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Title: Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples

Abstract

A magic-angle-spinning (MAS) nuclear magnetic resonance (NMR) probe is described that includes double containment enclosures configured to seal and contain hazardous samples for analysis. The probe is of a modular design that ensures containment of hazardous samples during sample analysis while preserving spin speeds for superior NMR performance and convenience of operation.

Inventors:
; ; ; ; ;
Issue Date:
Research Org.:
Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1257229
Patent Number(s):
9,366,736
Application Number:
14/106,441
Assignee:
BATTELLE MEMORIAL INSTITUTE (Richland, WA)
DOE Contract Number:  
AC05-76RL01830
Resource Type:
Patent
Resource Relation:
Patent File Date: 2013 Dec 13
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 47 OTHER INSTRUMENTATION

Citation Formats

Cho, Herman M., Washton, Nancy M., Mueller, Karl T., Sears, Jr., Jesse A., Townsend, Mark R., and Ewing, James R. Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples. United States: N. p., 2016. Web.
Cho, Herman M., Washton, Nancy M., Mueller, Karl T., Sears, Jr., Jesse A., Townsend, Mark R., & Ewing, James R. Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples. United States.
Cho, Herman M., Washton, Nancy M., Mueller, Karl T., Sears, Jr., Jesse A., Townsend, Mark R., and Ewing, James R. Tue . "Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples". United States. https://www.osti.gov/servlets/purl/1257229.
@article{osti_1257229,
title = {Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples},
author = {Cho, Herman M. and Washton, Nancy M. and Mueller, Karl T. and Sears, Jr., Jesse A. and Townsend, Mark R. and Ewing, James R.},
abstractNote = {A magic-angle-spinning (MAS) nuclear magnetic resonance (NMR) probe is described that includes double containment enclosures configured to seal and contain hazardous samples for analysis. The probe is of a modular design that ensures containment of hazardous samples during sample analysis while preserving spin speeds for superior NMR performance and convenience of operation.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2016},
month = {6}
}

Patent:

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Works referenced in this record:

Quantification of actinide α-radiation damage in minerals and ceramics
journal, January 2007

  • Farnan, Ian; Cho, Herman; Weber, William J.
  • Nature, Vol. 445, Issue 7124
  • DOI: 10.1038/nature05425

The aqueous complexation of thorium with citrate under neutral to basic conditions
journal, January 2006


Complexation of Cm(III)/Eu(III) with silicates in basic solutions
journal, January 2005


High-resolution solid-state nuclear magnetic resonance experiments on highly radioactive ceramics
journal, December 2004

  • Farnan, Ian; Cho, Herman; Weber, William J.
  • Review of Scientific Instruments, Vol. 75, Issue 12
  • DOI: 10.1063/1.1818512

Temperature and Isotope Substitution Effects on the Structure and NMR Properties of the Pertechnetate Ion in Water
journal, September 2004

  • Cho, Herman; de Jong, Wibe A.; McNamara, Bruce K.
  • Journal of the American Chemical Society, Vol. 126, Issue 37
  • DOI: 10.1021/ja047447i

Comprehensive Solid-State NMR Characterization of Electronic Structure in Ditechnetium Heptoxide
journal, September 2010

  • Cho, Herman; de Jong, Wibe A.; Sattelberger, Alfred P.
  • Journal of the American Chemical Society, Vol. 132, Issue 38
  • DOI: 10.1021/ja105687j