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Title: Method for high resolution magnetic resonance analysis using magic angle technique

Abstract

A method of performing a magnetic resonance analysis of a biological object that includes placing the biological object in a main magnetic field and in a radio frequency field, the main magnetic field having a static field direction; rotating the biological object at a rotational frequency of less than about 100 Hz around an axis positioned at an angle of about 54.degree.44' relative to the main magnetic static field direction; pulsing the radio frequency to provide a sequence that includes a magic angle turning pulse segment; and collecting data generated by the pulsed radio frequency. According to another embodiment, the radio frequency is pulsed to provide a sequence capable of producing a spectrum that is substantially free of spinning sideband peaks.

Inventors:
;
Issue Date:
Research Org.:
Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1174598
Patent Number(s):
6653832
Application Number:
09/803,381
Assignee:
Battelle Memorial Institute (Richland, WA)
Patent Classifications (CPCs):
G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES
DOE Contract Number:  
AC06-76RL01830
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY

Citation Formats

Wind, Robert A., and Hu, Jian Zhi. Method for high resolution magnetic resonance analysis using magic angle technique. United States: N. p., 2003. Web.
Wind, Robert A., & Hu, Jian Zhi. Method for high resolution magnetic resonance analysis using magic angle technique. United States.
Wind, Robert A., and Hu, Jian Zhi. Tue . "Method for high resolution magnetic resonance analysis using magic angle technique". United States. https://www.osti.gov/servlets/purl/1174598.
@article{osti_1174598,
title = {Method for high resolution magnetic resonance analysis using magic angle technique},
author = {Wind, Robert A. and Hu, Jian Zhi},
abstractNote = {A method of performing a magnetic resonance analysis of a biological object that includes placing the biological object in a main magnetic field and in a radio frequency field, the main magnetic field having a static field direction; rotating the biological object at a rotational frequency of less than about 100 Hz around an axis positioned at an angle of about 54.degree.44' relative to the main magnetic static field direction; pulsing the radio frequency to provide a sequence that includes a magic angle turning pulse segment; and collecting data generated by the pulsed radio frequency. According to another embodiment, the radio frequency is pulsed to provide a sequence capable of producing a spectrum that is substantially free of spinning sideband peaks.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2003},
month = {11}
}

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Works referenced in this record:

Two-Dimensional Sideband Separation in Magic-Angle-Spinning NMR
journal, July 1995


High-resolution chemical shift and chemical shift anisotropy correlation in solids using slow magic angle spinning
journal, October 1992


Fluorine-19 Solid-State NMR Magic-Angle-Turning Experiments Using Multiple-Pulse Homonuclear Decoupling
journal, June 1999


Magic-Angle-Turning Experiments for Measuring Chemical-Shift-Tensor Principal Values in Powdered Solids
journal, April 1995


Gradient, high-resolution, magic angle spinning1H nuclear magnetic resonance spectroscopy of intact cells
journal, March 1998


Nuclear magnetic resonance in a rotating magnetic field
journal, March 1968


Low-speed magic-angle-spinning carbon-13 NMR of fruit tissue
journal, September 1992


A sensitive, high resolution magic angle turning experiment for measuring chemical shift tensor principal values
journal, December 1998


Selective excitation in Fourier transform nuclear magnetic resonance
journal, March 1978


An investigation of rat mammary healthy and R3230AC tumor tissues and cells by means of solid-state 13C NMR
journal, December 1996


Quantitative neuropathology by high resolution magic angle spinning proton magnetic resonance spectroscopy
journal, June 1997


Improvements to the magic angle hopping experiment
journal, October 1993


High-resolution1H NMR spectroscopy in rat liver using magic angle turning at a 1 Hz spinning rate
journal, April 2002


An Isotropic Chemical Shift-Chemical Shift Anisotropy Magic-Angle Slow-Spinning 2D NMR Experiment
journal, October 1993


Correlation of isotropic shifts and chemical shift anisotropies by two-dimensional fourier-transform magic-angle hopping nmr spectroscopy
journal, March 1983