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Title: Integrated crystal mounting and alignment system for high-throughput biological crystallography

Abstract

A method and apparatus for the transportation, remote and unattended mounting, and visual alignment and monitoring of protein crystals for synchrotron generated x-ray diffraction analysis. The protein samples are maintained at liquid nitrogen temperatures at all times: during shipment, before mounting, mounting, alignment, data acquisition and following removal. The samples must additionally be stably aligned to within a few microns at a point in space. The ability to accurately perform these tasks remotely and automatically leads to a significant increase in sample throughput and reliability for high-volume protein characterization efforts. Since the protein samples are placed in a shipping-compatible layered stack of sample cassettes each holding many samples, a large number of samples can be shipped in a single cryogenic shipping container.

Inventors:
; ; ; ; ; ; ; ; ;
Issue Date:
Research Org.:
Univ. of California, Oakland, CA (United States); Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1175427
Patent Number(s):
6918698
Application Number:
10/319,282
Assignee:
The Regents of the University of California (Oakland, CA)
Patent Classifications (CPCs):
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01L - CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
DOE Contract Number:  
AC03-76SF00098
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
47 OTHER INSTRUMENTATION

Citation Formats

Nordmeyer, Robert A., Snell, Gyorgy P., Cornell, Earl W., Kolbe, William, Yegian, Derek, Earnest, Thomas N., Jaklevic, Joseph M., Cork, Carl W., Santarsiero, Bernard D., and Stevens, Raymond C. Integrated crystal mounting and alignment system for high-throughput biological crystallography. United States: N. p., 2005. Web.
Nordmeyer, Robert A., Snell, Gyorgy P., Cornell, Earl W., Kolbe, William, Yegian, Derek, Earnest, Thomas N., Jaklevic, Joseph M., Cork, Carl W., Santarsiero, Bernard D., & Stevens, Raymond C. Integrated crystal mounting and alignment system for high-throughput biological crystallography. United States.
Nordmeyer, Robert A., Snell, Gyorgy P., Cornell, Earl W., Kolbe, William, Yegian, Derek, Earnest, Thomas N., Jaklevic, Joseph M., Cork, Carl W., Santarsiero, Bernard D., and Stevens, Raymond C. Tue . "Integrated crystal mounting and alignment system for high-throughput biological crystallography". United States. https://www.osti.gov/servlets/purl/1175427.
@article{osti_1175427,
title = {Integrated crystal mounting and alignment system for high-throughput biological crystallography},
author = {Nordmeyer, Robert A. and Snell, Gyorgy P. and Cornell, Earl W. and Kolbe, William and Yegian, Derek and Earnest, Thomas N. and Jaklevic, Joseph M. and Cork, Carl W. and Santarsiero, Bernard D. and Stevens, Raymond C.},
abstractNote = {A method and apparatus for the transportation, remote and unattended mounting, and visual alignment and monitoring of protein crystals for synchrotron generated x-ray diffraction analysis. The protein samples are maintained at liquid nitrogen temperatures at all times: during shipment, before mounting, mounting, alignment, data acquisition and following removal. The samples must additionally be stably aligned to within a few microns at a point in space. The ability to accurately perform these tasks remotely and automatically leads to a significant increase in sample throughput and reliability for high-volume protein characterization efforts. Since the protein samples are placed in a shipping-compatible layered stack of sample cassettes each holding many samples, a large number of samples can be shipped in a single cryogenic shipping container.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2005},
month = {7}
}