materials subjected to the effects of centrifugal force by NMR analysis. The REGI comprises a cylindrical stator formed of an electrically conductive, non-magnetic material, a rotor contained in the cylindrical stator formed of an electrically non-conductive, non-magnetic material, and a conductor located along a central axis of the cylindrical stator. A sample is contained within the rotor. The stator and central conductor serve to generate the RF magnetic field for NMR analysis. The rotor containing the sample is rotated within a stable air bearing formed between the cylindrical stator and rotor.

Inventors:: Gerald, II, Rex E.; Klingler, Robert J.; Rathke, Jerome W.

Issue Date:: 2004-04-13

Research Org.:: The Univ. of Chicago, Chicago, IL (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1531474

Patent Number(s):: 6720769

Application Number:: 10/177,189

Assignee:: The University of Chicago (Chicago, IL)

Patent Classifications (CPCs):: G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES

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G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES
G01R33/48 - NMR imaging systems
G01R33/307 - {specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer}

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DOE Contract Number:: W-31-109-ENG-38

Resource Type:: Patent

Resource Relation:: Patent File Date: 2002-06-21

Country of Publication:: United States

Language:: English

Citation Formats


                    Gerald, II, Rex E., Klingler, Robert J., and Rathke, Jerome W. Rotational exchange gradient imager for in situ magnetic resonance analyses in ultracentrifuge sedimentation of biological materials and rheology investigations.  United States: N. p., 2004. 
        Web.

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                    Gerald, II, Rex E., Klingler, Robert J., & Rathke, Jerome W. Rotational exchange gradient imager for in situ magnetic resonance analyses in ultracentrifuge sedimentation of biological materials and rheology investigations.  United States.

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                    Gerald, II, Rex E., Klingler, Robert J., and Rathke, Jerome W. Tue .  
        "Rotational exchange gradient imager for in situ magnetic resonance analyses in ultracentrifuge sedimentation of biological materials and rheology investigations".  United States.  https://www.osti.gov/servlets/purl/1531474.

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@article{osti_1531474,

  title        = {Rotational exchange gradient imager for in situ magnetic resonance analyses in ultracentrifuge sedimentation of biological materials and rheology investigations},

  author       = {Gerald, II, Rex E. and Klingler, Robert J. and Rathke, Jerome W.},

  abstractNote = {A detecting method and detector expands the capabilities of Nuclear Magnetic Resonance (NMR) analysis. A Rotational Exchange Gradient Imager (REGI) allows for real-time, in situ investigation of materials subjected to the effects of centrifugal force by NMR analysis. The REGI comprises a cylindrical stator formed of an electrically conductive, non-magnetic material, a rotor contained in the cylindrical stator formed of an electrically non-conductive, non-magnetic material, and a conductor located along a central axis of the cylindrical stator. A sample is contained within the rotor. The stator and central conductor serve to generate the RF magnetic field for NMR analysis. The rotor containing the sample is rotated within a stable air bearing formed between the cylindrical stator and rotor.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2004},

  month        = {4}

}

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Works referencing / citing this record:

Capillary toroid cavity detector for high pressure NMR
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Gerald, II, Rex E.; Chen, Michael J.; Klingler, Robert J.
US Patent Document 7,268,552
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patent, June 2010

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Similar Records

Title: Rotational exchange gradient imager for in situ magnetic resonance analyses in ultracentrifuge sedimentation of biological materials and rheology investigations

Abstract

Citation Formats

Use of audio signals for monitoring sample spinning speeds in nuclear magnetic spectrometers patent, July 1997

Method and apparatus for precisely controlling the periodic motion of an object patent, May 1998

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Angular Flow in Toroid Cavity Probes journal, August 2001

NMR probe head with integrated remote tuning patent, March 2001

Turbine having a rotor forming a nutation and precession movement patent, October 1992

Magnetic resonance spectroscopy apparatus patent, August 1989

High speed spinner for NMR spectrometer patent, April 1988

Two dimensional B1-gradient NMR imager patent, March 2003

Use of audio signals for monitoring and remediating spinning irregularides in NMR spectrometers patent, March 1998

Nuclear magnetic resonance detector used for reducing probe ringing patent, February 2001

Near-electrode imager patent, April 2000

Capillary toroid cavity detector for high pressure NMR patent, September 2007

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Use of audio signals for monitoring sample spinning speeds in nuclear magnetic spectrometers
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Turbine having a rotor forming a nutation and precession movement
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High speed spinner for NMR spectrometer
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Two dimensional B1-gradient NMR imager
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Use of audio signals for monitoring and remediating spinning irregularides in NMR spectrometers
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