Solute-enhanced production of gamma-valerolactone (GVL) from aqueous solutions of levulinic acid

Dumesic, James A.; Wettstein, Stephanie G.; Alonso, David Martin; Gurbuz, Elif Ispir

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Title: Solute-enhanced production of gamma-valerolactone (GVL) from aqueous solutions of levulinic acid

Abstract

A method to produce levulinic acid (LA) and gamma-valerolactone (GVL) from biomass-derived cellulose or lignocellulose by selective extraction of LA using GVL and optionally converting the LA so isolated into GVL, with no purifications steps required to yield the GVL.

Inventors:: Dumesic, James A.; Wettstein, Stephanie G.; Alonso, David Martin; Gurbuz, Elif Ispir

Issue Date:: 2016-06-28

Research Org.:: Wisconsin Alumni Research Foundation, Madison, WI (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1344777

Patent Number(s):: 9376411

Application Number:: 14/596,357

Assignee:: Wisconsin Alumni Research Foundation (Madison, WI)

Patent Classifications (CPCs):: C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS

C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07D - HETEROCYCLIC COMPOUNDS

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C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS
C07C51/00 - Preparation of carboxylic acids or their salts, halides or anhydrides
C07C51/48 - by liquid-liquid treatment
C07C59/185 - Saturated compounds having only one carboxyl group and containing keto groups
C07C67/04 - by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds
C07C67/08 - by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
C07C69/716 - Esters of keto-carboxylic acids {or aldehydo-carboxylic acids}

C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07D - HETEROCYCLIC COMPOUNDS
C07D307/33 - in position 2, the oxygen atom being in its keto or unsubstituted enol form

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DOE Contract Number:: FC02-07ER64494

Resource Type:: Patent

Resource Relation:: Patent File Date: 2015 Jan 14

Country of Publication:: United States

Language:: English

Subject:: 09 BIOMASS FUELS; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats


                    Dumesic, James A., Wettstein, Stephanie G., Alonso, David Martin, and Gurbuz, Elif Ispir. Solute-enhanced production of gamma-valerolactone (GVL) from aqueous solutions of levulinic acid.  United States: N. p., 2016. 
        Web.

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                    Dumesic, James A., Wettstein, Stephanie G., Alonso, David Martin, & Gurbuz, Elif Ispir. Solute-enhanced production of gamma-valerolactone (GVL) from aqueous solutions of levulinic acid.  United States.

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                    Dumesic, James A., Wettstein, Stephanie G., Alonso, David Martin, and Gurbuz, Elif Ispir. Tue .  
        "Solute-enhanced production of gamma-valerolactone (GVL) from aqueous solutions of levulinic acid".  United States.  https://www.osti.gov/servlets/purl/1344777.

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@article{osti_1344777,

  title        = {Solute-enhanced production of gamma-valerolactone (GVL) from aqueous solutions of levulinic acid},

  author       = {Dumesic, James A. and Wettstein, Stephanie G. and Alonso, David Martin and Gurbuz, Elif Ispir},

  abstractNote = {A method to produce levulinic acid (LA) and gamma-valerolactone (GVL) from biomass-derived cellulose or lignocellulose by selective extraction of LA using GVL and optionally converting the LA so isolated into GVL, with no purifications steps required to yield the GVL.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2016},

  month        = {6}

}

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Works referenced in this record:

Method to produce and recover levulinic acid and/or gamma-valerolactone from aqueous solutions using alkylphenols
patent, March 2013

Dumesic, James A.; Bond, Jesse Quentin; Alonso, David Martin
US Patent Document 8,389,761
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8389761

Production of levulinic acid, furfural, and gamma valerolactone from C5 and C6 carbohydrates in mono- and biphasic systems using gamma-valerolactone as a solvent
patent, March 2013

Dumesic, James A.; Alonso, David Martin; Gurbuz, Elif Ispir
US Patent Document 8,399,688
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8399688