High energy density redox flow device

Title: High energy density redox flow device

Redox flow devices are described in which at least one of the positive electrode or negative electrode-active materials is a semi-solid or is a condensed ion-storing electroactive material, and in which at least one of the electrode-active materials is transported to and from an assembly at which the electrochemical reaction occurs, producing electrical energy. The electronic conductivity of the semi-solid is increased by the addition of conductive particles to suspensions and/or via the surface modification of the solid in semi-solids (e.g., by coating the solid with a more electron conductive coating material to increase the power of the device). High energy density and high power redox flow devices are disclosed. The redox flow devices described herein can also include one or more inventive design features. In addition, inventive chemistries for use in redox flow devices are also described.

Inventors:: Chiang, Yet-Ming; Carter, Craig W.; Ho, Bryan Y.; Duduta, Mihai; Limthongkul, Pimpa

Issue Date:: 2017-10-10

OSTI Identifier:: 1398970

Assignee:: Massachusetts Institute of Technology NETL

Patent Number(s):: 9,786,944

Application Number:: 12/970,753

Contract Number:: FC26-05NT42403

Resource Relation:: Patent File Date: 2010 Dec 16

Research Org:: Massachusetts Institute of Technology, Cambridge, MA (United States)

Sponsoring Org:: USDOE

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

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Fuel cell with proton conducting membrane
patent, December 2002

Peled, Emanuel; Duvdevani, Tair; Melman, Avi
US Patent Document 6,492,047
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A system for generating and consuming borohydride ions comprising two electrochemical cells. At least one of the cells is configured for installation on a vehicle that is propelled by electricity
patent, December 2002

Amendola, Steven
US Patent Document 6,497,973
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Thin lithium battery with slurry cathode
patent, April 2003

Moutsios, George W.; Xing, Xuekun; Nardi, Jay
US Patent Document 6,551,745
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Membrane-separated, bipolar multicell electrochemical reactor
patent, April 2003

Broman, Barry; Zocchi, Andrea
US Patent Document 6,555,267
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Stabilized vanadium electrolyte solutions for all-vanadium redox cells and batteries
patent, May 2003

Kazacos, Maria Skyllas; Kazacos, Michael
US Patent Document 6,562,514
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Battery and equipment or device having the battery as part of structure and locally distributed power generation method and power generation device therefor
patent, February 2004

Tsutsumi, Kazuo; Atsuta, Toshio; Kumagai, Chikanori
US Patent Document 6,689,507
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Redox gel battery
patent, April 2004

Holtom, Stephen Wayne; Menictas, Chris
US Patent Document 6,720,107
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Redox flow battery
patent, July 2004

Sekiguchi, Sumie; Furusato, Kouichi; Miyabayashi, Mitsutaka
US Patent Document 6,764,789
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Ion conductive matrixes and their use
patent, November 2004

Peled, Emanuel; Duvdevani, Tair; Melman, Avi
US Patent Document 6,811,911
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Colloidal battery
patent, December 2005

Phillips, Edward D.
US Patent Document 6,979,512
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Battery with bifunctional electrolyte
patent, January 2006

Clarke, Robert Lewis; Dougherty, Brian J.; Harrison, Stephen
US Patent Document 6,986,966
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Electric devices with improved bipolar electrode
patent, April 2006

Clarke, Robert Lewis; Dougherty, Brian J.; Harrison, Stephen
US Patent Document 7,033,696
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High energy density vanadium electrolyte solutions, methods of preparation thereof and all-vanadium redox cells and batteries containing high energy vanadium electrolyte solutions
patent, July 2006

Kazacos, Michael; Kazacos, Maria Skyllas
US Patent Document 7,078,123
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Secondary battery with autolytic dendrites
patent, May 2007

Clarke, Robert Lewis; Dougherty, Brian; Harrison, Stephen
US Patent Document 7,214,443
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Lanthanide batteries
patent, August 2007

Clarke, Robert; Dougherty, Brian; Harrison, Stephen
US Patent Document 7,252,905
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Load leveling battery and methods therefor
patent, September 2007

Clarke, Robert Lewis; Dougherty, Brian; Harrison, Stephen
US Patent Document 7,270,911
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Battery with gelled electrolyte
patent, November 2007

Clarke, Robert; Dougherty, Brian; Harrison, Stephen
US Patent Document 7,297,437
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Vanadium/polyhalide redox flow battery
patent, January 2008

Skyllas-Kazacos, Maria
US Patent Document 7,320,844
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Conductive lithium storage electrode
patent, March 2008

Chiang, Yet-Ming; Chung, Sung-Yoon; Bloking, Jason T.
US Patent Document 7,338,734
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Catalytic converter system for diesel engines
patent, August 2008

Newburry, Donald M.; Clary, William B.
US Patent Document 7,412,824
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High efficiency semi-fuel cell incorporating an ion exchange membrane
patent, April 2009

Medeiros, Maria G.; Dow, Eric G.; Bessette, Russell R.
US Patent Document 7,521,149
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Mixed electrolyte battery
patent, July 2009

Clarke, Robert Lewis; Dougherty, Brian; Harrison, Stephen
US Patent Document 7,560,189
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Cerium batteries
patent, December 2009

Clarke, Robert Lewis; Dougherty, Brian; Harrison, Stephen
US Patent Document 7,625,663
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Electroactive material for charge transport
patent, January 2012

Reynolds, Thomas A.
US Patent Document 8,097,364
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Fluidic distribution system and related methods
patent, March 2012

McLean, Gerard F.; Zimmermann, Joerg; Schrooten, Jeremy
US Patent Document 8,133,629
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Perfluorinated membranes and improved electrolytes for redox cells and batteries
patent, September 2013

Kazacos, George Christopher; Kazacos, Nicholas Michael
US Patent Document 8,541,138
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High energy density redox flow device
patent, May 2014

Chiang, Yet-Ming; Carter, William Craig; Duduta, Mihai
US Patent Document 8,722,226
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High energy density redox flow device
patent, May 2014

Chiang, Yet-Ming; Carter, W. Craig; Ho, Bryan Y.
US Patent Document 8,722,227
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Fuel system using redox flow battery
patent, July 2014

Chiang, Yet-Ming; Bazzarella, Ricardo
US Patent Document 8,778,552
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High energy density redox flow device
patent, October 2015

Chiang, Yet-Ming; Carter, W. Craig; Duduta, Mihai
US Patent Document 9,153,833
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Fuel system using redox flow battery
patent, March 2016

Chiang, Yet-Ming; Bazzarella, Ricardo
US Patent Document 9,293,781
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High Energy Density Vanadium Electrolyte Solutions, Methods of Preparation Thereof and All-Vanadium Redox Cells and Batteries Containing High Energy Vanadium Electrolyte Solutions
patent-application, October 2001

Kazacos, Michael; Kazacos, Maria Skyllas
US Patent Application 08/945869; 20010028977
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Four-way valve for battery circulation system
patent-application, December 2001

Eidler, Phillip A.; Lex, Peter J.; Rixford, Robert R.
US Patent Application 09/834673; 20010055713
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Pressurre fluctuation prevention tank structure, electrolyte circulation type secondary battery, and redox flow type secondary battery
patent-application, January 2003

Ito, Takefumi; Tokuda, Nobuyuki
US Patent Application 10/220023; 20030022059
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Enzymatic fuel cell
patent-application, February 2003

Liberatore, Michael James; Hozer, Leszek; Sreeram, Attiganal Narayanaswamy
US Patent Application 10/226841; 20030039868
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Fuel cell with proton conducting membrane
patent-application, May 2003

Peled, Emanuel; Duvdevani, Tair; Melman, Avi
US Patent Application \t10/181061; 20030091883
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Kazacos, Michael; Kazacos, Maria Skyllas
US Patent Document 10/226751; 20030143456
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Fuel-cell based power source having internal series redundancy
patent-application, November 2003

Holmes, Charles M.; Sundar, Rajagopalan; Vail, Kenneth Dean
US Patent Application 10/141631; 20030211377
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Regenerative fuel cell with ph control
patent-application, August 2004

Morrisey, Patrick John; Ward, Norman John
US Patent Application 10/475139; 20040151977
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Electrolyte for redox flow battery, and redox flow battery
patent-application, September 2004

Kubata, Michiru; Nakaishi, Hiroyuki
US Patent Application 10/479710; 20040191623
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Fuel cell with proton conducting membrane and with improved water and fuel management
patent-application, October 2004

Peled, Emanuel; Duvdevani, Tair; Blum, Arnon
US Patent Application 10/483340; 20040209153
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Vanadium/polyhalide redox flow battery
patent-application, November 2004

Skyllas-Kazacos, Maria
US Patent Application 10/487135; 20040234843
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Vanadium redox battery electrolyte
patent-application, December 2004

Skyllas-Kazacos, Maria
US Patent Application \t10/477017; 20040241552
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Basic cell for fuel cell with helical structure, production method thereof and fuel cell comprising numerous basic cells
patent-application, March 2005

Tiquet, Pascal; Marsacq, Didier
US Patent Application 10/484041; 20050069752
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Battery
patent-application, August 2005

Tsutsumi, Kazuo; Kumagai, Chikanori; Tsutsumi, Atsushi
US Patent Application 10/510416; 20050175890
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Metal halide redox flow battery
patent-application, November 2005

Skyllas-Kazacos, Maria; Kazacos, Michael; Mousa, Asem
US Patent Document 10/512417; 20050244707
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Electrolytic process and apparatus
patent-application, November 2005

DiMascio, Felice
US Patent Application 10/514175; 20050252786
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Thin-film cathode for 3-dimensional microbattery and method for preparing such cathode
patent-application, February 2006

Nathan, Menachem; Peled, Emanuel; Golodnitsky, Diana
US Patent Application 10/531529; 20060032046
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Battery with bifunctional electrolyte
patent-application, March 2006

Clarke, Robert Lewis; Dougherty, Brian J.; Harrison, Stephen
US Patent Application 11/248638; 20060063065
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Novel vanadium halide redox flow battery
patent-application, August 2006

Kazacos, Michael; Skyllas-Kazacos, Maria; Kazacos, Nicholasl
US Patent Document 10/548555; 20060183016
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Intercalation anode protection for cells with dissolved lithium polysulfides
patent-application, August 2006

De Jonghe, Lutgard C.; Nimon, Yevgeniy S.; Visco, Steven J.
US Patent Application 11/354223; 20060194115
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Organic fuel cell methods and apparatus
patent-application, September 2006

Surampudi, Subbarao; Narayanan, Sekharipuram R.; Vamos, Eugene
US Patent Application \t11/418976; 20060204810
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Multiple metal oxide submicron particles
patent-application, June 2008

Kumar, Sujeet; Reitz, Hariklia; Home, Craig
US Patent Application 12/009184; 20080131357
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Electrolytic Method To Make Alkali Alcoholates Using Ion Conducting Alkali Electrolyte/Seperator
patent-application, June 2008

Joshi, Ashok; Balagopal, Shekar; Pendelton, Justin
US Patent Application 11/611054; 20080142373
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Fuel cell with proton conducting membrane
patent-application, October 2008

Peled, Emanuel; Duvdevani, Tair; Melman, Avi
US Patent Application \t12/081362; 20080241629
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Perfluorinated Membranes and Improved Electrolytes for Redox Cells and Batteries
patent-application, November 2008

Kazacos, George Christopher; Kazacos, Nicholas Michael
US Patent Document 11/917989; 20080292964
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Secondary Battery, Power Supply System Using Same and Usage of Power Supply System
patent-application, January 2009

Inatomi, Yuu; Hojo, Nobuhiko; Kuranuki, Masaaki
US Patent Application 11/915456; 20090017379
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Shut-Off Valve Having Two Valve Seats Providing Pressure Equalization
patent-application, February 2009

Pechtold, Rainer
US Patent Application 12/200006; 20090032754
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Electrochemical Cell Having a Coiled Core
patent-application, June 2009

Zhou, Xiankai; Han, Lei; Gu, Hongjuan
US Patent Application 12/341787; 20090159347
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Sodium ion based aqueous electrolyte electrochemical secondary energy storage device
patent-application, October 2009

Whitacre, Jay
US Patent Application 12/385277; 20090253025
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High Energy Density Redox Flow Device
patent-application, February 2010

Chiang, Yet-Ming; Carter, W. Craig; Ho, Bryan H.
US Patent Document 12/484113; 20100047671
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Hybrid Electrochemical Generator with a Soluble Anode
patent-application, June 2010

Yazami, Rachid
US Patent Application 12/612409; 20100141211
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Electrochemical Energy Storage Device Having a Reservoir for an Additive
patent-application, July 2010

Wahl, Florian; Koenigsmann, Martin Holger
US Patent Application 12/451306; 20100190042
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Method of Creating Particle Size Distribution Model, Method of Predicting Degradation of Fuel Cell Catalyst Using the Method of Creating Particle Size Distribution Model, and Method of Controlling Fuel Cell Using the Method of Predicting Degradation of Fuel Cell Catalyst
patent-application, September 2010

Kimura, Hiroko; Takehiro, Naoki; Kato, Manabu
US Patent Application 12/751318; 20100248046
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Fuel System Using Redox Flow Battery
patent-application, December 2010

Chiang, Yet-Ming; Bazzarella, Ricardo
US Patent Document 12/755379; 20100323264
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High Energy Density Redox Flow Device
patent-application, August 2011

Carter, William; Chiang, Yet-Ming; Duduta, Mihai
US Patent Application 12/970773; 20110189520
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Energy Transfer Using Electrochemically Isolated Fluids
patent-application, November 2011

Duduta, Mihai; Carter, W. Craig; Chiang, Yet-Ming
US Patent Document 13/083167; 20110274948
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Galvanic Electrochemical Cells Utilizing Taylor Vortex Flows
patent-application, January 2012

Fischel, Halbert
US Patent Application 13/235480; 20120003518
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Stationary, Fluid Redox Electrode
patent-application, June 2012

Chiang, Yet-Ming; Carter, W. Craig; Duduta, Mihai
US Patent Document 13/212607; 20120164499
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High Energy Density Redox Flow Device
patent-application, June 2014

Carter, W. Craig; Chiang, Yet-Ming; Duduta, Mihai
US Patent Application 14/002304; 20140154546
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High Energy Density Redox Flow Device
patent-application, September 2014

Chiang, Yet-Ming; Carter, W. Craig; Duduta, Mihai
US Patent Document 14/276723; 20140248521
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Fuel System Using Redox Flow Battery
patent-application, May 2015

Chiang, Yet-Ming; Bazzarella, Ricardo
US Patent Application 14/306610; 20150129081
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Fuel System Using Redox Flow Battery
patent-application, January 2016

Chiang, Yet-Ming; Bazzarella, Ricardo
US Patent Document 14/824664; 20160013507
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High Energy Density Redox Flow Device
patent-application, July 2016

Chiang, Yet-Ming; Carter, W. Craig; Duduta, Mihai
US Patent Document 14/840810; 20160218375
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Fuel System Using Redox Flow Battery
patent-application, September 2016

Chiang, Yet-Ming; Bazzarella, Ricardo
US Patent Document 15/045718; 20160268621
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Conjugated dicarboxylate anodes for Li-ion batteries
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Armand, M.; Grugeon, S.; Vezin, H.
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Carbon Metal Fluoride Nanocomposites: High-Capacity Reversible Metal Fluoride Conversion Materials as Rechargeable Positive Electrodes for Li Batteries
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Badway, F.; Cosandey, F.; Pereira, N.
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Structure and Electrochemistry of Copper Fluoride Nanocomposites Utilizing Mixed Conducting Matrices
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Badway, F.; Mansour, A. N.; Pereira, N.
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Bismuth Fluoride Nanocomposite as a Positive Electrode Material for Rechargeable Lithium Batteries
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Bervas, M.; Badway, F.; Klein, L. C.
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Reversible Conversion Reactions with Lithium in Bismuth Oxyfluoride Nanocomposites
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High-performance lithium battery anodes using silicon nanowires
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