Production of nanocrystalline metal powders via combustion reaction synthesis

Frye, John G.; Weil, Kenneth Scott; Lavender, Curt A.; Kim, Jin Yong

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Title: Production of nanocrystalline metal powders via combustion reaction synthesis

Abstract

Nanocrystalline metal powders comprising tungsten, molybdenum, rhenium and/or niobium can be synthesized using a combustion reaction. Methods for synthesizing the nanocrystalline metal powders are characterized by forming a combustion synthesis solution by dissolving in water an oxidizer, a fuel, and a base-soluble, ammonium precursor of tungsten, molybdenum, rhenium, or niobium in amounts that yield a stoichiometric burn when combusted. The combustion synthesis solution is then heated to a temperature sufficient to substantially remove water and to initiate a self-sustaining combustion reaction. The resulting powder can be subsequently reduced to metal form by heating in a reducing gas environment.

Inventors:: Frye, John G.; Weil, Kenneth Scott; Lavender, Curt A.; Kim, Jin Yong

Issue Date:: Tue Oct 31 00:00:00 EDT 2017

Research Org.:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1406578

Patent Number(s):: 9802834

Application Number:: 12/700,923

Assignee:: Battelle Memorial Institute

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

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B - PERFORMING OPERATIONS B22 - CASTING B22F - WORKING METALLIC POWDER
B22F2301/20 - Refractory metals
B22F9/24 - starting from liquid metal compounds, e.g. solutions

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B21/38 - Nitric acid

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01G - COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
C01G33/00 - Compounds of niobium
C01G39/02 - Oxides
C01G41/02 - Oxides
C01G47/00 - Compounds of rhenium

C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS
C07C229/06 - having only one amino and one carboxyl group bound to the carbon skeleton

C - CHEMISTRY C22 - METALLURGY C22B - PRODUCTION AND REFINING OF METALS
C22B34/24 - Obtaining niobium or tantalum

C - CHEMISTRY C22 - METALLURGY C22C - ALLOYS
C22C1/045 - {Alloys based on refractory metals}
C22C1/058 - {by reaction sintering
C22C27/00 - Alloys based on rhenium or a refractory metal not mentioned in groups C22C14/00 or C22C16/00
C22C27/02 - Alloys based on vanadium, niobium, or tantalum
C22C27/04 - Alloys based on tungsten or molybdenum

G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N23/20075 - {by measuring interferences of X-rays, e.g. Borrmann effect}

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DOE Contract Number:: AC05-76RL01830

Resource Type:: Patent

Resource Relation:: Patent File Date: 2010 Feb 05

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats


                    Frye, John G., Weil, Kenneth Scott, Lavender, Curt A., and Kim, Jin Yong. Production of nanocrystalline metal powders via combustion reaction synthesis.  United States: N. p., 2017. 
        Web.

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                    Frye, John G., Weil, Kenneth Scott, Lavender, Curt A., & Kim, Jin Yong. Production of nanocrystalline metal powders via combustion reaction synthesis.  United States.

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                    Frye, John G., Weil, Kenneth Scott, Lavender, Curt A., and Kim, Jin Yong. Tue .  
        "Production of nanocrystalline metal powders via combustion reaction synthesis".  United States.  https://www.osti.gov/servlets/purl/1406578.

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@article{osti_1406578,

  title        = {Production of nanocrystalline metal powders via combustion reaction synthesis},

  author       = {Frye, John G. and Weil, Kenneth Scott and Lavender, Curt A. and Kim, Jin Yong},

  abstractNote = {Nanocrystalline metal powders comprising tungsten, molybdenum, rhenium and/or niobium can be synthesized using a combustion reaction. Methods for synthesizing the nanocrystalline metal powders are characterized by forming a combustion synthesis solution by dissolving in water an oxidizer, a fuel, and a base-soluble, ammonium precursor of tungsten, molybdenum, rhenium, or niobium in amounts that yield a stoichiometric burn when combusted. The combustion synthesis solution is then heated to a temperature sufficient to substantially remove water and to initiate a self-sustaining combustion reaction. The resulting powder can be subsequently reduced to metal form by heating in a reducing gas environment.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Oct 31 00:00:00 EDT 2017},

  month        = {Tue Oct 31 00:00:00 EDT 2017}

}

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Works referenced in this record:

Method of Preparing Lead and Alkaline Earth Titanates and Niobates and Coating Method Using the Same to Form a Capacitor
patent, July 1967

Pechini, Maggio P.
US Patent Document 3,330,697
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/3330697

Ceramic precursor mixture and technique for converting the same to ceramic
patent, October 1991

Aksay, Ilhan A.; Han, Chan; Maupin, Gary D.
US Patent Document 5,061,682
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5061682

Method of making metal oxide ceramic powders by using a combustible amino acid compound
patent, May 1992

Pederson, Larry R.; Chick, Lawrence A.; Exarhos, Gregory J.
US Patent Document 5,114,702
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5114702

Process for making ultra-fine ceramic particles
patent, November 1995

Stangle, Gregory C.; Venkatachari, Koththavasal R.; Ostrander, Steven P.
US Patent Document 5,468,427
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5468427

Combustion of emulsions: A method and process for producing fine powders
patent, November 1999

Bickmore, Clint; Galde, Benjamin; Yadav, Tapesh
US Patent Document 5,984,997
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5984997

Crystalline multinary metal oxide compositions, process for preparing and processes for using the composition
patent, January 2001

Bedard, Robert L.; Bogdan, Paula L.; King, Lisa M.
US Patent Document 6,171,571
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6171571

Solution method for making molybdate and tungstate negative thermal expansion materials and compounds made by the method
patent, February 2001

Sleight, Arthur W.; Closmann, Claire E.; Haygarth, John C.
US Patent Document 6,183,716
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6183716

Single step process for the synthesis of nanoparticles of ceramic oxide powders
patent, December 2004

James, Jose; Jose, Rajan; John, Asha Mary
US Patent Document 6,835,367
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6835367

Plasma arc reactor for the production of fine powders
patent, April 2006

Deegan, David; Chapman, Chris; Johnson, Timothy P.
US Patent Document 7,022,155
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7022155

Apparatus and method for friction stir welding of high strength materials, and articles made therefrom
patent, April 2006

Subramanian, Pazhayannur Ramanathan; Bewlay, Bernard Patrick; Helder, Earl Claude
US Patent Document 7,032,800
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7032800

Apparatus and method for friction stir welding of high strength materials, and articles made therefrom
patent, March 2008

Subramanian, Pazhayannur Ramanathan; Bewlay, Bernard Patrick; Helder, Earl Claude
US Patent Document 7,337,940
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7337940

Scintillator nanoparticles and method of making
patent, November 2008

Krishna, Kalaga Murali; Loureiro, Sergio Paulo Martins; Manoharan, Mohan
US Patent Document 7,449,128
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7449128

Tungsten rhenium compounds and composites and methods for forming the same
patent, January 2013

Liu, Qingyuan; Steel, Russell J.; Packer, Scott M.
US Patent Document 8,361,178
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8361178

Preparation of tungsten oxide
patent-application, February 2005

Bulian, Christopher J.; Dye, Robert C.; Son, Steven F.
US Patent Document 10/629489; 20050025700
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20050025700

Tungsten alloy high temperature tool materials
patent-application, June 2005

Ohriner, Evan K.; David, Stan A.
US Patent Document 10/735974; 20050129565
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20050129565

Process for plasma synthesis of rhenium nano and micro powders, and for coatings and near net shape deposits thereof and apparatus therefor
patent-application, September 2005

Jurewicz, Jerzy W.; Guo, Jiayin
US Patent Document 11/041870; 20050211018
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20050211018

Method of Making Nanocrystalline Tungsten Powder
patent-application, September 2008

Lunk, Hans-Joachim; Stevens, Henry J.
US Patent Document 12/036507; 20080223175
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20080223175

High strength and toughness steel structures by friction stir welding
patent-application, June 2010

Ayer, Raghavan; Fairchild, Douglas Paul; Ford, Steven Jeffrey
US Patent Document 12/590956; 20100136369
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20100136369

Refractory Metal Tool for Friction Stir Welding Comprising a Shoulder Made of Tungsten, Molybdenum, Tantalum, Niobium, or Hafnium Alloy and a Coated or Treated Surface
patent-application, November 2010

Rowe, Charles E. D.; Tuck, Jonathan R.; Staines, David George
US Patent Document 12/377702; 20100279146
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20100279146