Containerless synthesis of amorphous and nanophase organic materials
Abstract
The invention provides a method for producing a mixture of amorphous compounds, the method comprising supplying a solution containing the compounds; and allowing at least a portion of the solvent of the solution to evaporate while preventing the solute of the solution from contacting a nucleation point. Also provided is a method for transforming solids to amorphous material, the method comprising heating the solids in an environment to form a melt, wherein the environment contains no nucleation points; and cooling the melt in the environment.
- Inventors:
- Issue Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1250472
- Patent Number(s):
- 9327264
- Application Number:
- 13/361,164
- Assignee:
- UCHICAGO ARGONNE, LLC (Chicago, IL)
- Patent Classifications (CPCs):
-
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
- DOE Contract Number:
- AC02-06CH11357
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 2012 Jan 30
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE
Citation Formats
Benmore, Chris J., and Weber, Johann R. Containerless synthesis of amorphous and nanophase organic materials. United States: N. p., 2016.
Web.
Benmore, Chris J., & Weber, Johann R. Containerless synthesis of amorphous and nanophase organic materials. United States.
Benmore, Chris J., and Weber, Johann R. Tue .
"Containerless synthesis of amorphous and nanophase organic materials". United States. https://www.osti.gov/servlets/purl/1250472.
@article{osti_1250472,
title = {Containerless synthesis of amorphous and nanophase organic materials},
author = {Benmore, Chris J. and Weber, Johann R.},
abstractNote = {The invention provides a method for producing a mixture of amorphous compounds, the method comprising supplying a solution containing the compounds; and allowing at least a portion of the solvent of the solution to evaporate while preventing the solute of the solution from contacting a nucleation point. Also provided is a method for transforming solids to amorphous material, the method comprising heating the solids in an environment to form a melt, wherein the environment contains no nucleation points; and cooling the melt in the environment.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2016},
month = {5}
}
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Works referenced in this record:
Structure analysis using acoustically levitated droplets
journal, March 2008
- Leiterer, J.; Delißen, F.; Emmerling, F.
- Analytical and Bioanalytical Chemistry, Vol. 391, Issue 4
Solidification of acoustically levitated o-terphenyl crystals: a Raman study
journal, January 1995
- Biswas, A.
- Journal of Crystal Growth, Vol. 147, Issue 1-2, p. 155-164
Acoustic levitator for structure measurements on low temperature liquid droplets
journal, August 2009
- Weber, J. K. R.; Rey, C. A.; Neuefeind, J.
- Review of Scientific Instruments, Vol. 80, Issue 8
Effect of Synthesis Techniques on Crystallite Size and Morphology of Lithium Aluminate
journal, April 1995
- Carrera, Luz Maria; Jimenez-Becerril, Jaime; Bosch, Pedro
- Journal of the American Ceramic Society, Vol. 78, Issue 4
Physicochemical Properties of Indomethacin and Related Compounds Co-Spray Dried with Polyvinylpyrrolidone
journal, January 1985
- Corrigan, O. I.; Holohan, E. M.; Reilly, M. R.
- Drug Development and Industrial Pharmacy, Vol. 11, Issue 2-3
Combined Synchrotron XRD/Raman Measurements: In Situ Identification of Polymorphic Transitions during Crystallization Processes
journal, July 2010
- Klimakow, Maria; Leiterer, Jork; Kneipp, Janina
- Langmuir, Vol. 26, Issue 13
Two-dimensional detector software: From real detector to idealised image or two-theta scan
journal, January 1996
- Hammersley, A. P.; Svensson, S. O.; Hanfland, M.
- High Pressure Research, Vol. 14, Issue 4-6, p. 235-248
PDFgetX2: a GUI-driven program to obtain the pair distribution function from X-ray powder diffraction data
journal, July 2004
- Qiu, Xiangyun; Thompson, Jeroen W.; Billinge, Simon J. L.
- Journal of Applied Crystallography, Vol. 37, Issue 4, p. 678-678
Amorphous Pharmaceutical Solids: Characterization, Stabilization, and Development of Marketable Formulations of Poorly Soluble Drugs with Improved Oral Absorption
journal, November 2008
- Gao, Ping
- Molecular Pharmaceutics, Vol. 5, Issue 6
Sustained release drug delivery system
patent, July 1992
- Mulligan, Seamus; Sparks, Randall T.
- US Patent Document 5,128,142
Method for screening crystallization or amorphous stage conditions for molecules
patent, April 2007
- Nilsson, Staffan; Cedergren, Eila; Santesson, Sabina
- US Patent Document 7,200,493