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Title: Screening combinatorial arrays of inorganic materials with spectroscopy or microscopy

Abstract

Methods and apparatus for the preparation and use of a substrate having an array of diverse materials in predefined regions thereon. A substrate having an array of diverse materials thereon is generally prepared by delivering components of materials to predefined regions on a substrate, and simultaneously reacting the components to form at least two materials. Materials which can be prepared using the methods and apparatus of the present invention include, for example, covalent network solids, ionic solids and molecular solids. More particularly, materials which can be prepared using the methods and apparatus of the present invention include, for example, inorganic materials, intermetallic materials, metal alloys, ceramic materials, organic materials, organometallic materials, non-biological organic polymers, composite materials (e.g., inorganic composites, organic composites, or combinations thereof), etc. Once prepared, these materials can be screened for useful properties including, for example, electrical, thermal, mechanical, morphological, optical, magnetic, chemical, or other properties. Thus, the present invention provides methods for the parallel synthesis and analysis of novel materials having useful properties.

Inventors:
; ;
Issue Date:
Research Org.:
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1174713
Patent Number(s):
6686205
Application Number:
09/728,202
Assignee:
Lawrence Berkeley National Laboratory (Berkeley, CA)
Patent Classifications (CPCs):
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01F - MAGNETS
DOE Contract Number:  
AC03-76SF00098
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE

Citation Formats

Schultz, Peter G., Xiang, Xiaodong, and Goldwasser, Isy. Screening combinatorial arrays of inorganic materials with spectroscopy or microscopy. United States: N. p., 2004. Web.
Schultz, Peter G., Xiang, Xiaodong, & Goldwasser, Isy. Screening combinatorial arrays of inorganic materials with spectroscopy or microscopy. United States.
Schultz, Peter G., Xiang, Xiaodong, and Goldwasser, Isy. Tue . "Screening combinatorial arrays of inorganic materials with spectroscopy or microscopy". United States. https://www.osti.gov/servlets/purl/1174713.
@article{osti_1174713,
title = {Screening combinatorial arrays of inorganic materials with spectroscopy or microscopy},
author = {Schultz, Peter G. and Xiang, Xiaodong and Goldwasser, Isy},
abstractNote = {Methods and apparatus for the preparation and use of a substrate having an array of diverse materials in predefined regions thereon. A substrate having an array of diverse materials thereon is generally prepared by delivering components of materials to predefined regions on a substrate, and simultaneously reacting the components to form at least two materials. Materials which can be prepared using the methods and apparatus of the present invention include, for example, covalent network solids, ionic solids and molecular solids. More particularly, materials which can be prepared using the methods and apparatus of the present invention include, for example, inorganic materials, intermetallic materials, metal alloys, ceramic materials, organic materials, organometallic materials, non-biological organic polymers, composite materials (e.g., inorganic composites, organic composites, or combinations thereof), etc. Once prepared, these materials can be screened for useful properties including, for example, electrical, thermal, mechanical, morphological, optical, magnetic, chemical, or other properties. Thus, the present invention provides methods for the parallel synthesis and analysis of novel materials having useful properties.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2004},
month = {2}
}

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Works referenced in this record:

La-Eu Cuprates as Catalysts for Phenol Oxidation
journal, January 1994


Generation and screening of an oligonucleotide-encoded synthetic peptide library.
journal, November 1993


A design for a combined infrared cell/differential single-pass reactor
journal, September 1979


A New High- T c Oxide Superconductor without a Rare Earth Element
journal, February 1988


Isomerization and hydrolysis reactions of important disaccharides over inorganic heterogeneous catalysts
journal, November 1985


Compositional Determination of rf Co-Sputtered Multicomponent Systems
journal, January 1971


Applications of Combinatorial Technologies to Drug Discovery. 1. Background and Peptide Combinatorial Libraries
journal, April 1994


Solid-State Chemistry: A A Rediscovered Chemical Frontier
journal, February 1990


A simple-design high vacuum infrared cell for in situ studies of supported metal catalysts
journal, November 1981


Purification and crystallization of components of the protein-synthesizing system from Thermus thermophilus
journal, March 1991


The effect of solvent on the styrene-acrylonitrile copolymerization
journal, April 1992


In-situ Fourier transform infrared studies of reaction mechanisms in heterogeneous catalysis
conference, November 1990


Combinatorial Organic Synthesis Using Parke-Davis's DIVERSOMER Method
journal, January 1996


Sciencescope
journal, December 1991


High-pressure study of the new Y-Ba-Cu-O superconducting compound system
journal, March 1987


Silver, sodium halosodalites: class A sodalites
journal, June 1992


Complex synthetic chemical libraries indexed with molecular tags
journal, December 1993


Chemistry of High-Temperature Superconductors
journal, December 1988


The Current Status of Heterocyclic Combinatorial Libraries
journal, April 1997


Introduction:  Combinatorial Chemistry
journal, April 1997


Multisample thermoluminescence reading
journal, September 1980


Surface Analysis with FT-IR Emission Spectroscopy
journal, May 1992


Improving the cooperation of co-catalysts by locating them on different units of a copolymer
journal, December 1992


Spatially resolved characterization of HgCdTe materials and devices by scanning laser microscopy
journal, June 1993


The effect of grain size on the superconducting transition temperature of the transition metals
journal, October 1969


Searching for peptide ligands with an epitope library
journal, July 1990


The “One-Bead-One-Compound” Combinatorial Library Method
journal, April 1997


A surface spectroscopic study of molybdenum-alumina catalysts using x-ray photoelectron, ion-scattering, and Raman spectroscopies
journal, October 1980


An efficient navigational aid for road travel
journal, January 1989


Ethanol to gasoline process: effect of variables, mechanism, and kinetics
journal, April 1985


Strategies for epitope analysis using peptide synthesis
journal, September 1987


Possible highT c superconductivity in the Ba?La?Cu?O system
journal, June 1986


Calculation of composition of dilute cosputtered multicomponent films
journal, November 1973


Design, Synthesis, and Evaluation of Small-Molecule Libraries
journal, January 1996


Peptides on phage: a vast library of peptides for identifying ligands
journal, August 1990


An Improved Single-Pellet Reactor to Study the Interaction of Kinetics with Mass Transfer Effects in Heterogeneous Catalysis
journal, November 1972


Characterization of highly dealuminated faujasite-type zeolites: ultrastable zeolite Y and ZSM-20
journal, September 1993


Synthesis, Characterization, and Catalytic Properties of Metallo-Titanium Silicate Molecular Sieves with MEL Topology
journal, January 1994


Crystallization and preliminary characterization of mitogillin, a ribosomal ribonuclease from Aspergillus restrictus
journal, April 1991


Two approaches to the rapid screening of crystallization conditions
journal, August 1992


Infrared photoluminescence characterization of long-wavelength HgCdTe detector materials
journal, June 1993


Intermetallics for permanent magnets
journal, November 1993


Selectivity over unifunctional multicomponent catalysts with non-uniform distribution of components
journal, February 1985


Infrared Thermographic Screening of Combinatorial Libraries of Heterogeneous Catalysts
journal, January 1996


Guest Editorial
journal, January 1996


Generation and use of synthetic peptide combinatorial libraries for basic research and drug discovery
journal, November 1991


Characterization and deactivation of NiOThO2 catalysts
journal, March 1989


A fully programmable system for the study of catalytic gas reactions
journal, October 1985


Low temperature linear magnetic field sensor based on magnetoresistance of the perovskite oxide La–Sr–Co–O
journal, April 1995


Isomerization of Meta-Xylene Over Pentasil-Type Microporous Gallosilicates
journal, April 1992


Nucleic Acid Selection and the Challenge of Combinatorial Chemistry
journal, April 1997


DTA apparatus as a catalytic microreactor with on-line analysis of the products
journal, June 1989


Phage Display
journal, April 1997


A multifunctional in situ catalyst characterization apparatus
journal, January 1985


Crystallization of ribozymes and small RNA motifs by a sparse matrix approach.
journal, August 1993


At the crossroads of chemistry and immunology: catalytic antibodies
journal, May 1991


A stable catalyst for heavy oil processing
journal, June 1991


Dynamic measurements of the electrical conductivity of a non-metallic catalyst during adsorption and catalysis
journal, December 1979


Light-directed, spatially addressable parallel chemical synthesis
journal, February 1991


Organic Synthesis on Soluble Polymer Supports:  Liquid-Phase Methodologies
journal, April 1997


Four-reactor apparatus for chromatographic studies of catalysts and sorbents
journal, July 1982


Applications of Combinatorial Technologies to Drug Discovery. 2. Combinatorial Organic Synthesis, Library Screening Strategies, and Future Directions
journal, May 1994


In vitro selection of RNA molecules that bind specific ligands
journal, August 1990


The design and construction of a multichannel microreactor for catalyst evaluation
journal, January 1986


The thermal behavior of crystalline aluminosilicate catalysts
journal, January 1968


Statistical design of experiments for protein crystal growth and the use of a precrystallization assay
journal, July 1988


Lessons from the Immune System:  From Catalysis to Materials Science
journal, January 1996


Electroluminescence in ZnS: Mn x : Cu y rf–Sputtered Films
journal, January 1974


Catalytic antibodies
journal, December 1986


Local gas sampling and surface hydrogen detection in catalysis on planar surfaces
journal, January 1991


A Comparison of Some Catalytic Properties of Unsupported MOS2 and WS2 Catalysts Promoted by Group VIII Metals
journal, January 1984


Magnetoresistance in Metallic Crystals of La 1- x Sr x CoO 3
journal, June 1995


Selective chemical catalysis by an antibody
journal, December 1986


Spatially Addressable Combinatorial Libraries
journal, April 1997


Integrated enzyme reactor/detector for the determination of multiple substrates by image analysis
journal, September 1993


Multiple-Component Condensation Strategies for Combinatorial Library Synthesis
journal, January 1996


Acid-base properties of silica-aluminas: use of 1-butanol dehydration as a test reaction
journal, January 1991


Automated protein crystallization and a new crystal form of a subtilisin:eglin complex
journal, January 1987


Standing temperature waves on electrically heated catalytic ribbons
journal, January 1989


Assembly of combinatorial antibody libraries on phage surfaces: the gene III site.
journal, September 1991


Strategy and Tactics in Combinatorial Organic Synthesis. Applications to Drug Discovery
journal, January 1996


Surface reactions of alkanes and organometallic chemistry applied to the study of pure and bimetallic catalysts
journal, November 1989


Carbon monoxide hydrogenation over Fe/HZSM-5 catalysts. Effect of SiO2/Al2O3 zeolite ratio
journal, March 1993


IR Emission Analysis of Temperature Profiles in Pt/SiO2 Catalysts during Exothermic Reactions
journal, October 1987


Micro vials on a silicon wafer for sample introduction in capillary electrophoresis
journal, December 1992


Magnetic compounds wtth perovskite structure III. ferromagnetic compounds of cobalt
journal, January 1953


Evaluation of peptide libraries: An iterative strategy to analyze the reactivity of peptide mixtures with antibodies
journal, November 1992


Infrared Study of CO Oxidation over Pt-Rh/Al2O3 Catalysts
journal, July 1993


固定化金属錯体の有機合成への応用
journal, January 1978


Organometallics derived (Pd + Ln)/SiO2 catalysts for the reactions of synthesis gas conversion
journal, March 1994


In Vitro Selection of Catalytic Polynucleotides
journal, April 1997


Simple method for the simultaneous evaluation of combustion and selective oxidation catalysts
journal, January 1993


Synchrony and the emergence of chaos in oscillations on supported catalysts
journal, January 1990


Combinatorial chemistry
journal, September 1996


Unattended, robotic drug-release testing of enterically coated aspirin
journal, August 1986


In situ infrared measurements during hot filament CVD of diamond in a rotating substrate reactor
journal, April 1996


The combinatorial synthesis and chemical and biological evaluation of a 1,4-benzodiazepine library.
journal, May 1994


Two-dimensional crystallization of a bacterial surface protein on lipid vesicles under controlled conditions
journal, January 1992


Thousandfold Change in Resistivity in Magnetoresistive La-Ca-Mn-O Films
journal, April 1994


Synthesis of nanocomposites: Organoceramics
journal, September 1992


Random peptide libraries: a source of specific protein binding molecules
journal, July 1990


Superconductivity at 93 K in a new mixed-phase Y-Ba-Cu-O compound system at ambient pressure
journal, March 1987


In situ study of catalysts
journal, January 1988


A new type of synthetic peptide library for identifying ligand-binding activity
journal, November 1991


Radio‐Frequency‐Sputtered Films of β‐Tungsten Structure Compounds
journal, November 1970


A Class of Cobalt Oxide Magnetoresistance Materials Discovered with Combinatorial Synthesis
journal, October 1995


Photochemical Preparation of a Film-Based Catalyst with Spatial Control
journal, March 1994