Microsampler and method of making the same

Moorman, Matthew W.; Manginell, Ronald P.; Rejent, Jerome A.

Title: Microsampler and method of making the same

Abstract

An aspect of the present disclosure relates to a microsampler for hermetically sealing a sample. In particular, such microsamplers can be useful for encapsulation of chemical, biological, and explosive samples for the purposes of archival sample storage. Methods of making and using such microsamplers are also described herein.

Inventors:: Moorman, Matthew W.; Manginell, Ronald P.; Rejent, Jerome A.

Issue Date:: 2018-12-25

Research Org.:: Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1531388

Patent Number(s):: 10161835

Application Number:: 14/945,274

Assignee:: National Technology & Engineering Solutions of Sandia, LLC (Albuquerque, NM)

Patent Classifications (CPCs):: G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES

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G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N1/24 - Suction devices {
G01N2001/2285 - {Details of probe structures}
G01N2001/2282 - {with cooling means}
G01N1/2273 - {Atmospheric sampling}
G01N1/14 - Suction devices, e.g. pumps

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DOE Contract Number:: AC04-94AL85000

Resource Type:: Patent

Resource Relation:: Patent File Date: 2015-11-18

Country of Publication:: United States

Language:: English

Subject:: 47 OTHER INSTRUMENTATION; 42 ENGINEERING

Citation Formats


                    Moorman, Matthew W., Manginell, Ronald P., and Rejent, Jerome A. Microsampler and method of making the same.  United States: N. p., 2018. 
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                    Moorman, Matthew W., Manginell, Ronald P., & Rejent, Jerome A. Microsampler and method of making the same.  United States.

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                    Moorman, Matthew W., Manginell, Ronald P., and Rejent, Jerome A. Tue .  
        "Microsampler and method of making the same".  United States.  https://www.osti.gov/servlets/purl/1531388.

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@article{osti_1531388,

  title        = {Microsampler and method of making the same},

  author       = {Moorman, Matthew W. and Manginell, Ronald P. and Rejent, Jerome A.},

  abstractNote = {An aspect of the present disclosure relates to a microsampler for hermetically sealing a sample. In particular, such microsamplers can be useful for encapsulation of chemical, biological, and explosive samples for the purposes of archival sample storage. Methods of making and using such microsamplers are also described herein.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2018},

  month        = {12}

}

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Method for localized deposition of noble metal catalysts with control of morphology
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Ricco, Antonio J.; Manginell, Ronald P.; Huber, Robert J.
US Patent Document 5,820,922
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Testing capillary gas chromatographic columns
journal, November 1981

Grob, K.; Grob, G.; Grob, K.
Journal of Chromatography A, Vol. 219, Issue 1
https://doi.org/10.1016/S0021-9673(00)80568-3

Stability of methylnicotinate in aqueous solution as utilized in the 'niacin patch test'
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URL: http://patft.uspto.gov/netacgi/nph-Parser?patentnumber=7118712

Electrically conductive compositions and methods for the preparation and use thereof
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Capote, Miguel A.; Todd, Michael George; Manesis, Nicholas J.
US Patent Document 5,830,389
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Microstructure Evolution of Tin–Lead Solder
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Ubachs, R. L. J. M.; Schreurs, P. J. G.; Geers, M. G. D.
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Shul, Randy J.; Willison, Christi Gober; Schubert, W. Kent
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A Global Profiling System for Improved Weather and Climate Prediction
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Zhu, Jiangjiang; Bean, Heather D.; Kuo, Yin-Ming
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Flux composition and process for use thereof
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Worldwide Measurements of Atmospheric CO ₂ and Other Trace Gas Species Using Commercial Airlines
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Machida, T.; Matsueda, H.; Sawa, Y.
Journal of Atmospheric and Oceanic Technology, Vol. 25, Issue 10
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Title: Microsampler and method of making the same

Abstract

Citation Formats

Supramolecular ensembles in eutectic alloys journal, September 2003

Biological preconcentrator patent, September 2008

Regional US carbon sinks from three-dimensional atmospheric CO2 sampling journal, October 2010

Diagnostic potential of the pulsed discharged helium ionization detector (PDHID) for pathogenic Mycobacterial volatile biomarkers journal, July 2013

Phase Change Microvalve for Integrated Devices journal, July 2004

General Principles of Specimen Collection and Transport journal, May 1996

Solar energy storage using phase change materials☆ journal, December 2007

A Monolithically-Integrated μGC Chemical Sensor System journal, June 2011

On-Line Monitoring of Microbial Volatile Metabolites by Proton Transfer Reaction-Mass Spectrometry journal, February 2008

Design Considerations for High Throughput Screening and In Vitro Diagnostic Assays journal, July 2007

Temperature programmable microfabricated gas chromatography column patent, December 2003

Detection of organotin, organomercury, and organolead compounds with a pulsed discharge detector (PDD) journal, August 2002

Method for making electro-fluidic connections in microfluidic devices patent, August 2004

Evaluation of the pulsed discharge helium ionization detector for the analysis of hydrogen and methane in breath journal, February 2004

Carbon fiber composites having improved fatigue resistance patent, February 1992

Zoonotic aspects of Mycobacterium bovis and Mycobacterium avium-intracellulare complex (MAC) journal, May 2005

Methane emissions from terrestrial plants under aerobic conditions journal, January 2006

Solder alloy material layer composition, electroconductive and adhesive composition, flux material layer composition, solder ball transferring sheet, bump and bump forming process, and semiconductore device patent, December 2010

Microvalve for Fuel Cells and Miniature Gas Chromatographic System journal, December 2003

Response to MacDermid et al . journal, September 2014

Volatile compound profiling for the identification of Gram-negative bacteria by ion-molecule reaction-mass spectrometry journal, August 2012

Printable compositions, and their application to dielectric surfaces used in the manufacture of printed circuit boards patent, April 2006

Microfabricated fuel heating value monitoring device patent, May 2010

A phase-change type micropump with aluminum flap valves journal, January 2003

Rapid detection of pathogenic bacteria by volatile organic compound (VOC) analysis conference, February 2002

Method to fabricate silicon chromatographic column comprising fluid ports patent, March 2004

Method to fabricate multi-level silicon-based microstructures via use of an etching delay layer patent, August 2005

CLIMATE CHANGE: Carbon Crucible journal, April 2008

Analysis of non-methane hydrocarbons in air samples collected aboard the CARIBIC passenger aircraft journal, January 2010

Chemical preconcentrator with integral thermal flow sensor patent, March 2003

Review on thermal energy storage with phase change materials and applications journal, February 2009

Determination of product shelf life and activation energy for five drugs of abuse journal, March 1991

Microfabricated diffusion source patent, July 2008

Greenhouse gas analysis of air samples collected onboard the CARIBIC passenger aircraft journal, January 2009

Comprehensive, standardized quality test for glass capillary columns journal, August 1978

Ion mobility spectrometry for microbial volatile organic compounds: a new identification tool for human pathogenic bacteria journal, February 2012

Tin-silver-bismuth solders for electronics assembly patent, August 1995

AirCore: An Innovative Atmospheric Sampling System journal, November 2010

An unmanned aircraft vehicle system for boundary-layer flux measurements over forest canopies conference, January 1994

Microfabricated field calibration assembly for analytical instruments patent, March 2011

Microfabricated thermionic detector patent, October 2012

Gas chromatographic analysis of trace gas impurities in tungsten hexafluoride journal, March 2001

Observational Contrains on the Global Atmospheric Co2 Budget journal, March 1990

Detection of volatile metabolites produced by bacterial growth in blood culture media by selected ion flow tube mass spectrometry (SIFT-MS) journal, May 2006

Recent advancements in the gas-phase MicroChemLab journal, June 2006

Fusible powdered metal paste patent, December 1986

A review of microvalves journal, March 2006

A feasible Global Carbon Cycle Observing System: a plan to decipher today's carbon cycle based on observations journal, June 1996

Tedlar Bag Sampling Technique for Vertical Profiling of Carbon Dioxide through the Atmospheric Boundary Layer with High Precision and Accuracy journal, July 2004

Microsensor clusters journal, January 2002

Micropyrolyzer for chemical analysis of liquid and solid samples patent, July 2006

Varactor with integrated micro-discharge source patent, October 2016

The scent of Mycobacterium tuberculosis – Part II breath journal, July 2009

Individual Comparisons of the Levels of (E)-3-Methyl-2-Hexenoic Acid, an Axillary Odor-Related Compound, in Japanese journal, April 2006

High-accuracy continuous airborne measurements of greenhouse gases (CO 2 and CH 4 ) using the cavity ring-down spectroscopy (CRDS) technique journal, January 2010

Microcollection of Gases in a Capillary Tube: Preservation of Spatial and Temporal Resolution journal, September 2012

Quantifying greenhouse-gas emissions from atmospheric measurements: a critical reality check for climate legislation journal, May 2011

Apparatus for sensing volatile organic chemicals in fluids patent, June 2005

Performance Characteristics of the Aerosol Collectors of the Autonomous Pathogen Detection System (APDS) journal, May 2005

Capacitive chemical sensor patent, May 2014

The scent of Mycobacterium tuberculosis journal, July 2008

System and method for providing vertical profile measurements of atmospheric gases patent, October 2009

Microcombustor patent, September 2004

Radioimmunoassay of tuberculoprotein derived from Mycobacterium tuberculosis. journal, July 1980

Greenhouse gas production and emission from a forest nursery soil following fumigation with chloropicrin and methyl isothiocyanate journal, March 2005

Evaluation of a combination of SIFT-MS and multivariate data analysis for the diagnosis of Mycobacterium bovis in wild badgers journal, January 2009

Valve for fluid control patent, May 2001

Tortuous path chemical preconcentrator patent, September 2010

Methods for improved preconcentrators patent, June 2010

Rapid detection methods for viable Mycobacterium avium subspecies paratuberculosis in milk and cheese journal, July 2010

A latchable microvalve using phase change of paraffin wax journal, February 2007

Sub-to super-ambient temperature programmable microfabricated gas chromatography column patent, March 2004

Solder compositions and methods of making same patent, May 1995

Chemical preconcentrator patent, January 2001

Solder alloy material layer composition, electroconductive and adhesive composition, flux material layer composition, solder ball transferring sheet, bump and bump forming process, and semiconductor device patent, June 2006

LED-based CO2 Sensor for Balloon Deployment conference, January 2011

A gas chromatographic air analyzer fabricated on a silicon wafer journal, December 1979

Supramolecular ensembles in eutectic alloys
journal, September 2003

Biological preconcentrator
patent, September 2008

Regional US carbon sinks from three-dimensional atmospheric CO2 sampling
journal, October 2010

Diagnostic potential of the pulsed discharged helium ionization detector (PDHID) for pathogenic Mycobacterial volatile biomarkers
journal, July 2013

Phase Change Microvalve for Integrated Devices
journal, July 2004

General Principles of Specimen Collection and Transport
journal, May 1996

Solar energy storage using phase change materials☆
journal, December 2007

A Monolithically-Integrated μGC Chemical Sensor System
journal, June 2011

On-Line Monitoring of Microbial Volatile Metabolites by Proton Transfer Reaction-Mass Spectrometry
journal, February 2008

Design Considerations for High Throughput Screening and In Vitro Diagnostic Assays
journal, July 2007

Temperature programmable microfabricated gas chromatography column
patent, December 2003

Detection of organotin, organomercury, and organolead compounds with a pulsed discharge detector (PDD)
journal, August 2002

Method for making electro-fluidic connections in microfluidic devices
patent, August 2004

Evaluation of the pulsed discharge helium ionization detector for the analysis of hydrogen and methane in breath
journal, February 2004

Carbon fiber composites having improved fatigue resistance
patent, February 1992

Zoonotic aspects of Mycobacterium bovis and Mycobacterium avium-intracellulare complex (MAC)
journal, May 2005

Methane emissions from terrestrial plants under aerobic conditions
journal, January 2006

Solder alloy material layer composition, electroconductive and adhesive composition, flux material layer composition, solder ball transferring sheet, bump and bump forming process, and semiconductore device
patent, December 2010

Microvalve for Fuel Cells and Miniature Gas Chromatographic System
journal, December 2003

Response to MacDermid et al .
journal, September 2014

Volatile compound profiling for the identification of Gram-negative bacteria by ion-molecule reaction-mass spectrometry
journal, August 2012

Printable compositions, and their application to dielectric surfaces used in the manufacture of printed circuit boards
patent, April 2006

Microfabricated fuel heating value monitoring device
patent, May 2010

A phase-change type micropump with aluminum flap valves
journal, January 2003

Rapid detection of pathogenic bacteria by volatile organic compound (VOC) analysis
conference, February 2002

Method to fabricate silicon chromatographic column comprising fluid ports
patent, March 2004

Method to fabricate multi-level silicon-based microstructures via use of an etching delay layer
patent, August 2005

CLIMATE CHANGE: Carbon Crucible
journal, April 2008

Analysis of non-methane hydrocarbons in air samples collected aboard the CARIBIC passenger aircraft
journal, January 2010

Chemical preconcentrator with integral thermal flow sensor
patent, March 2003

Review on thermal energy storage with phase change materials and applications
journal, February 2009

Determination of product shelf life and activation energy for five drugs of abuse
journal, March 1991

Microfabricated diffusion source
patent, July 2008

Greenhouse gas analysis of air samples collected onboard the CARIBIC passenger aircraft
journal, January 2009

Comprehensive, standardized quality test for glass capillary columns
journal, August 1978

Ion mobility spectrometry for microbial volatile organic compounds: a new identification tool for human pathogenic bacteria
journal, February 2012

Tin-silver-bismuth solders for electronics assembly
patent, August 1995

AirCore: An Innovative Atmospheric Sampling System
journal, November 2010

An unmanned aircraft vehicle system for boundary-layer flux measurements over forest canopies
conference, January 1994

Microfabricated field calibration assembly for analytical instruments
patent, March 2011

Microfabricated thermionic detector
patent, October 2012

Gas chromatographic analysis of trace gas impurities in tungsten hexafluoride
journal, March 2001

Observational Contrains on the Global Atmospheric Co2 Budget
journal, March 1990

Detection of volatile metabolites produced by bacterial growth in blood culture media by selected ion flow tube mass spectrometry (SIFT-MS)
journal, May 2006

Recent advancements in the gas-phase MicroChemLab
journal, June 2006

Fusible powdered metal paste
patent, December 1986

A review of microvalves
journal, March 2006

A feasible Global Carbon Cycle Observing System: a plan to decipher today's carbon cycle based on observations
journal, June 1996

Tedlar Bag Sampling Technique for Vertical Profiling of Carbon Dioxide through the Atmospheric Boundary Layer with High Precision and Accuracy
journal, July 2004

Microsensor clusters
journal, January 2002

Micropyrolyzer for chemical analysis of liquid and solid samples
patent, July 2006

Varactor with integrated micro-discharge source
patent, October 2016

The scent of Mycobacterium tuberculosis – Part II breath
journal, July 2009

Individual Comparisons of the Levels of (E)-3-Methyl-2-Hexenoic Acid, an Axillary Odor-Related Compound, in Japanese
journal, April 2006

High-accuracy continuous airborne measurements of greenhouse gases (CO ₂ and CH ₄ ) using the cavity ring-down spectroscopy (CRDS) technique
journal, January 2010

Microcollection of Gases in a Capillary Tube: Preservation of Spatial and Temporal Resolution
journal, September 2012

Quantifying greenhouse-gas emissions from atmospheric measurements: a critical reality check for climate legislation
journal, May 2011

Apparatus for sensing volatile organic chemicals in fluids
patent, June 2005

Performance Characteristics of the Aerosol Collectors of the Autonomous Pathogen Detection System (APDS)
journal, May 2005

Capacitive chemical sensor
patent, May 2014

The scent of Mycobacterium tuberculosis
journal, July 2008

System and method for providing vertical profile measurements of atmospheric gases
patent, October 2009

Microcombustor
patent, September 2004

Radioimmunoassay of tuberculoprotein derived from Mycobacterium tuberculosis.
journal, July 1980

Greenhouse gas production and emission from a forest nursery soil following fumigation with chloropicrin and methyl isothiocyanate
journal, March 2005

Evaluation of a combination of SIFT-MS and multivariate data analysis for the diagnosis of Mycobacterium bovis in wild badgers
journal, January 2009

Valve for fluid control
patent, May 2001

Tortuous path chemical preconcentrator
patent, September 2010

Methods for improved preconcentrators
patent, June 2010

Rapid detection methods for viable Mycobacterium avium subspecies paratuberculosis in milk and cheese
journal, July 2010

A latchable microvalve using phase change of paraffin wax
journal, February 2007

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patent, March 2004

Solder compositions and methods of making same
patent, May 1995

Chemical preconcentrator
patent, January 2001

Solder alloy material layer composition, electroconductive and adhesive composition, flux material layer composition, solder ball transferring sheet, bump and bump forming process, and semiconductor device
patent, June 2006

LED-based CO2 Sensor for Balloon Deployment
conference, January 2011

A gas chromatographic air analyzer fabricated on a silicon wafer
journal, December 1979

Solder pastes for providing high elasticity, low rigidity solder joints
patent, March 2006

The STRATEOLE Project Status - 200 pressurized balloons for the polar vortex study
conference, February 2013

Evaluation of solid adsorbent materials for cryogen-free trapping—gas chromatographic analysis of atmospheric C2–C6 non-methane hydrocarbons
journal, November 2006