Transmission-geometry electrochemical cell for in-situ scattering and spectroscopy investigations

Chupas, Peter J.; Chapman, Karena W.; Kurtz, Charles A.; Borkiewicz, Olaf J.; Wiaderek, Kamila Magdelena; Shyam, Badri

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Title: Transmission-geometry electrochemical cell for in-situ scattering and spectroscopy investigations

Abstract

The present invention relates to a test chamber that can be used to perform a variety of X-ray and neutron spectroscopy experiments including powder diffraction, small-angle scattering, X-ray absorption spectroscopy, and pair distribution functions, such chamber comprising a first electrode with an X-ray transparent window; a second electrode with an X-ray transparent window; a plurality of insulating gaskets providing a hermetic seal around the sample and preventing contact between said first and second electrodes; and an insulating housing into which the first electrode is secured.

Inventors:: Chupas, Peter J.; Chapman, Karena W.; Kurtz, Charles A.; Borkiewicz, Olaf J.; Wiaderek, Kamila Magdelena; Shyam, Badri

Issue Date:: Tue May 05 00:00:00 EDT 2015

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1347439

Patent Number(s):: 9022652

Application Number:: 13/631,207

Assignee:: UChicago Argonne, LLC (Chicgo, IL)

Patent Classifications (CPCs):: G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY

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G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N2223/307 - cuvettes-sample holders
G01N23/20025 - Sample holders or supports therefor

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M10/48 - Accumulators combined with arrangements for measuring, testing or indicating condition, e.g. level or density of the electrolyte

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/10 - Energy storage

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DOE Contract Number:: AC02-06CH11357

Resource Type:: Patent

Resource Relation:: Patent File Date: 2012 Sep 28

Country of Publication:: United States

Language:: English

Subject:: 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY

Citation Formats


                    Chupas, Peter J., Chapman, Karena W., Kurtz, Charles A., Borkiewicz, Olaf J., Wiaderek, Kamila Magdelena, and Shyam, Badri. Transmission-geometry electrochemical cell for in-situ scattering and spectroscopy investigations.  United States: N. p., 2015. 
        Web.

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                    Chupas, Peter J., Chapman, Karena W., Kurtz, Charles A., Borkiewicz, Olaf J., Wiaderek, Kamila Magdelena, & Shyam, Badri. Transmission-geometry electrochemical cell for in-situ scattering and spectroscopy investigations.  United States.

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                    Chupas, Peter J., Chapman, Karena W., Kurtz, Charles A., Borkiewicz, Olaf J., Wiaderek, Kamila Magdelena, and Shyam, Badri. Tue .  
        "Transmission-geometry electrochemical cell for in-situ scattering and spectroscopy investigations".  United States.  https://www.osti.gov/servlets/purl/1347439.

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@article{osti_1347439,

  title        = {Transmission-geometry electrochemical cell for in-situ scattering and spectroscopy investigations},

  author       = {Chupas, Peter J. and Chapman, Karena W. and Kurtz, Charles A. and Borkiewicz, Olaf J. and Wiaderek, Kamila Magdelena and Shyam, Badri},

  abstractNote = {The present invention relates to a test chamber that can be used to perform a variety of X-ray and neutron spectroscopy experiments including powder diffraction, small-angle scattering, X-ray absorption spectroscopy, and pair distribution functions, such chamber comprising a first electrode with an X-ray transparent window; a second electrode with an X-ray transparent window; a plurality of insulating gaskets providing a hermetic seal around the sample and preventing contact between said first and second electrodes; and an insulating housing into which the first electrode is secured.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue May 05 00:00:00 EDT 2015},

  month        = {Tue May 05 00:00:00 EDT 2015}

}

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Works referenced in this record:

Sample cell support assembly for fluorescent X-ray analysis
patent, October 1993

Mizuta, Masao
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URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7729471

A compact high vacuum heating chamber for in-situ x-ray scattering studies
journal, August 2012

Bertram, F.; Deiter, C.; Pflaum, K.
Review of Scientific Instruments, Vol. 83, Issue 8
https://doi.org/10.1063/1.4746290

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