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Title: Reagents and methods for fluorinating a substrate

Abstract

Described herein are perfluoroalkylated zinc compounds having the structure of Formula (I) or Formula (II), which can be used to perfluoroalkylate organic, inorganic and organometallic substrates. Methods of making and using these compounds by reacting zinc or a dialkylzinc compound with a perfluoroalkyl dihalide in a solvent such as tetrahydrofuran, dioxane or diglyme, are also described.

Inventors:
Issue Date:
Research Org.:
Lehigh Univ., Bethlehem, PA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1496631
Patent Number(s):
10144747
Application Number:
14/903,724
Assignee:
Lehigh University, Bethlehem, PA
Patent Classifications (CPCs):
C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07F - ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS
DOE Contract Number:  
FG02-13ER16369
Resource Type:
Patent
Resource Relation:
Patent File Date: 2014 Jul 08
Country of Publication:
United States
Language:
English

Citation Formats

Vicic, David. Reagents and methods for fluorinating a substrate. United States: N. p., 2018. Web.
Vicic, David. Reagents and methods for fluorinating a substrate. United States.
Vicic, David. Tue . "Reagents and methods for fluorinating a substrate". United States. https://www.osti.gov/servlets/purl/1496631.
@article{osti_1496631,
title = {Reagents and methods for fluorinating a substrate},
author = {Vicic, David},
abstractNote = {Described herein are perfluoroalkylated zinc compounds having the structure of Formula (I) or Formula (II), which can be used to perfluoroalkylate organic, inorganic and organometallic substrates. Methods of making and using these compounds by reacting zinc or a dialkylzinc compound with a perfluoroalkyl dihalide in a solvent such as tetrahydrofuran, dioxane or diglyme, are also described.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2018},
month = {12}
}

Patent:

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