Mechanochemical solid/liquid reaction in formation of alane
Abstract
Methods for forming alane are described. The method drives the alane producing chemical reaction by a mechanical energy source such as a ball mill and includes stabilization of the product with solvent. At least one of the reactants is insoluble in the solvent. Thus, the product is both stabilized and phase-separated from the reactant(s) immediately upon formation. The method can be used to form .alpha.-alane, for instance for use in hydrogen storage.
- Inventors:
- Issue Date:
- Research Org.:
- Savannah River Site (SRS), Aiken, SC (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1495364
- Patent Number(s):
- 10138122
- Application Number:
- 15/482,913
- Assignee:
- Savannah River Nuclear Solutions, LLC (Aiken, SC)
- Patent Classifications (CPCs):
-
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
- DOE Contract Number:
- AC09-08SR22470
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 2017 Apr 10
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Zidan, Ragaiy, and Ward, Patrick A. Mechanochemical solid/liquid reaction in formation of alane. United States: N. p., 2018.
Web.
Zidan, Ragaiy, & Ward, Patrick A. Mechanochemical solid/liquid reaction in formation of alane. United States.
Zidan, Ragaiy, and Ward, Patrick A. Tue .
"Mechanochemical solid/liquid reaction in formation of alane". United States. https://www.osti.gov/servlets/purl/1495364.
@article{osti_1495364,
title = {Mechanochemical solid/liquid reaction in formation of alane},
author = {Zidan, Ragaiy and Ward, Patrick A.},
abstractNote = {Methods for forming alane are described. The method drives the alane producing chemical reaction by a mechanical energy source such as a ball mill and includes stabilization of the product with solvent. At least one of the reactants is insoluble in the solvent. Thus, the product is both stabilized and phase-separated from the reactant(s) immediately upon formation. The method can be used to form .alpha.-alane, for instance for use in hydrogen storage.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2018},
month = {11}
}
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Works referenced in this record:
Method of producing aluminum borohydride
patent, November 1959
- Schechter, William H.
- US Patent Document 2913306
Improvements in the preparation of aluminum hydride containing materials
patent, June 1963
- Koster, Roland
- US Patent Document 3092648
Preparation of sodium and potassium aluminum hydride
patent, May 1968
- Chini, Paolo; Baradel, Agostino; Vacca, Chiara
- US Patent Document 3383186
Process for preparing lithium aluminum hydride
patent, June 1968
- Brendel, Gottfried J.
- US Patent Document 3387947
Preparation of aluminum hydride
patent, May 1974
- Schmidt, Donald L.; Daniels, Arthur L.; Petrella, Ronald V.
- US Patent Document 3812244
Magnesium borohydride diammoniate and triammoniate
patent, August 1986
- Wagner, Ross I.; Grant, Louis R.
- US Patent Document 4,604,271
Method for preparation of an alane-etherate complex and alane
patent, January 2017
- Fisher, Allison M.
- US Patent Document 9,550,672