Zeolitic catalytic conversion of alcohols to hydrocarbons

Narula, Chaitanya K.; Davison, Brian H.; Keller, Martin

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Title: Zeolitic catalytic conversion of alcohols to hydrocarbons

Abstract

A method for converting an alcohol to a hydrocarbon, the method comprising contacting said alcohol with a metal-loaded zeolite catalyst at a temperature of at least 100.degree. C. and up to 550.degree. C., wherein said alcohol can be produced by a fermentation process, said metal is a positively-charged metal ion, and said metal-loaded zeolite catalyst is catalytically active for converting said alcohol to said hydrocarbon.

Inventors:: Narula, Chaitanya K.; Davison, Brian H.; Keller, Martin

Issue Date:: Tue Apr 10 00:00:00 EDT 2018

Research Org.:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1434702

Patent Number(s):: 9938467

Application Number:: 15/357,039

Assignee:: UT-BATTELLE, LLC (Oak Ridge, TN)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY

C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS

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B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2229/183 - in framework positions
B01J2229/186 - not in framework positions
B01J29/061 - {containing metallic elements added to the zeolite}
B01J29/072 - Iron group metals or copper
B01J29/076 - containing arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
B01J29/143 - {X-type faujasite}
B01J29/146 - {Y-type faujasite}
B01J29/163 - {X-type faujasite}
B01J29/166 - {Y-type faujasite}
B01J29/46 - Iron group metals or copper
B01J29/48 - containing arsenic, antimony, bismuth, vanadium, niobium tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
B01J29/68 - Iron group metals or copper
B01J29/69 - containing arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
B01J29/7615 - {Zeolite Beta}
B01J29/7661 - {MRE-type, e.g. ZSM-48}
B01J29/7669 - {MTW-type, e.g. ZSM-12, NU-13, TPZ-12 or Theta-3}
B01J29/7692 - {MTT-type, e.g. ZSM-23, KZ-1, ISI-4 or EU-13}
B01J29/7815 - {Zeolite Beta}
B01J29/7861 - {MRE-type, e.g. ZSM-48}
B01J29/7869 - {MTW-type, e.g. ZSM-12, NU-13, TPZ-12 or Theta-3}
B01J29/7892 - {MTT-type, e.g. ZSM-23, KZ-1, ISI-4 or EU-13}
B01J35/023 - {Catalysts characterised by dimensions, e.g. grain size}
B01J35/04 - Foraminous structures, sieves, grids, honeycombs
B01J37/0246 - {Coatings comprising a zeolite}

C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS
C07C1/22 - by reduction

C - CHEMISTRY C10 - PETROLEUM, GAS OR COKE INDUSTRIES C10G - CRACKING HYDROCARBON OILS
C10G2300/1011 - Biomass
C10G2300/1014 - of vegetal origin
C10G2300/4006 - Temperature
C10G2400/02 - Gasoline
C10G2400/04 - Diesel oil
C10G2400/08 - Jet fuel
C10G3/45 - {containing iron group metals or compounds thereof}
C10G3/49 - {containing crystalline aluminosilicates, e.g. molecular sieves}

C - CHEMISTRY C12 - BIOCHEMISTRY C12P - FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE {
C12P7/06 - Ethanol, i.e. non-beverage
C12P7/08 - produced as by-product or from waste or cellulosic material substrate
C12P7/10 - substrate containing cellulosic material
C12P7/16 - Butanols

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E50/10 - Biofuels

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02P - CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
Y02P30/20 - Bio-feedstock

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DOE Contract Number:: AC05-00OR22725

Resource Type:: Patent

Resource Relation:: Patent File Date: 2016 Nov 21

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

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                    Narula, Chaitanya K., Davison, Brian H., and Keller, Martin. Zeolitic catalytic conversion of alcohols to hydrocarbons.  United States: N. p., 2018. 
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                    Narula, Chaitanya K., Davison, Brian H., & Keller, Martin. Zeolitic catalytic conversion of alcohols to hydrocarbons.  United States.

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                    Narula, Chaitanya K., Davison, Brian H., and Keller, Martin. Tue .  
        "Zeolitic catalytic conversion of alcohols to hydrocarbons".  United States.  https://www.osti.gov/servlets/purl/1434702.

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@article{osti_1434702,

  title        = {Zeolitic catalytic conversion of alcohols to hydrocarbons},

  author       = {Narula, Chaitanya K. and Davison, Brian H. and Keller, Martin},

  abstractNote = {A method for converting an alcohol to a hydrocarbon, the method comprising contacting said alcohol with a metal-loaded zeolite catalyst at a temperature of at least 100.degree. C. and up to 550.degree. C., wherein said alcohol can be produced by a fermentation process, said metal is a positively-charged metal ion, and said metal-loaded zeolite catalyst is catalytically active for converting said alcohol to said hydrocarbon.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Apr 10 00:00:00 EDT 2018},

  month        = {Tue Apr 10 00:00:00 EDT 2018}

}

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Zeolitic catalytic conversion of alcohols to olefins

Patent Li, Zhenglong

A catalyst composition for converting an alcohol to olefins, the catalyst composition comprising the following components: (a) beta zeolite; (b) at least one element selected from the group consisting of zinc, magnesium, calcium, strontium, sodium, and potassium; and (c) at least one element selected from the group consisting of hafnium, yttrium, zirconium, tantalum, niobium, and tin; wherein the components (b) and (c) are independently within or on a surface of said beta zeolite. The catalyst may also further include component (d), which is copper or silver. Also described herein is a method for converting an alcohol to one or moremore » « less
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Zeolitic catalytic conversion of alochols to hydrocarbons

Patent Narula, Chaitanya K.; Davison, Brian H.; Keller, Martin

A method for converting an alcohol to a hydrocarbon, the method comprising contacting said alcohol with a metal-loaded zeolite catalyst at a temperature of at least 100.degree. C. and up to 550.degree. C., wherein said alcohol can be produced by a fermentation process, said metal is a positively-charged metal ion, and said metal-loaded zeolite catalyst is catalytically active for converting said alcohol to said hydrocarbon.
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Catalytic conversion of alcohols to hydrocarbons with low benzene content

Patent Narula, Chaitanya K.; Davison, Brian H.; Keller, Martin

A method for converting an alcohol to a hydrocarbon fraction having a lowered benzene content, the method comprising: converting said alcohol to a hydrocarbon fraction by contacting said alcohol, under conditions suitable for converting said alcohol to said hydrocarbon fraction, with a metal-loaded zeolite catalyst catalytically active for converting said alcohol to said hydrocarbon fraction, and contacting said hydrocarbon fraction with a benzene alkylation catalyst, under conditions suitable for alkylating benzene, to form alkylated benzene product in said hydrocarbon fraction. Also described is a catalyst composition useful in the method, comprising a mixture of (i) a metal-loaded zeolite catalyst catalyticallymore » « less
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Title: Zeolitic catalytic conversion of alcohols to hydrocarbons

Abstract

Citation Formats

Crystalline Zeolite ZSM-5 and Method of Preparing the Same patent, November 1972

Conversion of alcohols, mercaptans, sulfides, halides and/or amines patent, July 1975

Conversion of alcohols and ethers to hydrocarbons patent, August 1975

Production of gasoline hydrocarbons patent, December 1975

Conversion of methanol to gasoline components patent, January 1976

Conversion of alcohols and/or ethers to hydrocarbons patent, July 1976

Manufacture of gasoline patent, December 1976

Method for producing gasoline from methanol patent, December 1976

Manufacture of hydrocarbons patent, May 1977

Conversion of methanol to gasoline product patent, July 1977

Conversion of methanol to gasoline components patent, November 1977

Prolonging zeolite catalyst life in methanol conversion to gasoline by disposing of exothermic reaction heat patent, January 1978

Conversion of liquid alcohols and ethers with a fluid mass of ZSM-5 type catalyst patent, February 1979

Hydrocarbon manufacture from alcohols patent, April 1979

Hydrocarbon manufacture from alcohols patent, July 1981

Hydrocarbon cracking with mixture of zeolites Y and ZSM-5 patent, September 1981

Converting alcohols to hydrocarbons patent, July 1982

Conversion of methanol to gasoline patent, September 1983

Method for converting alcohols to hydrocarbons patent, December 1983

Activation of zeolites patent, January 1984

Production of light olefins patent, February 1985

Production of hydrocarbons with aluminophosphate molecular sieves patent, June 1985

Activation of zeolites patent, June 1986

Hydrocarbon conversion catalyst patent, August 1986

Hydrocarbon production patent, November 1986

Process for obtaining ethylene from ethanol patent, February 1988

System for conversion of methanol to gasoline patent, November 1988

Conversion of methanol to gasoline patent, November 1988

Catalytic aromatic saturation of hydrocarbons patent, July 1989

Catalysts for converting alcohols and/or aliphatic ether to unsaturated hydrocarbons and process for their production patent, August 1989

Conversion of alcohols to ether-rich gasoline patent, August 1991

Multireactor system for conversion of methanol to gasoline and distillate patent, September 1991

Integrated process for converting methanol to gasoline and distillates patent, January 1993

Benzene reduction in gasoline by alkylation with higher olefins patent, February 1996

Process for producing olefins and aromatics from non-aromatics patent, June 1998

Catalytic conversion of oxygenates to olefins patent, April 2000

Synthesis method of chemical industrial raw material and high-octane fuel, and high-octane fuel composition patent, November 2001

Catalyst for the conversion of low carbon number aliphatic hydrocarbons to higher carbon number hydrocarbons, process for preparing the catalyst and process using the catalyst patent, July 2002

Method for producing bio-fuel that integrates heat from carbon-carbon bond-forming reactions to drive biomass gasification reactions patent, January 2011

Reactive Distillation Process for the Alkylation of Aromatic Hydrocarbons patent-application, September 2003

Porous composite materials having micro and meso/macroporosity patent-application, April 2007

Processes for Converting Oxygenates to Olefins Using Aluminosilicate Catalysts patent-application, May 2008

Alkylaromatics Production patent-application, November 2008

Upper guide system for solenoid actuated fuel injectors patent-application, January 2010

Compositions and Methods for Fermentation of Biomass patent-application, October 2010

Ethanol producing process and apparatus patent-application, December 2010

Aviation-Grade Kerosene from Independently Produced Blendstocks patent-application, March 2011

Conversion Of Carbohydrates To Hydrocarbons patent-application, June 2011

Process to Make Olefins from Methanol and Isobutanol patent-application, August 2013

Zeolithic Catalytic Conversion of Alcohols to Hydrocarbons patent-application, April 2014

Process to Make Olefins from Isobutanol patent-application, May 2014

Synthesis of Drop-In Liquid Fuels and Chemicals from Methanol, Ethanol or Syngas Using Mixed Catalysts patent-application, June 2014

Catalytic Conversion of Alcohols Having at Least Three Carbon Atoms to Hydrocarbon Blendstock patent-application, January 2015

Conversion of ethanol over metal-exchanged zeolites journal, October 1993

Crystalline Zeolite ZSM-5 and Method of Preparing the Same
patent, November 1972

Conversion of alcohols, mercaptans, sulfides, halides and/or amines
patent, July 1975

Conversion of alcohols and ethers to hydrocarbons
patent, August 1975

Production of gasoline hydrocarbons
patent, December 1975

Conversion of methanol to gasoline components
patent, January 1976

Conversion of alcohols and/or ethers to hydrocarbons
patent, July 1976

Manufacture of gasoline
patent, December 1976

Method for producing gasoline from methanol
patent, December 1976

Manufacture of hydrocarbons
patent, May 1977

Conversion of methanol to gasoline product
patent, July 1977

Conversion of methanol to gasoline components
patent, November 1977

Prolonging zeolite catalyst life in methanol conversion to gasoline by disposing of exothermic reaction heat
patent, January 1978

Conversion of liquid alcohols and ethers with a fluid mass of ZSM-5 type catalyst
patent, February 1979

Hydrocarbon manufacture from alcohols
patent, April 1979

Hydrocarbon manufacture from alcohols
patent, July 1981

Hydrocarbon cracking with mixture of zeolites Y and ZSM-5
patent, September 1981

Converting alcohols to hydrocarbons
patent, July 1982

Conversion of methanol to gasoline
patent, September 1983

Method for converting alcohols to hydrocarbons
patent, December 1983

Activation of zeolites
patent, January 1984

Production of light olefins
patent, February 1985

Production of hydrocarbons with aluminophosphate molecular sieves
patent, June 1985

Activation of zeolites
patent, June 1986

Hydrocarbon conversion catalyst
patent, August 1986

Hydrocarbon production
patent, November 1986

Process for obtaining ethylene from ethanol
patent, February 1988

System for conversion of methanol to gasoline
patent, November 1988

Conversion of methanol to gasoline
patent, November 1988

Catalytic aromatic saturation of hydrocarbons
patent, July 1989

Catalysts for converting alcohols and/or aliphatic ether to unsaturated hydrocarbons and process for their production
patent, August 1989

Conversion of alcohols to ether-rich gasoline
patent, August 1991

Multireactor system for conversion of methanol to gasoline and distillate
patent, September 1991

Integrated process for converting methanol to gasoline and distillates
patent, January 1993

Benzene reduction in gasoline by alkylation with higher olefins
patent, February 1996

Process for producing olefins and aromatics from non-aromatics
patent, June 1998

Catalytic conversion of oxygenates to olefins
patent, April 2000

Synthesis method of chemical industrial raw material and high-octane fuel, and high-octane fuel composition
patent, November 2001

Catalyst for the conversion of low carbon number aliphatic hydrocarbons to higher carbon number hydrocarbons, process for preparing the catalyst and process using the catalyst
patent, July 2002

Method for producing bio-fuel that integrates heat from carbon-carbon bond-forming reactions to drive biomass gasification reactions
patent, January 2011

Reactive Distillation Process for the Alkylation of Aromatic Hydrocarbons
patent-application, September 2003

Porous composite materials having micro and meso/macroporosity
patent-application, April 2007

Processes for Converting Oxygenates to Olefins Using Aluminosilicate Catalysts
patent-application, May 2008

Alkylaromatics Production
patent-application, November 2008

Upper guide system for solenoid actuated fuel injectors
patent-application, January 2010

Compositions and Methods for Fermentation of Biomass
patent-application, October 2010

Ethanol producing process and apparatus
patent-application, December 2010

Aviation-Grade Kerosene from Independently Produced Blendstocks
patent-application, March 2011

Conversion Of Carbohydrates To Hydrocarbons
patent-application, June 2011

Process to Make Olefins from Methanol and Isobutanol
patent-application, August 2013

Zeolithic Catalytic Conversion of Alcohols to Hydrocarbons
patent-application, April 2014

Process to Make Olefins from Isobutanol
patent-application, May 2014

Synthesis of Drop-In Liquid Fuels and Chemicals from Methanol, Ethanol or Syngas Using Mixed Catalysts
patent-application, June 2014

Catalytic Conversion of Alcohols Having at Least Three Carbon Atoms to Hydrocarbon Blendstock
patent-application, January 2015

Conversion of ethanol over metal-exchanged zeolites
journal, October 1993