Mechanical design of thin-film diamond crystal mounting apparatus with optimized thermal contact and crystal strain for coherence preservation x-ray optics

Shu, Deming; Shvydko, Yury; Stoupin, Stanislav; Kim, Kwang-Je

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Title: Mechanical design of thin-film diamond crystal mounting apparatus with optimized thermal contact and crystal strain for coherence preservation x-ray optics

Abstract

A method and mechanical design for a thin-film diamond crystal mounting apparatus for coherence preservation x-ray optics with optimized thermal contact and minimized crystal strain are provided. The novel thin-film diamond crystal mounting apparatus mounts a thin-film diamond crystal supported by a thick chemical vapor deposition (CVD) diamond film spacer with a thickness slightly thicker than the thin-film diamond crystal, and two groups of thin film thermal conductors, such as thin CVD diamond film thermal conductor groups separated by the thick CVD diamond spacer. The two groups of thin CVD film thermal conductors provide thermal conducting interface media with the thin-film diamond crystal. A piezoelectric actuator is integrated into a flexural clamping mechanism generating clamping force from zero to an optimal level.

Inventors:: Shu, Deming; Shvydko, Yury; Stoupin, Stanislav; Kim, Kwang-Je

Issue Date:: 2018-05-08

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1440540

Patent Number(s):: 9966161

Application Number:: 14/859,697

Assignee:: UChicago Argonne, LLC (Chicago, IL)

Patent Classifications (CPCs):: G - PHYSICS G21 - NUCLEAR PHYSICS G21K - TECHNIQUES FOR HANDLING PARTICLES OR IONISING RADIATION NOT OTHERWISE PROVIDED FOR

H - ELECTRICITY H05 - ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR H05G - X-RAY TECHNIQUE

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G - PHYSICS G21 - NUCLEAR PHYSICS G21K - TECHNIQUES FOR HANDLING PARTICLES OR IONISING RADIATION NOT OTHERWISE PROVIDED FOR
G21K1/06 - using diffraction, refraction or reflection, e.g. monochromators

H - ELECTRICITY H05 - ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR H05G - X-RAY TECHNIQUE
H05G1/00 - X-ray apparatus involving X-ray tubes

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DOE Contract Number:: AC02-06CH11357

Resource Type:: Patent

Resource Relation:: Patent File Date: 2015 Sep 21

Country of Publication:: United States

Language:: English

Subject:: 42 ENGINEERING

Citation Formats


                    Shu, Deming, Shvydko, Yury, Stoupin, Stanislav, and Kim, Kwang-Je. Mechanical design of thin-film diamond crystal mounting apparatus with optimized thermal contact and crystal strain for coherence preservation x-ray optics.  United States: N. p., 2018. 
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                    Shu, Deming, Shvydko, Yury, Stoupin, Stanislav, & Kim, Kwang-Je. Mechanical design of thin-film diamond crystal mounting apparatus with optimized thermal contact and crystal strain for coherence preservation x-ray optics.  United States.

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                    Shu, Deming, Shvydko, Yury, Stoupin, Stanislav, and Kim, Kwang-Je. Tue .  
        "Mechanical design of thin-film diamond crystal mounting apparatus with optimized thermal contact and crystal strain for coherence preservation x-ray optics".  United States.  https://www.osti.gov/servlets/purl/1440540.

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@article{osti_1440540,

  title        = {Mechanical design of thin-film diamond crystal mounting apparatus with optimized thermal contact and crystal strain for coherence preservation x-ray optics},

  author       = {Shu, Deming and Shvydko, Yury and Stoupin, Stanislav and Kim, Kwang-Je},

  abstractNote = {A method and mechanical design for a thin-film diamond crystal mounting apparatus for coherence preservation x-ray optics with optimized thermal contact and minimized crystal strain are provided. The novel thin-film diamond crystal mounting apparatus mounts a thin-film diamond crystal supported by a thick chemical vapor deposition (CVD) diamond film spacer with a thickness slightly thicker than the thin-film diamond crystal, and two groups of thin film thermal conductors, such as thin CVD diamond film thermal conductor groups separated by the thick CVD diamond spacer. The two groups of thin CVD film thermal conductors provide thermal conducting interface media with the thin-film diamond crystal. A piezoelectric actuator is integrated into a flexural clamping mechanism generating clamping force from zero to an optimal level.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2018},

  month        = {5}

}

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DOI: https://doi.org/10.1063/1.4952839
Mechanical design of multiple zone plates precision alignment apparatus for hard X-ray focusing in twenty-nanometer scale

Patent Shu, Deming; Liu, Jie; Gleber, Sophie C.; ...

An enhanced mechanical design of multiple zone plates precision alignment apparatus for hard x-ray focusing in a twenty-nanometer scale is provided. The precision alignment apparatus includes a zone plate alignment base frame; a plurality of zone plates; and a plurality of zone plate holders, each said zone plate holder for mounting and aligning a respective zone plate for hard x-ray focusing. At least one respective positioning stage drives and positions each respective zone plate holder. Each respective positioning stage is mounted on the zone plate alignment base frame. A respective linkage component connects each respective positioning stage and the respectivemore » « less
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Apparatus and method for characterizing thin film and interfaces using an optical heat generator and detector

Patent Maris, Humphrey J [Barrington, RI]; Stoner, Robert J [Duxbury, MA]

An optical heat generation and detection system generates a first non-destructive pulsed beam of electromagnetic radiation that is directed upon a sample containing at least one interface between similar or dissimilar materials. The first pulsed beam of electromagnetic radiation, a pump beam (21a), produces a non-uniform temperature change within the sample. A second non-destructive pulsed beam of electromagnetic radiation, a probe beam (21b), is also directed upon the sample. Physical and chemical properties of the materials, and of the interface, are measured by observing changes in a transient optical response of the sample to the probe beam, as revealed bymore » « less
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Optical apparatus using liquid crystals for shaping the spatial intensity of optical beams having designated wavelengths

Patent Jacobs, Stephen D [Pittsford, NY]; Cerqua, Kathleen A [Rochester, NY]

The spatial intensity profile of an optical beam of designated wavelengths, such as a laser beam, is shaped (the beam is apodized) by means of cholesteric liquid crystals of opposite chirality disposed successively along the path of the beam. The crystals have curved surfaces, which may be defined by a lens which defines the thickness of the liquid crystal fluid gap in a liquid crystal cell, so as to vary the selective reflection of the designated wavelength across the aperture of the beam. In this way, a soft aperture is provided. By using tandem cell pairs having liquid crystals ofmore » « less
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Apparatus and method for measurement of the mechanical properties and electromigration of thin films

Patent Maris, Humphrey J [Barrington, RI]

A method for characterizing a sample comprising the steps of depositing the sample on a substrate, measuring a first change in optical response of the sample, changing the lateral strain of the sample, measuring a second change in optical response of the sample, comparing the second change in optical response of with the first change in optical response and associating a difference between the second change and the first change in optical response with a property of interest in the sample. The measurement of the first change in optical response is made with the sample having an initial lateral strain.more » « less
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Title: Mechanical design of thin-film diamond crystal mounting apparatus with optimized thermal contact and crystal strain for coherence preservation x-ray optics

Abstract

Citation Formats

Two-axis sagittal focusing monochromator patent, May 2014

Double crystal analyzer linkage patent, August 2006

X-ray spectrometer and apparatus for XAFS measurements patent, September 2002

Mechanical design of multiple zone plates precision alignment apparatus for hard X-ray focusing in twenty-nanometer scale patent, April 2017

All-diamond optical assemblies for a beam-multiplexing X-ray monochromator at the Linac Coherent Light Source journal, August 2014

Diamond-anvil high-pressure cell with improved X-ray collimation system patent, July 1986

Optical design for laser encoder resolution extension with three-dimensional motion decoupling patent, November 2004

Multi-beam X-ray system patent, February 2012

Method and device for generating ultra-high pressure patent, June 2010

Diamond uses/applications based on single-crystal CVD diamond produced at rapid growth rate patent, October 2010

Substrate including a diamond layer and a composite layer of diamond and silicon carbide, and, optionally, silicon patent, October 2016

Diamond crystal optics for self-seeding of hard X-rays in X-ray free-electron lasers journal, March 2013

X-ray exposure apparatus, X-ray exposure method, X-ray mask, X-ray mirror, synchrotron radiation apparatus, synchrotron radiation method and semiconductor device patent, September 2005

Diamond anvil cell assembly patent, December 1997

Single crystal silicon carbide layers on diamond and associated methods patent, September 2010

Hybrid diamond-silicon angular-dispersive x-ray monochromator with 0.25-meV energy bandwidth and high spectral efficiency journal, January 2013

Mechanical design of laminar weak-link rotary mechanisms with ten-degree-level travel range and ten-nanoradian-level positioning resolution patent, January 2012

XRF system having multiple excitation energy bands in highly aligned package patent, October 2013

Robot-based automation system for cryogenic crystal sample mounting patent, January 2007

Time-delayed beam splitting with energy separation of x-ray channels journal, October 2013

Performance of a beam-multiplexing diamond crystal monochromator at the Linac Coherent Light Source journal, June 2014

X-ray beam conditioning patent, February 2016

High crystalline quality synthetic diamond patent, September 2015

Redundantly constrained laminar structure as weak-link mechanisms patent, January 2006

High pressure anvil and optical window patent, April 2003

Anvils and ultra-high pressure apparatuses using the same patent, November 2015

Tunable optical cavity for an x-ray free-electron-laser oscillator journal, March 2009

Method and device for generating ultra-high pressure patent, February 2008

High energy resolution, high angular acceptance crystal monochromator patent, June 1996

Redundantly constrained laminar structure as weak-link mechanisms patent, August 2003

Colorless single-crystal CVD diamond at rapid growth rate patent, February 2011

Method for achieving high pressure using isotopically-pure diamond anvils patent, March 1994

Energy storage arrangement patent, May 1992

Method for manufacturing diamond monocrystal having a thin film, and diamond monocrystal having a thin film patent, February 2012

Precision mechanical structure of an ultra-high-resolution spectrometer for inelastic X-ray scattering instrument patent, April 2015

Energy storage arrangement patent, September 2009

Tuning and synthesis of metallic nanostructures by mechanical compression patent, November 2015

Demonstration of self-seeding in a hard-X-ray free-electron laser journal, August 2012

System and method for producing synthetic diamond patent, June 2003

Surface acoustic wave (SAW) devices based on cubic boron nitride/diamond composite structures patent, August 2009

X-ray diffractometer having co-exiting stages optimized for single crystal and bulk diffraction patent, December 2010

Fluorescent X-ray analysis apparatus patent, April 2005

Sagittal focusing Laue monochromator patent, March 2009

Highly aligned x-ray optic and source assembly for precision x-ray analysis applications patent, June 2010

Mechanical design of deformation compensated flexural pivots structured for linear nanopositioning stages patent, February 2015

Diamond-coated electrode and method for producing same patent, January 2008

Diamond composite substrate and process for producing the same patent, February 2011

Electronic device and method of use thereof patent, July 2000

Monocrystalline diamond layer and method for the production thereof patent, July 2008

X-ray monitoring optical elements patent, December 2016

Diamond field emission tip and a method of formation patent, September 2010

Chemically bonded diamond films and method for producing same patent, April 1989

Tunable CVD diamond structures patent, February 2005

Ultratough CVD single crystal diamond and three dimensional growth thereof patent, September 2009

Diamond substrate and manufacturing method thereof patent, June 2008

Optical contact micrometer patent, August 2014

Method for making nanomaterials patent, June 2013

Method and apparatus for making parallel X-ray beam and X-ray diffraction apparatus patent, July 2005

Double bevel construction of a diamond anvil patent, October 1988

Multidimensional alignment apparatus for hard x-ray focusing with two multilayer laue lenses patent, October 2009

Target and X-ray generating tube including the same, X-ray generating apparatus, X-ray imaging system patent, November 2016

BX90: A new diamond anvil cell design for X-ray diffraction and optical measurements journal, December 2012

Design of a diamond-crystal monochromator for the LCLS hard x-ray self-seeding project journal, March 2013

Diamond anvil cell and high-pressure physical investigations journal, January 1983

Channel-cut monochromator patent, June 2003

Method of growing diamond thin film patent, December 2015

X-ray diffraction apparatus patent, October 2004

Asymmetrical 4-crystal monochromator patent, April 1996

Confinement of hydrogen at high pressure in carbon nanotubes patent, December 2011

Two-axis sagittal focusing monochromator
patent, May 2014

Double crystal analyzer linkage
patent, August 2006

X-ray spectrometer and apparatus for XAFS measurements
patent, September 2002

Mechanical design of multiple zone plates precision alignment apparatus for hard X-ray focusing in twenty-nanometer scale
patent, April 2017

All-diamond optical assemblies for a beam-multiplexing X-ray monochromator at the Linac Coherent Light Source
journal, August 2014

Diamond-anvil high-pressure cell with improved X-ray collimation system
patent, July 1986

Optical design for laser encoder resolution extension with three-dimensional motion decoupling
patent, November 2004

Multi-beam X-ray system
patent, February 2012

Method and device for generating ultra-high pressure
patent, June 2010

Diamond uses/applications based on single-crystal CVD diamond produced at rapid growth rate
patent, October 2010

Substrate including a diamond layer and a composite layer of diamond and silicon carbide, and, optionally, silicon
patent, October 2016

Diamond crystal optics for self-seeding of hard X-rays in X-ray free-electron lasers
journal, March 2013

X-ray exposure apparatus, X-ray exposure method, X-ray mask, X-ray mirror, synchrotron radiation apparatus, synchrotron radiation method and semiconductor device
patent, September 2005

Diamond anvil cell assembly
patent, December 1997

Single crystal silicon carbide layers on diamond and associated methods
patent, September 2010

Hybrid diamond-silicon angular-dispersive x-ray monochromator with 0.25-meV energy bandwidth and high spectral efficiency
journal, January 2013

Mechanical design of laminar weak-link rotary mechanisms with ten-degree-level travel range and ten-nanoradian-level positioning resolution
patent, January 2012

XRF system having multiple excitation energy bands in highly aligned package
patent, October 2013

Robot-based automation system for cryogenic crystal sample mounting
patent, January 2007

Time-delayed beam splitting with energy separation of x-ray channels
journal, October 2013

Performance of a beam-multiplexing diamond crystal monochromator at the Linac Coherent Light Source
journal, June 2014

X-ray beam conditioning
patent, February 2016

High crystalline quality synthetic diamond
patent, September 2015

Redundantly constrained laminar structure as weak-link mechanisms
patent, January 2006

High pressure anvil and optical window
patent, April 2003

Anvils and ultra-high pressure apparatuses using the same
patent, November 2015

Tunable optical cavity for an x-ray free-electron-laser oscillator
journal, March 2009

Method and device for generating ultra-high pressure
patent, February 2008

High energy resolution, high angular acceptance crystal monochromator
patent, June 1996

Redundantly constrained laminar structure as weak-link mechanisms
patent, August 2003

Colorless single-crystal CVD diamond at rapid growth rate
patent, February 2011

Method for achieving high pressure using isotopically-pure diamond anvils
patent, March 1994

Energy storage arrangement
patent, May 1992

Method for manufacturing diamond monocrystal having a thin film, and diamond monocrystal having a thin film
patent, February 2012

Precision mechanical structure of an ultra-high-resolution spectrometer for inelastic X-ray scattering instrument
patent, April 2015

Energy storage arrangement
patent, September 2009

Tuning and synthesis of metallic nanostructures by mechanical compression
patent, November 2015

Demonstration of self-seeding in a hard-X-ray free-electron laser
journal, August 2012

System and method for producing synthetic diamond
patent, June 2003

Surface acoustic wave (SAW) devices based on cubic boron nitride/diamond composite structures
patent, August 2009

X-ray diffractometer having co-exiting stages optimized for single crystal and bulk diffraction
patent, December 2010

Fluorescent X-ray analysis apparatus
patent, April 2005

Sagittal focusing Laue monochromator
patent, March 2009

Highly aligned x-ray optic and source assembly for precision x-ray analysis applications
patent, June 2010

Mechanical design of deformation compensated flexural pivots structured for linear nanopositioning stages
patent, February 2015

Diamond-coated electrode and method for producing same
patent, January 2008

Diamond composite substrate and process for producing the same
patent, February 2011

Electronic device and method of use thereof
patent, July 2000

Monocrystalline diamond layer and method for the production thereof
patent, July 2008

X-ray monitoring optical elements
patent, December 2016

Diamond field emission tip and a method of formation
patent, September 2010

Chemically bonded diamond films and method for producing same
patent, April 1989

Tunable CVD diamond structures
patent, February 2005

Ultratough CVD single crystal diamond and three dimensional growth thereof
patent, September 2009

Diamond substrate and manufacturing method thereof
patent, June 2008

Optical contact micrometer
patent, August 2014

Method for making nanomaterials
patent, June 2013

Method and apparatus for making parallel X-ray beam and X-ray diffraction apparatus
patent, July 2005

Double bevel construction of a diamond anvil
patent, October 1988

Multidimensional alignment apparatus for hard x-ray focusing with two multilayer laue lenses
patent, October 2009

Target and X-ray generating tube including the same, X-ray generating apparatus, X-ray imaging system
patent, November 2016

BX90: A new diamond anvil cell design for X-ray diffraction and optical measurements
journal, December 2012

Design of a diamond-crystal monochromator for the LCLS hard x-ray self-seeding project
journal, March 2013

Diamond anvil cell and high-pressure physical investigations
journal, January 1983

Channel-cut monochromator
patent, June 2003

Method of growing diamond thin film
patent, December 2015

X-ray diffraction apparatus
patent, October 2004

Asymmetrical 4-crystal monochromator
patent, April 1996

Confinement of hydrogen at high pressure in carbon nanotubes
patent, December 2011