Methods for controlling pore morphology in aerogels using electric fields and products thereof
Abstract
In one embodiment, an aerogel or xerogel includes column structures of a material having minor pores therein and major pores devoid of the material positioned between the column structures, where longitudinal axes of the major pores are substantially parallel to one another. In another embodiment, a method includes heating a sol including aerogel or xerogel precursor materials to cause gelation thereof to form an aerogel or xerogel and exposing the heated sol to an electric field, wherein the electric field causes orientation of a microstructure of the sol during gelation, which is retained by the aerogel or xerogel. In one approach, an aerogel has elongated pores extending between a material arranged in column structures having structural characteristics of being formed from a sol exposed to an electric field that causes orientation of a microstructure of the sol during gelation which is retained by the elongated pores of the aerogel.
- Inventors:
- Issue Date:
- Research Org.:
- Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1414912
- Patent Number(s):
- 9852824
- Application Number:
- 13/180,440
- Assignee:
- Lawrence Livermore National Security, LLC (Livermore, CA)
- Patent Classifications (CPCs):
-
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01B - CABLES
- DOE Contract Number:
- AC52-07NA27344
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 2011 Jul 11
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Worsley, Marcus A., Baumann, Theodore F., Satcher, Jr., Joe H., Olson, Tammy Y., Kuntz, Joshua D., and Rose, Klint A. Methods for controlling pore morphology in aerogels using electric fields and products thereof. United States: N. p., 2017.
Web.
Worsley, Marcus A., Baumann, Theodore F., Satcher, Jr., Joe H., Olson, Tammy Y., Kuntz, Joshua D., & Rose, Klint A. Methods for controlling pore morphology in aerogels using electric fields and products thereof. United States.
Worsley, Marcus A., Baumann, Theodore F., Satcher, Jr., Joe H., Olson, Tammy Y., Kuntz, Joshua D., and Rose, Klint A. Sat .
"Methods for controlling pore morphology in aerogels using electric fields and products thereof". United States. https://www.osti.gov/servlets/purl/1414912.
@article{osti_1414912,
title = {Methods for controlling pore morphology in aerogels using electric fields and products thereof},
author = {Worsley, Marcus A. and Baumann, Theodore F. and Satcher, Jr., Joe H. and Olson, Tammy Y. and Kuntz, Joshua D. and Rose, Klint A.},
abstractNote = {In one embodiment, an aerogel or xerogel includes column structures of a material having minor pores therein and major pores devoid of the material positioned between the column structures, where longitudinal axes of the major pores are substantially parallel to one another. In another embodiment, a method includes heating a sol including aerogel or xerogel precursor materials to cause gelation thereof to form an aerogel or xerogel and exposing the heated sol to an electric field, wherein the electric field causes orientation of a microstructure of the sol during gelation, which is retained by the aerogel or xerogel. In one approach, an aerogel has elongated pores extending between a material arranged in column structures having structural characteristics of being formed from a sol exposed to an electric field that causes orientation of a microstructure of the sol during gelation which is retained by the elongated pores of the aerogel.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2017},
month = {12}
}
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- Wolff, Matthias; Braun, Adelina; Bartscherer, Erik
- 27th Annual Cocoa Beach Conference on Advanced Ceramics and Composites: A: Ceramic Engineering and Science Proceedings, Vol. 24, Issue 3
3-D micro-ceramic components from hydrothermally processed carbon nanotube–boehmite powders by electrophoretic deposition
journal, July 2010
- Zaman, Ali Can; Üstündağ, Cem B.; Kuşkonmaz, Nilgün
- Ceramics International, Vol. 36, Issue 5, p. 1703-1710
Orientation and Dynamics of ZnO Nanorod Liquid Crystals in Electric Fields
journal, May 2010
- Zorn, Matthias; Tahir, Muhammad Nawaz; Bergmann, Björn
- Macromolecular Rapid Communications, Vol. 31, Issue 12, p. 1101-1107