Controllable reductive method for synthesizing metal-containing particles

Moon, Ji-Won; Jung, Hyunsung; Phelps, Tommy Joe; Duty, Chad E.; Ivanov, Ilia N.; Joshi, Pooran Chandra; Jellison, Gerald Earle; Armstrong, Beth Louise; Smith, Sean Campbell; Rondinone, Adam Justin; Love, Lonnie J.

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Title: Controllable reductive method for synthesizing metal-containing particles

Abstract

The invention is directed to a method for producing metal-containing particles, the method comprising subjecting an aqueous solution comprising a metal salt, E.sub.h, lowering reducing agent, pH adjusting agent, and water to conditions that maintain the E.sub.h value of the solution within the bounds of an E.sub.h-pH stability field corresponding to the composition of the metal-containing particles to be produced, and producing said metal-containing particles in said aqueous solution at a selected E.sub.h value within the bounds of said E.sub.h-pH stability field. The invention is also directed to the resulting metal-containing particles as well as devices in which they are incorporated.

Inventors:: Moon, Ji-Won; Jung, Hyunsung; Phelps, Tommy Joe; Duty, Chad E.; Ivanov, Ilia N.; Joshi, Pooran Chandra; Jellison, Jr., Gerald Earle; Armstrong, Beth Louise; Smith, Sean Campbell; Rondinone, Adam Justin; Love, Lonnie J.

Issue Date:: 2018-03-06

Research Org.:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1425879

Patent Number(s):: 9909221

Application Number:: 14/205,589

Assignee:: UT-BATTELLE, LLC (Oak Ridge, TN)

Patent Classifications (CPCs):: C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25B - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS

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C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B19/007 - {Tellurides or selenides of metals

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25B - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS
C25B1/00 - Electrolytic production of inorganic compounds or non-metals
C25B1/21 - of manganese oxides

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DOE Contract Number:: AC05-00OR22725

Resource Type:: Patent

Resource Relation:: Patent File Date: 2014 Mar 12

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats


                    Moon, Ji-Won, Jung, Hyunsung, Phelps, Tommy Joe, Duty, Chad E., Ivanov, Ilia N., Joshi, Pooran Chandra, Jellison, Jr., Gerald Earle, Armstrong, Beth Louise, Smith, Sean Campbell, Rondinone, Adam Justin, and Love, Lonnie J. Controllable reductive method for synthesizing metal-containing particles.  United States: N. p., 2018. 
        Web.

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                    Moon, Ji-Won, Jung, Hyunsung, Phelps, Tommy Joe, Duty, Chad E., Ivanov, Ilia N., Joshi, Pooran Chandra, Jellison, Jr., Gerald Earle, Armstrong, Beth Louise, Smith, Sean Campbell, Rondinone, Adam Justin, & Love, Lonnie J. Controllable reductive method for synthesizing metal-containing particles.  United States.

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                    Moon, Ji-Won, Jung, Hyunsung, Phelps, Tommy Joe, Duty, Chad E., Ivanov, Ilia N., Joshi, Pooran Chandra, Jellison, Jr., Gerald Earle, Armstrong, Beth Louise, Smith, Sean Campbell, Rondinone, Adam Justin, and Love, Lonnie J. Tue .  
        "Controllable reductive method for synthesizing metal-containing particles".  United States.  https://www.osti.gov/servlets/purl/1425879.

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@article{osti_1425879,

  title        = {Controllable reductive method for synthesizing metal-containing particles},

  author       = {Moon, Ji-Won and Jung, Hyunsung and Phelps, Tommy Joe and Duty, Chad E. and Ivanov, Ilia N. and Joshi, Pooran Chandra and Jellison, Jr., Gerald Earle and Armstrong, Beth Louise and Smith, Sean Campbell and Rondinone, Adam Justin and Love, Lonnie J.},

  abstractNote = {The invention is directed to a method for producing metal-containing particles, the method comprising subjecting an aqueous solution comprising a metal salt, E.sub.h, lowering reducing agent, pH adjusting agent, and water to conditions that maintain the E.sub.h value of the solution within the bounds of an E.sub.h-pH stability field corresponding to the composition of the metal-containing particles to be produced, and producing said metal-containing particles in said aqueous solution at a selected E.sub.h value within the bounds of said E.sub.h-pH stability field. The invention is also directed to the resulting metal-containing particles as well as devices in which they are incorporated.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2018},

  month        = {3}

}

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Works referenced in this record:

Mixed oxide nanoparticles and method of making
patent, September 2002

Lauf, Robert J.; Phelps, Tommy J.; Zhang, Chuanlun
US Patent Document 6,444,453
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6444453

Fermentative process for making inorganic nanoparticles
patent, June 2006

Phelps, Tommy J.; Lauf, Robert J.; Moon, Ji-won
US Patent Document 7,060,473
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7060473

Method of producing prussian blue-type metal complex nanoparticles, and prussian blue-type metal complex nanoparticles obtained by the method, dispersion of the nanoparticles, method of regulating the color of the nanoparticles, and electrode and transmitted light-regulator each using the nanoparticles
patent, January 2013

Kawamoto, Tohru; Tanaka, Hisashi; Hara, Shigeo
US Patent Document 8,349,221
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8349221

Microbially-mediated method for synthesis of non-oxide semiconductor nanoparticles
patent, June 2014

Phelps, Tommy J.; Lauf, Robert J.; Moon, Ji-won
US Patent Document 8,759,053
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8759053

Microbial-mediated method for metal oxide nanoparticle formation
patent, September 2015

Rondinone, Adam J.; Moon, Ji-won; Love, Lonnie J.
US Patent Document 9,127,295
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/9127295

Mixed oxide nanoparticles and apparatus for making same
patent-application, December 2002

Lauf, Robert; Phelps, Tommy; Zhang, Chuanlun
US Patent Application 10/174184; 20020187889
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20020187889

Metal oxide processing methods and systems
patent-application, April 2005

Boren, Richard M.; Hammel, Charles F.
US Patent Application 10/902439; 20050074380
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20050074380

Process for the recovery of value metals from base metal sulfide ores
patent-application, January 2009

Harris, G. Bryn; Lakshmanan, Vaikuntam I.; Sridhar, Ramamritham
US Patent Application 12/216940; 20090013829
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20090013829

Process for Recovering Titanium Dioxide
patent-application, April 2010

Cooke, Graham; Jha, Animesh; Lahiri, Abhishek
US Patent Application 12/561855; 20100086454
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20100086454

Microbial-mediated method for metal oxide nanoparticle formation
patent-application, July 2010

Rondinone, Adam; Moon, Ji; Love, Lonnie
US Patent Application 12/357523; 20100184179
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20100184179

Microbially-mediated method for synthesis of non-oxide semiconductor nanoparticles
patent-application, December 2010

Phelps, Tommy; Lauf, Robert; Moon, Ji
US Patent Application 12/874522; 20100330367
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20100330367

Direct Leaching of sulfides: Chemistry and applications
journal, December 1976

Peters, Ernest
Metallurgical Transactions B, Vol. 7, Issue 4, p. 505-517
https://doi.org/10.1007/BF02698582

Precipitation of Sulfides form Homogeneous Solutions by Thioacetamide
journal, February 1956

Swift, E. H.; Butler, E. A.
Analytical Chemistry, Vol. 28, Issue 2, p. 146-153
https://doi.org/10.1021/ac60110a001

Particulate pyrite formation by the reaction in aqueous solutions: effects of solution composition
journal, November 1996

Wei, Dawei; Osseo-Asare, K.
Colloids and Surfaces A: Physicochemical and Engineering Aspects, Vol. 118, Issue 1-2, p. 51-61
https://doi.org/10.1016/0927-7757(96)03568-6

Biosynthesis of cadmium sulphide quantum semiconductor crystallites
journal, April 1989

Dameron, C. T.; Reese, R. N.; Mehra, R. K.
Nature, Vol. 338, Issue 6216, p. 596-597
https://doi.org/10.1038/338596a0

Synthesis, Characterization, and Spectroscopic Properties of ZnO Nanoparticles
journal, January 2012

Talam, Satyanarayana; Karumuri, Srinivasa Rao; Gunnam, Nagarjuna
ISRN Nanotechnology, Vol. 2012, p. 1-6
https://doi.org/10.5402/2012/372505

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Similar Records

Title: Controllable reductive method for synthesizing metal-containing particles

Abstract

Citation Formats

Mixed oxide nanoparticles and method of making patent, September 2002

Fermentative process for making inorganic nanoparticles patent, June 2006

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Microbial-mediated method for metal oxide nanoparticle formation patent-application, July 2010

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Direct Leaching of sulfides: Chemistry and applications journal, December 1976

Precipitation of Sulfides form Homogeneous Solutions by Thioacetamide journal, February 1956

Particulate pyrite formation by the reaction in aqueous solutions: effects of solution composition journal, November 1996

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Synthesis, Characterization, and Spectroscopic Properties of ZnO Nanoparticles journal, January 2012

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Microbially-mediated method for synthesis of non-oxide semiconductor nanoparticles
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patent-application, April 2005

Process for the recovery of value metals from base metal sulfide ores
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patent-application, April 2010

Microbial-mediated method for metal oxide nanoparticle formation
patent-application, July 2010

Microbially-mediated method for synthesis of non-oxide semiconductor nanoparticles
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Direct Leaching of sulfides: Chemistry and applications
journal, December 1976

Precipitation of Sulfides form Homogeneous Solutions by Thioacetamide
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Particulate pyrite formation by the reaction in aqueous solutions: effects of solution composition
journal, November 1996

Biosynthesis of cadmium sulphide quantum semiconductor crystallites
journal, April 1989

Synthesis, Characterization, and Spectroscopic Properties of ZnO Nanoparticles
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