High capacity anode materials for lithium ion batteries

Lopez, Herman A.; Anguchamy, Yogesh Kumar; Deng, Haixia; Han, Yongbong; Masarapu, Charan; Venkatachalam, Subramanian; Kumar, Sujeet

Title: High capacity anode materials for lithium ion batteries

Abstract

High capacity silicon based anode active materials are described for lithium ion batteries. These materials are shown to be effective in combination with high capacity lithium rich cathode active materials. Supplemental lithium is shown to improve the cycling performance and reduce irreversible capacity loss for at least certain silicon based active materials. In particular silicon based active materials can be formed in composites with electrically conductive coatings, such as pyrolytic carbon coatings or metal coatings, and composites can also be formed with other electrically conductive carbon components, such as carbon nanofibers and carbon nanoparticles. Additional alloys with silicon are explored.

Inventors:: Lopez, Herman A.; Anguchamy, Yogesh Kumar; Deng, Haixia; Han, Yongbong; Masarapu, Charan; Venkatachalam, Subramanian; Kumar, Sujeet

Issue Date:: 2018-06-19

Research Org.:: Zenlabs Energy, Inc., Fremont, CA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1458524

Patent Number(s):: 10003068

Application Number:: 14/851,405

Assignee:: Zenlabs Energy, Inc. (Fremont, CA)

Patent Classifications (CPCs):: C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25F - PROCESSES FOR THE ELECTROLYTIC REMOVAL OF MATERIALS FROM OBJECTS

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY

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C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25F - PROCESSES FOR THE ELECTROLYTIC REMOVAL OF MATERIALS FROM OBJECTS
C25F3/12 - of semiconducting materials

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M10/0525 - Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes
H01M2004/027 - {Negative electrodes}
H01M2004/028 - {Positive electrodes}
H01M2220/30 - Batteries in portable systems, e.g. mobile phone, laptop
H01M4/131 - Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
H01M4/133 - Electrodes based on carbonaceous material, e.g. graphite-intercalation compounds or CFx
H01M4/134 - Electrodes based on metals, Si or alloys
H01M4/364 - {as mixtures}
H01M4/38 - of elements or alloys
H01M4/386 - {Silicon or alloys based on silicon}
H01M4/505 - of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
H01M4/525 - of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
H01M4/587 - for inserting or intercalating light metals
H01M4/621 - {Binders}
H01M4/622 - {being polymers}

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/10 - Energy storage

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DOE Contract Number:: AR0000034

Resource Type:: Patent

Resource Relation:: Patent File Date: 2015 Sep 11

Country of Publication:: United States

Language:: English

Subject:: 25 ENERGY STORAGE

Citation Formats


                    Lopez, Herman A., Anguchamy, Yogesh Kumar, Deng, Haixia, Han, Yongbong, Masarapu, Charan, Venkatachalam, Subramanian, and Kumar, Sujeet. High capacity anode materials for lithium ion batteries.  United States: N. p., 2018. 
        Web.

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                    Lopez, Herman A., Anguchamy, Yogesh Kumar, Deng, Haixia, Han, Yongbong, Masarapu, Charan, Venkatachalam, Subramanian, & Kumar, Sujeet. High capacity anode materials for lithium ion batteries.  United States.

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                    Lopez, Herman A., Anguchamy, Yogesh Kumar, Deng, Haixia, Han, Yongbong, Masarapu, Charan, Venkatachalam, Subramanian, and Kumar, Sujeet. Tue .  
        "High capacity anode materials for lithium ion batteries".  United States.  https://www.osti.gov/servlets/purl/1458524.

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@article{osti_1458524,

  title        = {High capacity anode materials for lithium ion batteries},

  author       = {Lopez, Herman A. and Anguchamy, Yogesh Kumar and Deng, Haixia and Han, Yongbong and Masarapu, Charan and Venkatachalam, Subramanian and Kumar, Sujeet},

  abstractNote = {High capacity silicon based anode active materials are described for lithium ion batteries. These materials are shown to be effective in combination with high capacity lithium rich cathode active materials. Supplemental lithium is shown to improve the cycling performance and reduce irreversible capacity loss for at least certain silicon based active materials. In particular silicon based active materials can be formed in composites with electrically conductive coatings, such as pyrolytic carbon coatings or metal coatings, and composites can also be formed with other electrically conductive carbon components, such as carbon nanofibers and carbon nanoparticles. Additional alloys with silicon are explored.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2018},

  month        = {6}

}

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High Capacity, Temperature-Stable Lithium Aluminum Manganese Oxide Cathodes for Rechargeable Batteries
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AlF₃-Coating to Improve High Voltage Cycling Performance of Li[Ni_1∕3]Co_1∕3]Mn_1∕3]O₂ Cathode Materials for Lithium Secondary Batteries
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Battery Packs for Vehicles and High Capacity Pouch Secondary Batteries for Incorporation into Compact Battery Packs
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Method of producing porous silicon particles by stain-etching and silicon nanoparticles from stain-etched silicon powder
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SI/C Composite, Anode Active Materials, and Lithium Battery Including the Same
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Coated Positive Electrode Materials For Lithium Ion Batteries
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Carbon-Coated Silicon Particle Powder as the Anode Material for Lithium Ion Batteries and Method of Making the Same
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Silicon composite particles, preparation thereof, and negative electrode material for non-aqueous electrolyte secondary cell
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Lithium metal oxide electrodes for lithium cells and batteries
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Negative electrode for rechargeable lithium battery and method for fabrication thereof
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Schönenberger, Christian; Forró, Laszlo
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https://doi.org/10.1088/2058-7058/13/6/27

Secondary battery
patent, July 1990

Miyabayashi, Mitsutaka; Nishii, Toshifumi; Yui, Hiroshi
US Patent Document 4,945,014
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4945014

Lithium Insertion in Carbon-Silicon Composite Materials Produced by Mechanical Milling
journal, January 1998

Wang, C. S.; Wu, G. T.; Zhang, X. B.
Journal of The Electrochemical Society, Vol. 145, Issue 8, p. 2751-2758
https://doi.org/10.1149/1.1838709

Secondary battery
patent, April 2005

Fujita, Shigeru; Akashi, Hiroyuki; Adachi, Momoe
US Patent Document 6,884,546
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6884546

Electrode material for anode of rechargeable lithium battery, electrode structural body using said electrode material, rechargeable lithium battery using said electrode structural body, process for producing said electrode structural body, and process for producing said rechargeable lithium battery
patent-application, August 2005

Kawakami, Soichiro; Asao, Masaya
US Patent Application 11/104440; 20050175901
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20050175901

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Title: High capacity anode materials for lithium ion batteries

Abstract

Citation Formats

High energy electrochemical cell having composite solid-state anode patent, September 1992

Nonaqueous electrolyte secondary battery patent-application, September 2008

Method of Depositing Silicon on Carbon Nanomaterials patent-application, October 2012

Battery including carbon foam current collectors patent, December 2005

Negative active material for a rechargeable lithium battery, a method of preparing the same, and a rechargeable lithium battery comprising the same patent, April 2009

Silicon composite, making method, and non-aqueous electrolyte secondary cell negative electrode material patent-application, January 2006

A new approach to improve the high-voltage cyclic performance of Li-rich layered cathode material by electrochemical pre-treatment journal, August 2008

Electrochemical secondary element patent, November 1992

Electrode for use in lithium battery and rechargeable lithium battery patent, March 2007

Lithium Ion Battery With High Voltage Electrolytes And Additives patent-application, June 2011

Nanowire battery methods and arrangements patent, October 2010

Secondary Battery patent-application, December 2009

Negative Electrode Material For Lithium Secondary Battery, Negative Electrode Using The Material, Lithium Secondary Battery Using The Negative Electrode, And Manufacturing Method Of Negative Electrode Material patent-application, May 2008

A new SiO/C anode composition for lithium-ion battery journal, April 2008

Electrode structure for lithium secondary battery and secondary battery having such electrode structure patent, November 2009

Negative electrode for nonaqueous secondary battery patent-application, March 2006

Layered Li(Li0.2Ni0.15+0.5zCo0.10Mn0.55−0.5z)O2−zFz cathode materials for Li-ion secondary batteries journal, August 2005

Cyclic deterioration and its improvement for Li-rich layered cathode material Li[Ni0.17Li0.2Co0.07Mn0.56]O2 journal, January 2010

Amorphous electrode compositions patent, March 2004

Lithium Ion Batteries With Long Cycling Performance patent-application, January 2011

Electrochemical behaviors of silicon based anode material journal, August 2005

Battery including an electrolyte solution comprising a halogenated carbonate derivative patent, July 2010

Nano-sized SiOx/C composite anode for lithium ion batteries journal, May 2011

Interweaved Si@SiOx/C nanoporous spheres as anode materials for Li-ion batteries journal, July 2012

Silicon/germanium particle inks, doped particles, printing and processes for semiconductor applications patent-application, July 2008

High Energy Lithium Ion Batteries With Particular Negative Electrode Compositions patent-application, December 2009

Secondary lithium ion battery containing a prelithiated anode patent-application, July 2010

Very Long Cycling of Lithium Ion Batteries with Lithium Rich Cathode Materials patent-application, March 2012

Multiphase nanocomposite material and method for its manufacture patent-application, July 2004

Improvement of High-Voltage Cycling Behavior of Surface-Modified Li[Ni[sub 1∕3]Co[sub 1∕3]Mn[sub 1∕3]]O[sub 2] Cathodes by Fluorine Substitution for Li-Ion Batteries journal, July 2005

Method for intercalating alkali metal ions into carbon electrodes patent, August 1995

Lithium Secondary Battery with High Energy Density patent-application, December 2010

Establishing Sustainable US HEV/PHEV Manufacturing Base: Stabilized Lithium Metal Powder, Enabling Material And Revolutionary Technology For High Energy Li-Ion Batteries report, December 2012

Hybrid anode compositions for lithium ion batteries patent-application, May 2009

Anode for Lithium Ion Cell patent-application, November 2008

Carbon−Silicon Core−Shell Nanowires as High Capacity Electrode for Lithium Ion Batteries journal, September 2009

Superior Storage Performance of a Si@SiOx/C Nanocomposite as Anode Material for Lithium-Ion Batteries journal, February 2008

Non-aqueous electrolyte secondary battery and its production method patent, March 1995

Negative electrode material for use in lithium-ion secondary battery and process for producing the same patent, August 1998

Lithium ion cell patent, February 2000

Non-aqueous electrolyte secondary battery patent, July 2000

High density electrode and battery using the electrode patent-application, August 2006

Composite Compositions, Negative Electrodes with Composite Compositions and Corresponding Batteries patent-application, May 2010

Alloy composition for lithium ion batteries patent, January 2011

Composite Anode Active Material, Anode Including the Same and Lithium Battery Using the Anode patent-application, January 2009

Method of making activated carbon derived from pitches patent, June 2001

Electrode composite, battery electrode formed from said composite, and lithium battery comprising such as electrode patent-application, July 2011

High capacity Li[Li0.2Ni0.2Mn0.6]O2 cathode materials via a carbonate co-precipitation method journal, November 2006

Conductive silicon composite, preparation thereof, and negative electrode material for non-aqueous electrolyte secondary cell patent-application, November 2003

High-performance lithium battery anodes using silicon nanowires book, October 2010

Synthesis of spherical Li[Ni(1/3−z)Co(1/3−z)Mn(1/3−z)Mgz]O2 as positive electrode material for lithium-ion battery journal, February 2006

Preloading Lithium Ion Cell Components With Lithium patent-application, May 2011

Secondary lithium-ion cell with an auxiliary electrode patent, January 2002

High Energy Lithium Ion Secondary Batteries patent-application, October 2009

Electrolytes, Electrolyte Additives And Cells patent-application, June 2008

Lithium secondary battery, anode for lithium secondary battery, and method for manufacturing the anode patent-application, October 2001

Alloy compositions for lithium ion batteries patent, December 2010

Nonaqueous secondary battery containing silicic material patent, May 2001

Metal Halide Coatings On Lithium Ion Battery Positive Electrode Materials And Corresponding Batteries patent-application, March 2012

Nonaqueous Secondary Battery patent-application, September 2010

Electrochemical characterization of a novel Si–graphite–Li2.6Co0.4N composite as anode material for lithium secondary batteries journal, January 2005

Silicon-Containing Alloys Useful as Electrodes for Lithium-Ion Batteries patent-application, June 2007

Lithium Ion Batteries Based On Nanoporous Silicon patent-application, March 2013

Silicon-silicon oxide-lithium composite, making method, and non-aqueous electrolyte secondary cell negative electrode material patent, August 2010

Electrical transport in doped multiwalled carbon nanotubes journal, April 2001

Lithium secondary battery, anode for lithium secondary battery, and method for manufacturing the anode patent, November 2003

Lithium Ion Batteries With Supplemental Lithium patent-application, May 2012

Method of Producing Silicon Oxide, Negative Electrode Active Material for lithium Ion Secondary Battery and Lithium Ion Secondary Battery Using the Same patent-application, July 2010

Lithium-ion battery patent, September 2009

Negative Electrode for Lithium Ion Secondary Battery and Lithium Ion Secondary Battery patent-application, September 2008

Fluorine Doped Lithium Rich Metal Oxide Positive Electrode Battery Materials With High Specific Capacity and Corresponding Batteries patent-application, April 2010

Anodes for rechargeable lithium batteries patent, March 2003

Lithium metal dispersion in secondary battery anodes patent, October 2007

Improvement of cycling stability of Si anode by mechanochemcial reduction and carbon coating journal, April 2009

High-performance lithium battery anodes using silicon nanowires journal, December 2007

Rechargeable lithium battery having improved reversible capacity patent, February 1998

Comments on the structural complexity of lithium-rich Li1+xM1−xO2 electrodes (M=Mn, Ni, Co) for lithium batteries journal, September 2006

High energy electrochemical cell having composite solid-state anode
patent, September 1992

Nonaqueous electrolyte secondary battery
patent-application, September 2008

Method of Depositing Silicon on Carbon Nanomaterials
patent-application, October 2012

Battery including carbon foam current collectors
patent, December 2005

Negative active material for a rechargeable lithium battery, a method of preparing the same, and a rechargeable lithium battery comprising the same
patent, April 2009

Silicon composite, making method, and non-aqueous electrolyte secondary cell negative electrode material
patent-application, January 2006

A new approach to improve the high-voltage cyclic performance of Li-rich layered cathode material by electrochemical pre-treatment
journal, August 2008

Electrochemical secondary element
patent, November 1992

Electrode for use in lithium battery and rechargeable lithium battery
patent, March 2007

Lithium Ion Battery With High Voltage Electrolytes And Additives
patent-application, June 2011

Nanowire battery methods and arrangements
patent, October 2010

Secondary Battery
patent-application, December 2009

Negative Electrode Material For Lithium Secondary Battery, Negative Electrode Using The Material, Lithium Secondary Battery Using The Negative Electrode, And Manufacturing Method Of Negative Electrode Material
patent-application, May 2008

A new SiO/C anode composition for lithium-ion battery
journal, April 2008

Electrode structure for lithium secondary battery and secondary battery having such electrode structure
patent, November 2009

Negative electrode for nonaqueous secondary battery
patent-application, March 2006

Layered Li(Li_0.2Ni_0.15+0.5zCo_0.10Mn_0.55−0.5z)O_2−zF_z cathode materials for Li-ion secondary batteries
journal, August 2005

Cyclic deterioration and its improvement for Li-rich layered cathode material Li[Ni_0.17Li_0.2Co_0.07Mn_0.56]O₂
journal, January 2010

Amorphous electrode compositions
patent, March 2004

Lithium Ion Batteries With Long Cycling Performance
patent-application, January 2011

Electrochemical behaviors of silicon based anode material
journal, August 2005

Battery including an electrolyte solution comprising a halogenated carbonate derivative
patent, July 2010

Nano-sized SiO_x/C composite anode for lithium ion batteries
journal, May 2011

Interweaved Si@SiO_x/C nanoporous spheres as anode materials for Li-ion batteries
journal, July 2012

Silicon/germanium particle inks, doped particles, printing and processes for semiconductor applications
patent-application, July 2008

High Energy Lithium Ion Batteries With Particular Negative Electrode Compositions
patent-application, December 2009

Secondary lithium ion battery containing a prelithiated anode
patent-application, July 2010

Very Long Cycling of Lithium Ion Batteries with Lithium Rich Cathode Materials
patent-application, March 2012

Multiphase nanocomposite material and method for its manufacture
patent-application, July 2004

Improvement of High-Voltage Cycling Behavior of Surface-Modified Li[Ni[sub 1∕3]Co[sub 1∕3]Mn[sub 1∕3]]O[sub 2] Cathodes by Fluorine Substitution for Li-Ion Batteries
journal, July 2005

Method for intercalating alkali metal ions into carbon electrodes
patent, August 1995

Lithium Secondary Battery with High Energy Density
patent-application, December 2010

Establishing Sustainable US HEV/PHEV Manufacturing Base: Stabilized Lithium Metal Powder, Enabling Material And Revolutionary Technology For High Energy Li-Ion Batteries
report, December 2012

Hybrid anode compositions for lithium ion batteries
patent-application, May 2009

Anode for Lithium Ion Cell
patent-application, November 2008

Carbon−Silicon Core−Shell Nanowires as High Capacity Electrode for Lithium Ion Batteries
journal, September 2009

Superior Storage Performance of a Si@SiO_x/C Nanocomposite as Anode Material for Lithium-Ion Batteries
journal, February 2008

Non-aqueous electrolyte secondary battery and its production method
patent, March 1995

Negative electrode material for use in lithium-ion secondary battery and process for producing the same
patent, August 1998

Lithium ion cell
patent, February 2000

Non-aqueous electrolyte secondary battery
patent, July 2000

High density electrode and battery using the electrode
patent-application, August 2006

Composite Compositions, Negative Electrodes with Composite Compositions and Corresponding Batteries
patent-application, May 2010

Alloy composition for lithium ion batteries
patent, January 2011

Composite Anode Active Material, Anode Including the Same and Lithium Battery Using the Anode
patent-application, January 2009

Method of making activated carbon derived from pitches
patent, June 2001

Electrode composite, battery electrode formed from said composite, and lithium battery comprising such as electrode
patent-application, July 2011

High capacity Li[Li_0.2Ni_0.2Mn_0.6]O₂ cathode materials via a carbonate co-precipitation method
journal, November 2006

Conductive silicon composite, preparation thereof, and negative electrode material for non-aqueous electrolyte secondary cell
patent-application, November 2003

High-performance lithium battery anodes using silicon nanowires
book, October 2010

Synthesis of spherical Li[Ni_(1/3−z)Co_(1/3−z)Mn_(1/3−z)Mg_z]O₂ as positive electrode material for lithium-ion battery
journal, February 2006

Preloading Lithium Ion Cell Components With Lithium
patent-application, May 2011

Secondary lithium-ion cell with an auxiliary electrode
patent, January 2002

High Energy Lithium Ion Secondary Batteries
patent-application, October 2009

Electrolytes, Electrolyte Additives And Cells
patent-application, June 2008

Lithium secondary battery, anode for lithium secondary battery, and method for manufacturing the anode
patent-application, October 2001

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patent, December 2010

Nonaqueous secondary battery containing silicic material
patent, May 2001

Metal Halide Coatings On Lithium Ion Battery Positive Electrode Materials And Corresponding Batteries
patent-application, March 2012

Nonaqueous Secondary Battery
patent-application, September 2010

Electrochemical characterization of a novel Si–graphite–Li_2.6Co_0.4N composite as anode material for lithium secondary batteries
journal, January 2005

Silicon-Containing Alloys Useful as Electrodes for Lithium-Ion Batteries
patent-application, June 2007

Lithium Ion Batteries Based On Nanoporous Silicon
patent-application, March 2013

Silicon-silicon oxide-lithium composite, making method, and non-aqueous electrolyte secondary cell negative electrode material
patent, August 2010

Electrical transport in doped multiwalled carbon nanotubes
journal, April 2001

Lithium secondary battery, anode for lithium secondary battery, and method for manufacturing the anode
patent, November 2003

Lithium Ion Batteries With Supplemental Lithium
patent-application, May 2012

Method of Producing Silicon Oxide, Negative Electrode Active Material for lithium Ion Secondary Battery and Lithium Ion Secondary Battery Using the Same
patent-application, July 2010

Lithium-ion battery
patent, September 2009

Negative Electrode for Lithium Ion Secondary Battery and Lithium Ion Secondary Battery
patent-application, September 2008

Fluorine Doped Lithium Rich Metal Oxide Positive Electrode Battery Materials With High Specific Capacity and Corresponding Batteries
patent-application, April 2010

Anodes for rechargeable lithium batteries
patent, March 2003

Lithium metal dispersion in secondary battery anodes
patent, October 2007

Improvement of cycling stability of Si anode by mechanochemcial reduction and carbon coating
journal, April 2009

High-performance lithium battery anodes using silicon nanowires
journal, December 2007

Rechargeable lithium battery having improved reversible capacity
patent, February 1998

Comments on the structural complexity of lithium-rich Li_1+xM_1−xO₂ electrodes (M=Mn, Ni, Co) for lithium batteries
journal, September 2006

Significant Improvement of Electrochemical Performance of AlF₃-Coated Li[Ni_0.8Co_0.1Mn_0.1]O₂ Cathode Materials
journal, January 2007

Negative active material for a rechargeable lithium battery, a method of preparing the same, and a rechargeable lithium battery comprising the same
patent-application, October 2005

High Energy Density Redox Flow Device
patent-application, February 2010