Method of making highly porous, stable aluminum oxides doped with silicon

Title: Method of making highly porous, stable aluminum oxides doped with silicon

Inventors:: Khosravi-Mardkhe, Maryam; Woodfield, Brian F.; Bartholomew, Calvin H.; Huang, Baiyu

Issue Date:: 2016-03-22

Research Org.:: Brigham Young University Provo, UT (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1243055

Patent Number(s):: 9289750

Application Number:: 14/201,538

Assignee:: Brigham Young University (Provo, UT)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS

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B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J37/04 - Mixing {

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
C01P2004/53 - bimodal size distribution

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J35/1019 - {100-500 m2/g}

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01F - COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
C01F7/441 - {by calcination}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J35/109 - {bimodal}
B01J35/1042 - {0.5-1.0 ml/g}

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01F - COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
C01F7/36 - from organic aluminium salts

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J35/1047 - {more than 1.0 ml/g}

C - CHEMISTRY C04 - CEMENTS C04B - LIME, MAGNESIA
C04B35/10 - based on aluminium oxide

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J21/12 - Silica and alumina

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
C01P2006/14 - Pore volume

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J20/16 - Alumino-silicates
B01J35/1061 - {2-50 nm}

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
C01P2004/82 - two phases having the same anion, e.g. both oxidic phases

C - CHEMISTRY C04 - CEMENTS C04B - LIME, MAGNESIA
C04B38/06 - by burning-out added substances {by burning natural expanding materials or by sublimating or melting out added substances}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J20/3078 - {Thermal treatment, e.g. calcining or pyrolizing}
B01J37/033 - {Using Hydrolysis}
B01J37/03 - Precipitation
B01J37/082 - {Decomposition and pyrolysis}

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
C01P2004/04 - obtained by TEM, STEM, STM or AFM

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01F - COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
C01F7/02 - Aluminium oxide

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J35/1038 - {less than 0.5 ml/g}

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
C01P2006/12 - Surface area
C01P2002/72 - by d-values or two theta-values, e.g. as X-ray diagram

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DOE Contract Number:: FG02-05ER15666

Resource Type:: Patent

Resource Relation:: Patent File Date: 2014 Mar 07

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats


                    Khosravi-Mardkhe, Maryam, Woodfield, Brian F., Bartholomew, Calvin H., and Huang, Baiyu. Method of making highly porous, stable aluminum oxides doped with silicon.  United States: N. p., 2016. 
        Web.

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                    Khosravi-Mardkhe, Maryam, Woodfield, Brian F., Bartholomew, Calvin H., & Huang, Baiyu. Method of making highly porous, stable aluminum oxides doped with silicon.  United States.

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                    Khosravi-Mardkhe, Maryam, Woodfield, Brian F., Bartholomew, Calvin H., and Huang, Baiyu. Tue .  
        "Method of making highly porous, stable aluminum oxides doped with silicon".  United States.  https://www.osti.gov/servlets/purl/1243055.

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@article{osti_1243055,

  title        = {Method of making highly porous, stable aluminum oxides doped with silicon},

  author       = {Khosravi-Mardkhe, Maryam and Woodfield, Brian F. and Bartholomew, Calvin H. and Huang, Baiyu},

  abstractNote = {},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2016},

  month        = {3}

}

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Similar Records

Title: Method of making highly porous, stable aluminum oxides doped with silicon

Citation Formats

Sol-Gel transition and structural evolution on multicomponent gels derived from the alumina-silica system journal, October 1997

Preparation of Nanometer Zinc Oxide Powders by Plasma Pyrolysis Technology and Their Applications journal, November 2000

Preparations of Nickel, Cobalt, and Iron Nanoparticles through the Rapid Expansion of Supercritical Fluid Solutions (RESS) and Chemical Reduction journal, January 1999

Simple synthesis of MgFe2O4 nanoparticles as gas sensing materials journal, June 2005

Synthesis and characterization of ZnO nanoparticles assembled in one-dimensional order journal, July 2003

Non-isothermal kinetics studies on the thermal decomposition of zinc hydroxide carbonate journal, November 2005

Characterisation of ZnO-based varistors prepared from nanometre Precursor powders journal, September 1999

Ultrafine iron oxide powders generated using a flow-through hydrothermal process journal, August 1992

Preparation of nanometre size oxide particles using filter expansion aerosol generator journal, January 1996

Citrate route to the piezoelectric Pb(Zr,Ti)O3 oxide journal, January 1997

Supercritical Antisolvent Precipitation of Nanoparticles of Superconductor Precursors journal, March 1998

Synthesis and Growth of ZnO Nanoparticles journal, July 1998

Preparation of Platinum Nanoparticles by Sonochemical Reduction of the Pt(II) Ion journal, April 1999

Pyrochlore-free Pb(Mg1/3Nb2/3)O3 prepared by a combination of the partial oxalate and the polymerized complex methods journal, January 2001

Cerium oxide nanoparticles: Size-selective formation and structure analysis journal, January 2002

ZnO nanoparticles prepared by thermal decomposition of β-cyclodextrin coated zinc acetate journal, May 2003

Synthesis of Nanocrystalline α-Al 2 O 3 Powders from Nanometric Ammonium Aluminum Carbonate Hydroxide journal, August 2003

Generation of metal and metal oxide nanoparticles by liquid flame spray process journal, April 2004

Preparation of zinc oxide nanoparticles coated with homogeneous Al2O3 layer journal, August 2005

Synthesis of bismuth oxide nanoparticles using bismuth nitrate and urea journal, January 2005

Synthesis of bismuth oxide nanoparticles at 100 °C journal, August 2005

Non-aqueous routes to crystalline metal oxide nanoparticles: Formation mechanisms and applications journal, January 2005

One-step solid-state reaction synthesis and gas sensing property of tin oxide nanoparticles journal, January 2002

Optical and electrochemical properties of nanosized NiO via thermal decomposition of nickel oxalate nanofibres journal, December 2004

Preparation and characterization of α-FeOOH and α-Fe2O3 by sol–gel method journal, June 2005

Ferrimagnetic Nanogranular Co 3 O 4 through Solvothermal Decomposition of Colloidally Dispersed Monolayers of α-Cobalt Hydroxide journal, June 2005

From the organized nanoparticles of copper and vanadium containing LDHs to the small nanoparticles of mixtures of mixed oxides: A simple route journal, October 2005

Polyol method for the preparation of nanosized Gd2O3, boehmite and other oxides journal, December 2005

Molecular Encoding at the Nanoscale From Complex Cubes to Bimetallic Oxides journal, December 2005

Novel preparation of nanosized ZnO–SnO2 with high photocatalytic activity by homogeneous co-precipitation method journal, December 2005

Extracellular Synthesis of Magnetite and Metal-Substituted Magnetite Nanoparticles journal, November 2006

Synthesis and characterization of Ca3Co4O9 nanoparticles by citrate sol-gel method journal, September 2006

Cobalt nanoparticles synthesis from Co(CH3COO)2 by thermal decomposition journal, September 2006

Nonisothermal Synthesis of Yttria-Stabilized Zirconia Nanopowder through Oxalate Processing: I, Characteristics of Y-Zr Oxalate Synthesis and Its Decomposition journal, September 2000

RF Induction Plasma Synthesized Calcium Phosphate Nanoparticles journal, May 2006

The solid-state synthesis of metal nanoparticles from organometallic precursors journal, July 2005

Low-temperature synthesis of ZnO nanoparticles by solid-state pyrolytic reaction journal, December 2002

Preparation of nanocrystalline zinc carbonate and zinc oxide via solid-state reaction at room temperature journal, September 2006

High temperature stability of alumina fibre journal, September 1991

Effect of silica on the stability of the nanostructure and texture of fine-particle alumina journal, February 2012

Control of micropore size distribution in alumina by the hydrothermal treatment of an alkoxide derived-alcogel journal, June 1996

Stabilization of alumina toward thermal sintering by silicon addition journal, February 1991

Lithium metal oxides patent, June 2004

Inorganic material that has metal nanoparticles that are trapped in a mesostructured matrix patent, July 2012

Sol-Gel transition and structural evolution on multicomponent gels derived from the alumina-silica system
journal, October 1997

Preparation of Nanometer Zinc Oxide Powders by Plasma Pyrolysis Technology and Their Applications
journal, November 2000

Preparations of Nickel, Cobalt, and Iron Nanoparticles through the Rapid Expansion of Supercritical Fluid Solutions (RESS) and Chemical Reduction
journal, January 1999

Simple synthesis of MgFe₂O₄ nanoparticles as gas sensing materials
journal, June 2005

Synthesis and characterization of ZnO nanoparticles assembled in one-dimensional order
journal, July 2003

Non-isothermal kinetics studies on the thermal decomposition of zinc hydroxide carbonate
journal, November 2005

Characterisation of ZnO-based varistors prepared from nanometre Precursor powders
journal, September 1999

Ultrafine iron oxide powders generated using a flow-through hydrothermal process
journal, August 1992

Preparation of nanometre size oxide particles using filter expansion aerosol generator
journal, January 1996

Citrate route to the piezoelectric Pb(Zr,Ti)O3 oxide
journal, January 1997

Supercritical Antisolvent Precipitation of Nanoparticles of Superconductor Precursors
journal, March 1998

Synthesis and Growth of ZnO Nanoparticles
journal, July 1998

Preparation of Platinum Nanoparticles by Sonochemical Reduction of the Pt(II) Ion
journal, April 1999

Pyrochlore-free Pb(Mg_1/3Nb_2/3)O₃ prepared by a combination of the partial oxalate and the polymerized complex methods
journal, January 2001

Cerium oxide nanoparticles: Size-selective formation and structure analysis
journal, January 2002

ZnO nanoparticles prepared by thermal decomposition of β-cyclodextrin coated zinc acetate
journal, May 2003

Synthesis of Nanocrystalline α-Al ₂ O ₃ Powders from Nanometric Ammonium Aluminum Carbonate Hydroxide
journal, August 2003

Generation of metal and metal oxide nanoparticles by liquid flame spray process
journal, April 2004

Preparation of zinc oxide nanoparticles coated with homogeneous Al₂O₃ layer
journal, August 2005

Synthesis of bismuth oxide nanoparticles using bismuth nitrate and urea
journal, January 2005

Synthesis of bismuth oxide nanoparticles at 100 °C
journal, August 2005

Non-aqueous routes to crystalline metal oxide nanoparticles: Formation mechanisms and applications
journal, January 2005

One-step solid-state reaction synthesis and gas sensing property of tin oxide nanoparticles
journal, January 2002

Optical and electrochemical properties of nanosized NiO via thermal decomposition of nickel oxalate nanofibres
journal, December 2004

Preparation and characterization of α-FeOOH and α-Fe2O3 by sol–gel method
journal, June 2005

Ferrimagnetic Nanogranular Co ₃ O ₄ through Solvothermal Decomposition of Colloidally Dispersed Monolayers of α-Cobalt Hydroxide
journal, June 2005

From the organized nanoparticles of copper and vanadium containing LDHs to the small nanoparticles of mixtures of mixed oxides: A simple route
journal, October 2005

Polyol method for the preparation of nanosized Gd₂O₃, boehmite and other oxides
journal, December 2005

Molecular Encoding at the Nanoscale From Complex Cubes to Bimetallic Oxides
journal, December 2005

Novel preparation of nanosized ZnO–SnO2 with high photocatalytic activity by homogeneous co-precipitation method
journal, December 2005

Extracellular Synthesis of Magnetite and Metal-Substituted Magnetite Nanoparticles
journal, November 2006

Synthesis and characterization of Ca₃Co₄O₉ nanoparticles by citrate sol-gel method
journal, September 2006

Cobalt nanoparticles synthesis from Co(CH₃COO)₂ by thermal decomposition
journal, September 2006

Nonisothermal Synthesis of Yttria-Stabilized Zirconia Nanopowder through Oxalate Processing: I, Characteristics of Y-Zr Oxalate Synthesis and Its Decomposition
journal, September 2000

RF Induction Plasma Synthesized Calcium Phosphate Nanoparticles
journal, May 2006

The solid-state synthesis of metal nanoparticles from organometallic precursors
journal, July 2005

Low-temperature synthesis of ZnO nanoparticles by solid-state pyrolytic reaction
journal, December 2002

Preparation of nanocrystalline zinc carbonate and zinc oxide via solid-state reaction at room temperature
journal, September 2006

High temperature stability of alumina fibre
journal, September 1991

Effect of silica on the stability of the nanostructure and texture of fine-particle alumina
journal, February 2012

Control of micropore size distribution in alumina by the hydrothermal treatment of an alkoxide derived-alcogel
journal, June 1996

Stabilization of alumina toward thermal sintering by silicon addition
journal, February 1991

Lithium metal oxides
patent, June 2004

Inorganic material that has metal nanoparticles that are trapped in a mesostructured matrix
patent, July 2012