Method for monitoring the crystallization of an organic material from a liquid
Abstract
Method for monitoring the crystallization of at least one organic material from a liquid. According to the method, a liquid having at least one organic material capable of existing in at least one non-centrosymmetric phase is prepared. The liquid is interrogated with a laser beam at a chosen wavelength. As at least a portion of the at least one organic material crystallizes from the liquid, the intensity of any light scattered by the crystallized material at a wavelength equal to one-half the chosen wavelength of the interrogating laser beam is monitored. If the intensity of this scattered light, increases, then the crystals that form include at least one non-cetrosymmetric phase.
- Inventors:
- Issue Date:
- Research Org.:
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1175063
- Patent Number(s):
- 6800487
- Application Number:
- 10/259,345
- Assignee:
- University Of California, The Regents Of
- Patent Classifications (CPCs):
-
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- DOE Contract Number:
- W-7405-ENG-36
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE
Citation Formats
Asay, Blaine W., Henson, Bryan F., Sander, Robert K., Robinson, Jeanne M., Son, Steven F., and Dickson, Peter M. Method for monitoring the crystallization of an organic material from a liquid. United States: N. p., 2004.
Web.
Asay, Blaine W., Henson, Bryan F., Sander, Robert K., Robinson, Jeanne M., Son, Steven F., & Dickson, Peter M. Method for monitoring the crystallization of an organic material from a liquid. United States.
Asay, Blaine W., Henson, Bryan F., Sander, Robert K., Robinson, Jeanne M., Son, Steven F., and Dickson, Peter M. Tue .
"Method for monitoring the crystallization of an organic material from a liquid". United States. https://www.osti.gov/servlets/purl/1175063.
@article{osti_1175063,
title = {Method for monitoring the crystallization of an organic material from a liquid},
author = {Asay, Blaine W. and Henson, Bryan F. and Sander, Robert K. and Robinson, Jeanne M. and Son, Steven F. and Dickson, Peter M.},
abstractNote = {Method for monitoring the crystallization of at least one organic material from a liquid. According to the method, a liquid having at least one organic material capable of existing in at least one non-centrosymmetric phase is prepared. The liquid is interrogated with a laser beam at a chosen wavelength. As at least a portion of the at least one organic material crystallizes from the liquid, the intensity of any light scattered by the crystallized material at a wavelength equal to one-half the chosen wavelength of the interrogating laser beam is monitored. If the intensity of this scattered light, increases, then the crystals that form include at least one non-cetrosymmetric phase.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2004},
month = {10}
}
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.
Works referenced in this record:
The applicability of second harmonic generation for in situ measurement of induction time of selected crystallization systems
journal, June 1999
- LeCaptain, Dale J.; Berglund, Kris A.
- Journal of Crystal Growth, Vol. 203, Issue 4
Polymorphs of Tamoxifen Citrate: Detailed Structural Characterization of the Stable Form
journal, March 1987
- Goldberg, Israel; Becker, Yigal
- Journal of Pharmaceutical Sciences, Vol. 76, Issue 3
Quantitative Measurements of Multilayer Physical Adsorption on Heterogeneous Surfaces from Nonlinear Light Scattering
journal, August 1997
- Henson, B. F.; Wilson, K. R.; Robinson, J. M.
- Physical Review Letters, Vol. 79, Issue 8
Dynamic Observation of a Thermally Activated Structure Change in 1,3,5-Triamino-2,4,6-trinitrobenzene (TATB) by Second Harmonic Generation
journal, July 1999
- Son, S. F.; Asay, B. W.; Henson, B. F.
- The Journal of Physical Chemistry B, Vol. 103, Issue 26
Application of solid-phase transition kinetics to the properties of HMX
journal, February 1983
- Karpowicz, R. J.; Gelfand, L. S.; Brill, T. B.
- AIAA Journal, Vol. 21, Issue 2
Dynamic Measurement of the HMX - Phase Transition by Second Harmonic Generation
journal, February 1999
- Henson, B. F.; Asay, B. W.; Sander, R. K.
- Physical Review Letters, Vol. 82, Issue 6