Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples
Abstract
A magic-angle-spinning (MAS) nuclear magnetic resonance (NMR) probe is described that includes double containment enclosures configured to seal and contain hazardous samples for analysis. The probe is of a modular design that ensures containment of hazardous samples during sample analysis while preserving spin speeds for superior NMR performance and convenience of operation.
- Inventors:
- Issue Date:
- Research Org.:
- Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1257229
- Patent Number(s):
- 9366736
- Application Number:
- 14/106,441
- Assignee:
- BATTELLE MEMORIAL INSTITUTE (Richland, WA)
- Patent Classifications (CPCs):
-
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES
- DOE Contract Number:
- AC05-76RL01830
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 2013 Dec 13
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; 47 OTHER INSTRUMENTATION
Citation Formats
Cho, Herman M., Washton, Nancy M., Mueller, Karl T., Sears, Jr., Jesse A., Townsend, Mark R., and Ewing, James R. Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples. United States: N. p., 2016.
Web.
Cho, Herman M., Washton, Nancy M., Mueller, Karl T., Sears, Jr., Jesse A., Townsend, Mark R., & Ewing, James R. Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples. United States.
Cho, Herman M., Washton, Nancy M., Mueller, Karl T., Sears, Jr., Jesse A., Townsend, Mark R., and Ewing, James R. Tue .
"Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples". United States. https://www.osti.gov/servlets/purl/1257229.
@article{osti_1257229,
title = {Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples},
author = {Cho, Herman M. and Washton, Nancy M. and Mueller, Karl T. and Sears, Jr., Jesse A. and Townsend, Mark R. and Ewing, James R.},
abstractNote = {A magic-angle-spinning (MAS) nuclear magnetic resonance (NMR) probe is described that includes double containment enclosures configured to seal and contain hazardous samples for analysis. The probe is of a modular design that ensures containment of hazardous samples during sample analysis while preserving spin speeds for superior NMR performance and convenience of operation.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2016},
month = {6}
}
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Works referenced in this record:
Quantification of actinide α-radiation damage in minerals and ceramics
journal, January 2007
- Farnan, Ian; Cho, Herman; Weber, William J.
- Nature, Vol. 445, Issue 7124
The aqueous complexation of thorium with citrate under neutral to basic conditions
journal, January 2006
- Felmy, Andrew R.; Cho, Herman; Dixon, David A.
- Radiochimica Acta, Vol. 94, Issue 4
Complexation of Cm(III)/Eu(III) with silicates in basic solutions
journal, January 2005
- Wang, Zheming; Felmy, Andrew R.; Xia, Y. X.
- Radiochimica Acta, Vol. 93, Issue 12
High-resolution solid-state nuclear magnetic resonance experiments on highly radioactive ceramics
journal, December 2004
- Farnan, Ian; Cho, Herman; Weber, William J.
- Review of Scientific Instruments, Vol. 75, Issue 12
Temperature and Isotope Substitution Effects on the Structure and NMR Properties of the Pertechnetate Ion in Water
journal, September 2004
- Cho, Herman; de Jong, Wibe A.; McNamara, Bruce K.
- Journal of the American Chemical Society, Vol. 126, Issue 37
Comprehensive Solid-State NMR Characterization of Electronic Structure in Ditechnetium Heptoxide
journal, September 2010
- Cho, Herman; de Jong, Wibe A.; Sattelberger, Alfred P.
- Journal of the American Chemical Society, Vol. 132, Issue 38