Electrically conductive polycrystalline diamond and particulate metal based electrodes

Swain, Greg M.; Wang, Jian

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Title: Electrically conductive polycrystalline diamond and particulate metal based electrodes

Abstract

An electrically conducting and dimensionally stable diamond (12, 14) and metal particle (13) electrode produced by electrodepositing the metal on the diamond is described. The electrode is particularly useful in harsh chemical environments and at high current densities and potentials. The electrode is particularly useful for generating hydrogen, and for reducing oxygen and oxidizing methanol in reactions which are of importance in fuel cells.

Inventors:: Swain, Greg M.; Wang, Jian

Issue Date:: 2005-04-26

Research Org.:: Michigan State Univ., East Lansing, MI (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1175327

Patent Number(s):: 6884290

Application Number:: 10/338,318

Assignee:: Board of Trustees of Michigan State University (East Lansing, MI)

Patent Classifications (CPCs):: C - CHEMISTRY C02 - TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE C02F - TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE

C - CHEMISTRY C23 - COATING METALLIC MATERIAL C23C - COATING METALLIC MATERIAL

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C - CHEMISTRY C02 - TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE C02F - TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
C02F1/46109 - {Electrodes}
C02F2001/46133 - {characterised by the material}
C02F2001/46142 - {Catalytic coating}

C - CHEMISTRY C23 - COATING METALLIC MATERIAL C23C - COATING METALLIC MATERIAL
C23C16/274 - {using microwave discharges}
C23C16/278 - {doping or introduction of a secondary phase in the diamond}

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25D - PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS
C25D3/50 - of platinum group metals

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M4/8853 - {Electrodeposition}
H01M4/92 - Metals of platinum group
H01M4/926 - {on carbon or graphite}

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/50 - Fuel cells

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DOE Contract Number:: FG02-01ER15120

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Swain, Greg M., and Wang, Jian. Electrically conductive polycrystalline diamond and particulate metal based electrodes.  United States: N. p., 2005. 
        Web.

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                    Swain, Greg M., & Wang, Jian. Electrically conductive polycrystalline diamond and particulate metal based electrodes.  United States.

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                    Swain, Greg M., and Wang, Jian. Tue .  
        "Electrically conductive polycrystalline diamond and particulate metal based electrodes".  United States.  https://www.osti.gov/servlets/purl/1175327.

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@article{osti_1175327,

  title        = {Electrically conductive polycrystalline diamond and particulate metal based electrodes},

  author       = {Swain, Greg M. and Wang, Jian},

  abstractNote = {An electrically conducting and dimensionally stable diamond (12, 14) and metal particle (13) electrode produced by electrodepositing the metal on the diamond is described. The electrode is particularly useful in harsh chemical environments and at high current densities and potentials. The electrode is particularly useful for generating hydrogen, and for reducing oxygen and oxidizing methanol in reactions which are of importance in fuel cells.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2005},

  month        = {4}

}

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Works referenced in this record:

Peer Reviewed: Boron-Doped Diamond Thin-Film Electrodes
journal, October 1997

Xu, Jishou; Granger, Michael C.; Chen, Qingyun
Analytical Chemistry, Vol. 69, Issue 19
https://doi.org/10.1021/ac971791z

Applications of Diamond Thin Films in Electrochemistry
journal, September 1998

Swain, Greg M.; Anderson, Alfred B.; Angus, John C.
MRS Bulletin, Vol. 23, Issue 9
https://doi.org/10.1557/S0883769400029389

Electrochemical Oxidation of NADH at Highly Boron-Doped Diamond Electrodes
journal, July 1999

Rao, Tata N.; Yagi, I.; Miwa, T.
Analytical Chemistry, Vol. 71, Issue 13
https://doi.org/10.1021/ac981376m

Summary of Recent Progress with Diamond Electrodes in Electroanalysis, Spectroelectrochemistry and Electrocatalysis
journal, January 2001

Witek, M.; Wang, J.; Stotter, J.
Journal of Wide Bandgap Materials, Vol. 8, Issue 3-4
https://doi.org/10.1106/152451102024653

Incorporation of Pt Particles in Boron-Doped Diamond Thin Films Applications in Electrocatalysis
journal, January 1999

Wang, Jian
Electrochemical and Solid-State Letters, Vol. 3, Issue 6
https://doi.org/10.1149/1.1391126

The Susceptibility to Surface Corrosion in Acidic Fluoride Media: A Comparison of Diamond, HOPG, and Glassy Carbon Electrodes
journal, January 1994

Swain, Greg M.
Journal of The Electrochemical Society, Vol. 141, Issue 12
https://doi.org/10.1149/1.2059343

Diamond Electrodes
journal, January 1998

Tenne, Reshef; Lévy-Clément, Claude
Israel Journal of Chemistry, Vol. 38, Issue 1-2
https://doi.org/10.1002/ijch.199800007

Morphological and Microstructural Stability of Boron-Doped Diamond Thin Film Electrodes in an Acidic Chloride Medium at High Anodic Current Densities
journal, January 1997

Chen, Qingyun
Journal of The Electrochemical Society, Vol. 144, Issue 11
https://doi.org/10.1149/1.1838096

Carbons as supports for industrial precious metal catalysts
journal, October 1998

Auer, E.; Freund, A.; Pietsch, J.
Applied Catalysis A: General, Vol. 173, Issue 2
https://doi.org/10.1016/S0926-860X(98)00184-7

Synthetic diamond in electrochemistry
journal, May 1999

Pleskov, Yurii V.
Russian Chemical Reviews, Vol. 68, Issue 5
https://doi.org/10.1070/RC1999v068n05ABEH000494

Electrochemical Behavior of Boron-Doped Diamond Electrodes
journal, January 1996

Vinokur, N.
Journal of The Electrochemical Society, Vol. 143, Issue 10
https://doi.org/10.1149/1.1837157

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Similar Records

Title: Electrically conductive polycrystalline diamond and particulate metal based electrodes

Abstract

Citation Formats

Peer Reviewed: Boron-Doped Diamond Thin-Film Electrodes journal, October 1997

Applications of Diamond Thin Films in Electrochemistry journal, September 1998

Electrochemical Oxidation of NADH at Highly Boron-Doped Diamond Electrodes journal, July 1999

Summary of Recent Progress with Diamond Electrodes in Electroanalysis, Spectroelectrochemistry and Electrocatalysis journal, January 2001

Incorporation of Pt Particles in Boron-Doped Diamond Thin Films Applications in Electrocatalysis journal, January 1999

The Susceptibility to Surface Corrosion in Acidic Fluoride Media: A Comparison of Diamond, HOPG, and Glassy Carbon Electrodes journal, January 1994

Diamond Electrodes journal, January 1998

Morphological and Microstructural Stability of Boron-Doped Diamond Thin Film Electrodes in an Acidic Chloride Medium at High Anodic Current Densities journal, January 1997

Carbons as supports for industrial precious metal catalysts journal, October 1998

Synthetic diamond in electrochemistry journal, May 1999

Electrochemical Behavior of Boron-Doped Diamond Electrodes journal, January 1996

Peer Reviewed: Boron-Doped Diamond Thin-Film Electrodes
journal, October 1997

Applications of Diamond Thin Films in Electrochemistry
journal, September 1998

Electrochemical Oxidation of NADH at Highly Boron-Doped Diamond Electrodes
journal, July 1999

Summary of Recent Progress with Diamond Electrodes in Electroanalysis, Spectroelectrochemistry and Electrocatalysis
journal, January 2001

Incorporation of Pt Particles in Boron-Doped Diamond Thin Films Applications in Electrocatalysis
journal, January 1999

The Susceptibility to Surface Corrosion in Acidic Fluoride Media: A Comparison of Diamond, HOPG, and Glassy Carbon Electrodes
journal, January 1994

Diamond Electrodes
journal, January 1998

Morphological and Microstructural Stability of Boron-Doped Diamond Thin Film Electrodes in an Acidic Chloride Medium at High Anodic Current Densities
journal, January 1997

Carbons as supports for industrial precious metal catalysts
journal, October 1998

Synthetic diamond in electrochemistry
journal, May 1999

Electrochemical Behavior of Boron-Doped Diamond Electrodes
journal, January 1996