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Title: System and process for efficient separation of biocrudes and water in a hydrothermal liquefaction system

Abstract

A system and process are described for clean separation of biocrudes and water by-products from hydrothermal liquefaction (HTL) product mixtures of organic and biomass-containing feedstocks at elevated temperatures and pressures. Inorganic compound solids are removed prior to separation of biocrude and water by-product fractions to minimize formation of emulsions that impede separation. Separation may be performed at higher temperatures that reduce heat loss and need to cool product mixtures to ambient. The present invention thus achieves separation efficiencies not achieved in conventional HTL processing.

Inventors:
; ; ; ; ; ;
Issue Date:
Research Org.:
Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1281062
Patent Number(s):
9404063
Application Number:
14/534,010
Assignee:
Battelle Memorial Institute (Richland, WA)
Patent Classifications (CPCs):
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
C - CHEMISTRY C10 - PETROLEUM, GAS OR COKE INDUSTRIES C10G - CRACKING HYDROCARBON OILS
DOE Contract Number:  
AC05-76RL01830
Resource Type:
Patent
Resource Relation:
Patent File Date: 2014 Nov 05
Country of Publication:
United States
Language:
English
Subject:
09 BIOMASS FUELS; 54 ENVIRONMENTAL SCIENCES

Citation Formats

Elliott, Douglas C., Hart, Todd R., Neuenschwander, Gary G., Oyler, James R., Rotness, Jr, Leslie J., Schmidt, Andrew J., and Zacher, Alan H. System and process for efficient separation of biocrudes and water in a hydrothermal liquefaction system. United States: N. p., 2016. Web.
Elliott, Douglas C., Hart, Todd R., Neuenschwander, Gary G., Oyler, James R., Rotness, Jr, Leslie J., Schmidt, Andrew J., & Zacher, Alan H. System and process for efficient separation of biocrudes and water in a hydrothermal liquefaction system. United States.
Elliott, Douglas C., Hart, Todd R., Neuenschwander, Gary G., Oyler, James R., Rotness, Jr, Leslie J., Schmidt, Andrew J., and Zacher, Alan H. Tue . "System and process for efficient separation of biocrudes and water in a hydrothermal liquefaction system". United States. https://www.osti.gov/servlets/purl/1281062.
@article{osti_1281062,
title = {System and process for efficient separation of biocrudes and water in a hydrothermal liquefaction system},
author = {Elliott, Douglas C. and Hart, Todd R. and Neuenschwander, Gary G. and Oyler, James R. and Rotness, Jr, Leslie J. and Schmidt, Andrew J. and Zacher, Alan H.},
abstractNote = {A system and process are described for clean separation of biocrudes and water by-products from hydrothermal liquefaction (HTL) product mixtures of organic and biomass-containing feedstocks at elevated temperatures and pressures. Inorganic compound solids are removed prior to separation of biocrude and water by-product fractions to minimize formation of emulsions that impede separation. Separation may be performed at higher temperatures that reduce heat loss and need to cool product mixtures to ambient. The present invention thus achieves separation efficiencies not achieved in conventional HTL processing.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2016},
month = {8}
}

Works referenced in this record:

Process for producing hydrocarbon-containing liquids from biomass
patent, June 1987


20120055077
patent-application, May 2005


Process development for hydrothermal liquefaction of algae feedstocks in a continuous-flow reactor
journal, October 2013