Method for sealing an oxygen transport membrane assembly
Abstract
An improved method of sealing a ceramic part to a solid part made of ceramic, metal, cermet or a ceramic coated metal is provided. The improved method includes placing a bond agent comprising an Al2O3 and SiO2 based glass-ceramic material and organic binder material on adjoining surfaces of the ceramic part and the solid part. The assembly is heated to a first target temperature that removes or dissolves the organic binder material from the bond agent and the assembly is subjected to a second induction heating step at a temperature ramp rate of between about 100.degree. C. and 200.degree. C. per minute to temperatures where the glass-ceramic material flows and wets the interface between adjoining surfaces. The assembly is rapidly cooled at a cooling rate of about 140.degree. C. per minute or more to induce nucleation and re-crystallization of the glass-ceramic material to form a dense, durable and gas-tight seal.
- Inventors:
- Issue Date:
- Research Org.:
- Praxair, Inc., Danbury, CT (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1438381
- Patent Number(s):
- 9969645
- Application Number:
- 14/134,276
- Assignee:
- Praxair Technology, Inc. (Danbury, CT)
- Patent Classifications (CPCs):
-
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
C - CHEMISTRY C03 - GLASS C03C - CHEMICAL COMPOSITION OF GLASSES, GLAZES, OR VITREOUS ENAMELS
- DOE Contract Number:
- FC26-07NT43088
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 2013 Dec 19
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE
Citation Formats
Gonzalez, Javier E., and Grant, Arthur F. Method for sealing an oxygen transport membrane assembly. United States: N. p., 2018.
Web.
Gonzalez, Javier E., & Grant, Arthur F. Method for sealing an oxygen transport membrane assembly. United States.
Gonzalez, Javier E., and Grant, Arthur F. Tue .
"Method for sealing an oxygen transport membrane assembly". United States. https://www.osti.gov/servlets/purl/1438381.
@article{osti_1438381,
title = {Method for sealing an oxygen transport membrane assembly},
author = {Gonzalez, Javier E. and Grant, Arthur F.},
abstractNote = {An improved method of sealing a ceramic part to a solid part made of ceramic, metal, cermet or a ceramic coated metal is provided. The improved method includes placing a bond agent comprising an Al2O3 and SiO2 based glass-ceramic material and organic binder material on adjoining surfaces of the ceramic part and the solid part. The assembly is heated to a first target temperature that removes or dissolves the organic binder material from the bond agent and the assembly is subjected to a second induction heating step at a temperature ramp rate of between about 100.degree. C. and 200.degree. C. per minute to temperatures where the glass-ceramic material flows and wets the interface between adjoining surfaces. The assembly is rapidly cooled at a cooling rate of about 140.degree. C. per minute or more to induce nucleation and re-crystallization of the glass-ceramic material to form a dense, durable and gas-tight seal.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2018},
month = {5}
}
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Method and apparatus for producing carbon dioxide
patent, March 2003
- Prasad, Ravi; Gottzmann, Christian Friedrich; Keskar, Nitin Ramesh
- US Patent Document 6,537,514