Solution growth of single-crystal perovskite structures
Abstract
A method for growing single-crystal perovskite structures comprises immersing a film of a metal precursor compound on a surface of a substrate, the metal precursor compound comprising a metal ion B, in a solution comprising a cation precursor compound, the cation precursor compound comprising a cation ion A and an anion X, at a concentration of the cation precursor compound, a growth time, and a growth temperature sufficient to dissolve the film to release the metal ion B to form a complex with the anion X and sufficient to induce recrystallization of the complex with the cation ion A to form a plurality of single-crystal perovskite structures composed of A, B and X. The single-crystal perovskite structures, devices incorporating the same, and methods of using the devices are also provided.
- Inventors:
- Issue Date:
- Research Org.:
- Wisconsin Alumni Research Foundation, Madison, WI (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1483380
- Patent Number(s):
- 10077507
- Application Number:
- 14/954,442
- Assignee:
- Wisconsin Alumni Research Foundation (Madison, WI)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07F - ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
C - CHEMISTRY C30 - CRYSTAL GROWTH C30B - SINGLE-CRYSTAL-GROWTH
- DOE Contract Number:
- SC0002162
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 2015 Nov 30
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE
Citation Formats
Jin, Song, and Fu, Yongping. Solution growth of single-crystal perovskite structures. United States: N. p., 2018.
Web.
Jin, Song, & Fu, Yongping. Solution growth of single-crystal perovskite structures. United States.
Jin, Song, and Fu, Yongping. Tue .
"Solution growth of single-crystal perovskite structures". United States. https://www.osti.gov/servlets/purl/1483380.
@article{osti_1483380,
title = {Solution growth of single-crystal perovskite structures},
author = {Jin, Song and Fu, Yongping},
abstractNote = {A method for growing single-crystal perovskite structures comprises immersing a film of a metal precursor compound on a surface of a substrate, the metal precursor compound comprising a metal ion B, in a solution comprising a cation precursor compound, the cation precursor compound comprising a cation ion A and an anion X, at a concentration of the cation precursor compound, a growth time, and a growth temperature sufficient to dissolve the film to release the metal ion B to form a complex with the anion X and sufficient to induce recrystallization of the complex with the cation ion A to form a plurality of single-crystal perovskite structures composed of A, B and X. The single-crystal perovskite structures, devices incorporating the same, and methods of using the devices are also provided.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2018},
month = {9}
}
Works referenced in this record:
Room-Temperature Near-Infrared High-Q Perovskite Whispering-Gallery Planar Nanolasers
journal, September 2014
- Zhang, Qing; Ha, Son Tung; Liu, Xinfeng
- Nano Letters, Vol. 14, Issue 10
Ultrasmooth organic–inorganic perovskite thin-film formation and crystallization for efficient planar heterojunction solar cells
journal, January 2015
- Zhang, Wei; Saliba, Michael; Moore, David T.
- Nature Communications, Vol. 6, Issue 1
Low-temperature solution-processed wavelength-tunable perovskites for lasing
journal, March 2014
- Xing, Guichuan; Mathews, Nripan; Lim, Swee Sien
- Nature Materials, Vol. 13, Issue 5
Formation Mechanism of Freestanding CH3NH3PbI3 Functional Crystals: In Situ Transformation vs Dissolution–Crystallization
journal, November 2014
- Yang, Shuang; Zheng, Yi Chu; Hou, Yu
- Chemistry of Materials, Vol. 26, Issue 23, p. 6705-6710
Conformal Organohalide Perovskites Enable Lasing on Spherical Resonators
journal, October 2014
- Sutherland, Brandon R.; Hoogland, Sjoerd; Adachi, Michael M.
- ACS Nano, Vol. 8, Issue 10
Solution Growth of Single Crystal Methylammonium Lead Halide Perovskite Nanostructures for Optoelectronic and Photovoltaic Applications
journal, April 2015
- Fu, Yongping; Meng, Fei; Rowley, Matthew B.
- Journal of the American Chemical Society, Vol. 137, Issue 17
High-performance photovoltaic perovskite layers fabricated through intramolecular exchange
journal, May 2015
- Yang, W. S.; Noh, J. H.; Jeon, N. J.
- Science, Vol. 348, Issue 6240
Shape Evolution and Single Particle Luminescence of Organometal Halide Perovskite Nanocrystals
journal, February 2015
- Zhu, Feng; Men, Long; Guo, Yijun
- ACS Nano, Vol. 9, Issue 3
Perovskite Microdisk Microlasers Self-Assembled from Solution
journal, April 2015
- Liao, Qing; Hu, Ke; Zhang, Haihua
- Advanced Materials, Vol. 27, Issue 22
Self-Template-Directed Synthesis of Porous Perovskite Nanowires at Room Temperature for High-Performance Visible-Light Photodetectors
journal, March 2015
- Zhuo, Sifei; Zhang, Jingfang; Shi, Yanmei
- Angewandte Chemie International Edition, Vol. 54, Issue 19
High Photoluminescence Efficiency and Optically Pumped Lasing in Solution-Processed Mixed Halide Perovskite Semiconductors
journal, March 2014
- Deschler, Felix; Price, Michael; Pathak, Sandeep
- The Journal of Physical Chemistry Letters, Vol. 5, Issue 8
An extended Tolerance Factor approach for organic–inorganic perovskites
journal, January 2015
- Kieslich, Gregor; Sun, Shijing; Cheetham, Anthony K.
- Chemical Science, Vol. 6, Issue 6
Compositional engineering of perovskite materials for high-performance solar cells
journal, January 2015
- Jeon, Nam Joong; Noh, Jun Hong; Yang, Woon Seok
- Nature, Vol. 517, Issue 7535
Vapor Phase Synthesis of Organometal Halide Perovskite Nanowires for Tunable Room-Temperature Nanolasers
journal, June 2015
- Xing, Jun; Liu, Xin Feng; Zhang, Qing
- Nano Letters, Vol. 15, Issue 7
Lower threshold for nanowire lasers
journal, May 2015
- Fu, Anthony; Yang, Peidong
- Nature Materials, Vol. 14, Issue 6
Polymer/Perovskite Amplifying Waveguides for Active Hybrid Silicon Photonics
journal, August 2015
- Suárez, Isaac; Juárez-Pérez, Emilio J.; Bisquert, Juan
- Advanced Materials, Vol. 27, Issue 40
Shape-controlled synthesis of organolead halide perovskite nanocrystals and their tunable optical absorption
journal, March 2014
- Chen, Zhenhua; Li, Hui; Tang, Yongbing
- Materials Research Express, Vol. 1, Issue 1, Article No. 015034
Nanowire Perovskite Solar Cell
journal, February 2015
- Im, Jeong-Hyeok; Luo, Jingshan; Franckevičius, Marius
- Nano Letters, Vol. 15, Issue 3
Lead halide perovskite nanowire lasers with low lasing thresholds and high quality factors
journal, April 2015
- Zhu, Haiming; Fu, Yongping; Meng, Fei
- Nature Materials, Vol. 14, Issue 6
Enhanced Amplified Spontaneous Emission in Perovskites Using a Flexible Cholesteric Liquid Crystal Reflector
journal, July 2015
- Stranks, Samuel D.; Wood, Simon M.; Wojciechowski, Konrad
- Nano Letters, Vol. 15, Issue 8
Synthesis and Characterization of Organic−Inorganic Perovskite Thin Films Prepared Using a Versatile Two-Step Dipping Technique
journal, January 1998
- Liang, Kangning; Mitzi, David B.; Prikas, Michael T.
- Chemistry of Materials, Vol. 10, Issue 1, p. 403-411
Synthesis of Organic-Inorganic Lead Halide Perovskite Nanoplatelets: Towards High-Performance Perovskite Solar Cells and Optoelectronic Devices
journal, May 2014
- Ha, Son Tung; Liu, Xinfeng; Zhang, Qing
- Advanced Optical Materials, Vol. 2, Issue 9
Solid-state principles applied to organic–inorganic perovskites: new tricks for an old dog
journal, January 2014
- Kieslich, Gregor; Sun, Shijing; Cheetham, Anthony K.
- Chem. Sci., Vol. 5, Issue 12