High heating rate thermal desorption for molecular surface sampling

Ovchinnikova, Olga S.; Van Berkel, Gary J.

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Title: High heating rate thermal desorption for molecular surface sampling

Abstract

A method for analyzing a sample having at least one analyte includes the step of heating the sample at a rate of at least 10.sup.6 K/s to thermally desorb at least one analyte from the sample. The desorbed analyte is collected. The analyte can then be analyzed.

Inventors:: Ovchinnikova, Olga S.; Van Berkel, Gary J.

Issue Date:: Tue Mar 29 00:00:00 EDT 2016

Research Org.:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1244232

Patent Number(s):: 9297828

Application Number:: 14/227,364

Assignee:: UT-BATTELLE, LLC (Oak Ridge, TN)

Patent Classifications (CPCs):: G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES

G - PHYSICS G01 - MEASURING G01Q - SCANNING-PROBE TECHNIQUES OR APPARATUS

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G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N1/4022 - {by thermal techniques
G01N1/405 - {by adsorption or absorption}

G - PHYSICS G01 - MEASURING G01Q - SCANNING-PROBE TECHNIQUES OR APPARATUS
G01Q30/02 - Non-SPM analysing devices, e.g. SEM [Scanning Electron Microscope], spectrometer or optical microscope

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01J - ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
H01J49/049 - {with means for applying heat to desorb the sample

Show less

DOE Contract Number:: AC05-00OR22725

Resource Type:: Patent

Resource Relation:: Patent File Date: 2014 Mar 27

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 36 MATERIALS SCIENCE

Citation Formats


                    Ovchinnikova, Olga S., and Van Berkel, Gary J. High heating rate thermal desorption for molecular surface sampling.  United States: N. p., 2016. 
        Web.

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                    Ovchinnikova, Olga S., & Van Berkel, Gary J. High heating rate thermal desorption for molecular surface sampling.  United States.

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                    Ovchinnikova, Olga S., and Van Berkel, Gary J. Tue .  
        "High heating rate thermal desorption for molecular surface sampling".  United States.  https://www.osti.gov/servlets/purl/1244232.

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@article{osti_1244232,

  title        = {High heating rate thermal desorption for molecular surface sampling},

  author       = {Ovchinnikova, Olga S. and Van Berkel, Gary J.},

  abstractNote = {A method for analyzing a sample having at least one analyte includes the step of heating the sample at a rate of at least 10.sup.6 K/s to thermally desorb at least one analyte from the sample. The desorbed analyte is collected. The analyte can then be analyzed.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Mar 29 00:00:00 EDT 2016},

  month        = {Tue Mar 29 00:00:00 EDT 2016}

}

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Similar Records

Title: High heating rate thermal desorption for molecular surface sampling

Abstract

Citation Formats

Mass spectra of underivatized peptide amides related to substance P journal, September 1977

Mass spectrometry of intact neutral macromolecules using intense non-resonant femtosecond laser vaporization with electrospray post-ionization journal, October 2009

Femtosecond laser aperturless near-field nanomachining of metals assisted by scanning probe microscopy journal, February 2003

Matrix-assisted filament desorption/ionization mass spectrometry journal, November 1998

Nanoscale Thermal Analysis of an Energetic Material journal, September 2006

Electrical, Thermal, and Mechanical Characterization of Silicon Microcantilever Heaters journal, December 2006

Laser-Scanning Probe Microscope Based Nanoprocessing of Electronics Materials journal, June 2001

Evidence for thermalization of surface‐desorbed molecules at heating rates of 10 8 K/s journal, June 1996

Thermomechanical writing with an atomic force microscope tip journal, August 1992

Floating Tip Nanolithography journal, July 2008

Heating of an Atomic Force Microscope tip by femtosecond laser pulses journal, March 2010

Pulsed laser heating of surfaces: nanosecond timescale temperature measurement using black body radiation journal, June 1996

Pulsed heating of surfaces: Comparison between numerical simulation, analytical models, and experiments journal, June 1989

Mechanisms of Pulsed Laser Ablation of Biological Tissues journal, February 2003

Apparatus and method for laser desorption of molecules for quantitation patent, January 1991

Systems for differential ion mobility analysis patent, August 2009

High power laser induced acoustic desorption probe patent, November 2009

Cantilevered probe detector with piezoelectric element patent, April 2010

Methods for detecting catecholamines by mass spectrometry patent, May 2011

Sensor for detecting and differentiating chemical analytes patent, July 2011

Device for desorption and ionization patent, August 2012

Thermochemical nanolithography components, systems, and methods patent, June 2013

High power laser induced acoustic desorption probe patent-application, December 2007

Spatially resolved thermal desorption/ionization coupled with mass spectrometry patent-application, March 2012

Mass spectra of underivatized peptide amides related to substance P
journal, September 1977

Mass spectrometry of intact neutral macromolecules using intense non-resonant femtosecond laser vaporization with electrospray post-ionization
journal, October 2009

Femtosecond laser aperturless near-field nanomachining of metals assisted by scanning probe microscopy
journal, February 2003

Matrix-assisted filament desorption/ionization mass spectrometry
journal, November 1998

Nanoscale Thermal Analysis of an Energetic Material
journal, September 2006

Electrical, Thermal, and Mechanical Characterization of Silicon Microcantilever Heaters
journal, December 2006

Laser-Scanning Probe Microscope Based Nanoprocessing of Electronics Materials
journal, June 2001

Evidence for thermalization of surface‐desorbed molecules at heating rates of 10 ⁸ K/s
journal, June 1996

Thermomechanical writing with an atomic force microscope tip
journal, August 1992

Floating Tip Nanolithography
journal, July 2008

Heating of an Atomic Force Microscope tip by femtosecond laser pulses
journal, March 2010

Pulsed laser heating of surfaces: nanosecond timescale temperature measurement using black body radiation
journal, June 1996

Pulsed heating of surfaces: Comparison between numerical simulation, analytical models, and experiments
journal, June 1989

Mechanisms of Pulsed Laser Ablation of Biological Tissues
journal, February 2003

Apparatus and method for laser desorption of molecules for quantitation
patent, January 1991

Systems for differential ion mobility analysis
patent, August 2009

High power laser induced acoustic desorption probe
patent, November 2009

Cantilevered probe detector with piezoelectric element
patent, April 2010

Methods for detecting catecholamines by mass spectrometry
patent, May 2011

Sensor for detecting and differentiating chemical analytes
patent, July 2011

Device for desorption and ionization
patent, August 2012

Thermochemical nanolithography components, systems, and methods
patent, June 2013

High power laser induced acoustic desorption probe
patent-application, December 2007

Spatially resolved thermal desorption/ionization coupled with mass spectrometry
patent-application, March 2012