Methods for pretreating biomass

Balan, Venkatesh; Dale, Bruce E; Chundawat, Shishir; Sousa, Leonardo

Title: Methods for pretreating biomass

Abstract

A method of alkaline pretreatment of biomass, in particular, pretreating biomass with gaseous ammonia.

Inventors:: Balan, Venkatesh; Dale, Bruce E; Chundawat, Shishir; Sousa, Leonardo

Issue Date:: 2015-03-03

Research Org.:: Michigan State Univ., East Lansing, MI (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1171703

Patent Number(s):: 8968515

Application Number:: 12/976,344

Assignee:: Board of Trustees of Michigan State University (East Lansing, MI)

Patent Classifications (CPCs):: C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08B - POLYSACCHARIDES

C - CHEMISTRY C12 - BIOCHEMISTRY C12P - FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE {

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C - CHEMISTRY C08 - ORGANIC MACROMOLECULAR COMPOUNDS C08B - POLYSACCHARIDES
C08B1/003 - {Preparation of cellulose solutions, i.e. dopes, with different possible solvents, e.g. ionic liquids

C - CHEMISTRY C12 - BIOCHEMISTRY C12P - FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE {
C12P19/02 - Monosaccharides
C12P19/14 - produced by the action of a carbohydrase {
C12P2201/00 - Pretreatment of cellulosic or lignocellulosic material for subsequent enzymatic treatment or hydrolysis
C12P7/10 - substrate containing cellulosic material

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E50/10 - Biofuels

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02P - CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
Y02P30/20 - Bio-feedstock

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DOE Contract Number:: XCO-3-33033-01

Resource Type:: Patent

Resource Relation:: Patent File Date: 2010 Dec 22

Country of Publication:: United States

Language:: English

Subject:: 09 BIOMASS FUELS

Citation Formats


                    Balan, Venkatesh, Dale, Bruce E, Chundawat, Shishir, and Sousa, Leonardo. Methods for pretreating biomass.  United States: N. p., 2015. 
        Web.

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                    Balan, Venkatesh, Dale, Bruce E, Chundawat, Shishir, & Sousa, Leonardo. Methods for pretreating biomass.  United States.

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                    Balan, Venkatesh, Dale, Bruce E, Chundawat, Shishir, and Sousa, Leonardo. Tue .  
        "Methods for pretreating biomass".  United States.  https://www.osti.gov/servlets/purl/1171703.

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@article{osti_1171703,

  title        = {Methods for pretreating biomass},

  author       = {Balan, Venkatesh and Dale, Bruce E and Chundawat, Shishir and Sousa, Leonardo},

  abstractNote = {A method of alkaline pretreatment of biomass, in particular, pretreating biomass with gaseous ammonia.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2015},

  month        = {3}

}

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Ferrer, Alexis; Byers, Floyd M.; Sulbarán-de-Ferrer, Betzabé
Twenty-First Symposium on Biotechnology for Fuels and Chemicals
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Fiorentini, R.; Galoppini, C.
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Enzymatic Hydrolysis of Ammonia-Treated Sugar Beet Pulp
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Applied Biochemistry and Biotechnology, Vol. 91-93, Issue 1-9
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A Review of Solid Materials as Alternative Ammonia Sources for Lean NOx Reduction with SCR
conference, April 2009

Fulks, Gary; Fisher, Galen B.; Rahmoeller, Ken
SAE World Congress & Exhibition, SAE Technical Paper Series
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Mixture optimization of six core glycosyl hydrolases for maximizing saccharification of ammonia fiber expansion (AFEX) pretreated corn stover
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Gao, Dahai; Chundawat, Shishir P. S.; Krishnan, Chandraraj
Bioresource Technology, Vol. 101, Issue 8, p. 2770-2781
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Bioethanol
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Gray, Kevin A.; Zhao, Lishan; Emptage, Mark
Current Opinion in Chemical Biology, Vol. 10, Issue 2, p. 141-146
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Bio-ethanol – the fuel of tomorrow from the residues of today
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Hahn-Hägerdal, B.; Galbe, M.; Gorwa-Grauslund, M. F.
Trends in Biotechnology, Vol. 24, Issue 12, p. 549-556
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Separation of Glucose and Pentose Sugars by Selective Enzyme Hydrolysis of AFEX-Treated Corn Fiber
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Hanchar, Robert J.; Teymouri, Farzaneh; Nielson, Chandra D.
Applied Biochemistry and Biotecnology
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The ammonia freeze explosion (AFEX) process: A practical lignocellulose pretreatment
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Holtzapple, Mark T.; Jun, Jae-Hoon; Ashok, Ganesh
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Fungal Upgrading of Wheat Straw for Straw-Thermoplastics Production
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Houghton, Tracy P.; Thompson, David N.; Hess, J. Richard
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Bio-technologies of Recycling Agro-industrial Wastes for the Production of Commercially Important Fungal Polysaccharides and Mushrooms
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Biotechnology and Genetic Engineering Reviews, Vol. 20, Issue 1
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Cellulose, Vol. 13, Issue 3
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Two-step SSCF to convert AFEX-treated switchgrass to ethanol using commercial enzymes and Saccharomyces cerevisiae 424A(LNH-ST)
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Jin, Mingjie; Lau, Ming W.; Balan, Venkatesh
Bioresource Technology, Vol. 101, Issue 21, p. 8171-8178
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Kamm, B.; Kamm, M.
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Microbial Pretreatment of Biomass: Potential for Reducing Severity of Thermochemical Biomass Pretreatment
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Enhancement of the Enzymatic Digestibility of Waste Newspaper Using Tween
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Kim, Sung Bae; Kim, Hyun Joo; Kim, Chang Joon
Twenty-Seventh Symposium on Biotechnology for Fuels and Chemicals
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Lime pretreatment and enzymatic hydrolysis of corn stover
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Kim, Sehoon; Holtzapple, Mark T.
Bioresource Technology, Vol. 96, Issue 18, p. 1994-2006
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Pretreatment and fractionation of corn stover by ammonia recycle percolation process
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Kim, Tae Hyun; Lee, Yoon Y.
Bioresource Technology, Vol. 96, Issue 18, p. 2007-2013
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Pretreatment of Corn Stover by Low-Liquid Ammonia Recycle Percolation Process
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Kim, Tae Hyun; Lee, Yoon Y.; Sunwoo, Changshin
Applied Biochemistry and Biotechnology, Vol. 133, Issue 1, p. 41-58
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Does densification influence the steam pretreatment and enzymatic hydrolysis of softwoods to sugars?
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Kumar, Linoj; Tooyserkani, Zahra; Sokhansanj, Shahab
Bioresource Technology, Vol. 121, p. 190-198
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Cellulosic ethanol production from AFEX-treated corn stover using Saccharomyces cerevisiae 424A(LNH-ST)
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Proceedings of the National Academy of Sciences, Vol. 106, Issue 5, p. 1368-1373
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Comparing the fermentation performance of Escherichia coli KO11, Saccharomyces cerevisiae 424A(LNH-ST) and Zymomonas mobilis AX101 for cellulosic ethanol production
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Lau, Ming W.; Gunawan, Christa; Balan, Venkatesh
Biotechnology for Biofuels, Vol. 3, Issue 1
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The impacts of pretreatment on the fermentability of pretreated lignocellulosic biomass: a comparative evaluation between ammonia fiber expansion and dilute acid pretreatment
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Lau, Ming W.; Gunawan, Christa; Dale, Bruce E.
Biotechnology for Biofuels, Vol. 2, Issue 1
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Understanding Factors that Limit Enzymatic Hydrolysis of Biomass: Characterization of Pretreated Corn Stover
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Applied Biochemistry and Biotechnology, Vol. 124, Issue 1-3
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Ethanol fermentation from biomass resources: current state and prospects
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Lin, Yan; Tanaka, Shuzo
Applied Microbiology and Biotechnology, Vol. 69, Issue 6
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Partial flow of compressed-hot water through corn stover to enhance hemicellulose sugar recovery and enzymatic digestibility of cellulose
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Liu, Chaogang; Wyman, Charles E.
Bioresource Technology, Vol. 96, Issue 18, p. 1978-1985
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Combined sugar yields for dilute sulfuric acid pretreatment of corn stover followed by enzymatic hydrolysis of the remaining solids
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Lloyd, Todd A.; Wyman, Charles E.
Bioresource Technology, Vol. 96, Issue 18, p. 1967-1977
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Lovrien, Rex; Matulis, Daumantas; Coligan, John E.
Current Protocols in Protein Science
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Cellulase Adsorption and an Evaluation of Enzyme Recycle During Hydrolysis of Steam-Exploded Softwood Residues
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Lu, Yanpin; Yang, Bin; Gregg, David
Applied Biochemistry and Biotechnology, Vol. 98-100, Issue 1-9
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Cutting Frequency and Nitrogen Fertilization Effects on Yield and Nitrogen Concentration of Switchgrass in a Short Season Area
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Madakadze, I. C.; Stewart, K. A.; Peterson, P. R.
Crop Science, Vol. 39, Issue 2
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Economics of Producing fuel Pellets from Biomass
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Applied Engineering in Agriculture, Vol. 22, Issue 3
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Cooperative and Competitive Binding in Synergistic Mixtures of Thermobifida fusca Cellulases Cel5A, Cel6B, and Cel9A
journal, August 2002

Jeoh, T.; Wilson, D. B.; Walker, L. P.
Biotechnology Progress, Vol. 18, Issue 4
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A novel integrated biological process for cellulosic ethanol production featuring high ethanol productivity, enzyme recycling and yeast cells reuse
journal, January 2012

Jin, Mingjie; Gunawan, Christa; Uppugundla, Nirmal
Energy & Environmental Science, Vol. 5, Issue 5
https://doi.org/10.1039/C2EE03058F

Method of removing ammonia from ammonia containing liquor
patent, November 1975

Schroeder, James; Naso, Anthony
US Patent Document 3,920,419
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Process for the production of ammoniated straw and other plant materials containing lignocellulose
patent, December 1977

Conradsen, Arne; Lie, Ole Hannibal
US Patent Document 4,064,276
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Ammonia absorber
patent, May 1979

Fischer, William A.
US Patent Document 4,153,435
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Method of making compost and spawned compost, mushroom spawn and generating methane gas
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Stoller, Benjamin B.
US Patent Document 4,263,744
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Separation of ammonia from ammonia containing gases
patent, September 1981

Scheibel, Edward G.
US Patent Document 4,287,162
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Process for treating alfalfa and other cellulosic agricultural crops
patent, October 1982

Hultquist, Joe H.
US Patent Document 4,356,196
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Process for enriching the protein content of food and feedstuff and products thereof
patent, January 1983

Harper, James L.
US Patent Document 4,370,351
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4370351

Method for increasing the accessibility of cellulose in lignocellulosic materials, particularly hardwoods agricultural residues and the like
patent, July 1984

Foody, Patrick J.
US Patent Document 4,461,648
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4461648

Bioconversion of agricultural wastes into proteinaceous animal feed
patent, July 1985

Young, Murray M.
US Patent Document 4,526,791
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4526791

Process for separating carbonic acid gas from methane-rich gas
patent, April 1986

Uno, Masaru; Ihara, Satoshi; Tanabe, Takeo
US Patent Document 4,581,044
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4581044

Apparatus for treating cellulose-containing matter, e.g. straw, with gaseous ammonia
patent, May 1986

Andersen, Arne
US Patent Document 4,589,334
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4589334

Process for removing ammonia and acid gases from process streams
patent, June 1986

Maier, Edward E.
US Patent Document 4,594,131
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4594131

Method for increasing the reactivity and digestibility of cellulose with ammonia
patent, July 1986

Dale, Bruce E.
US Patent Document 4,600,590
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4600590

Process for recovery of protein from agricultural commodities prior to alcohol production
patent, November 1986

Lawhon, James T.
US Patent Document 4,624,805
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4624805

Supercritical ammonia treatment of lignocellulosic materials
patent, February 1987

Chou, Yu-Chia T.
US Patent Document 4,644,060
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4644060

Composting process for the production of mushroom cultivation substrates
patent, July 1989

Dunn-Coleman, Nigel; Michaels, Thomas J.
US Patent Document 4,848,026
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4848026

Process for separating and recovering carbonic acid gas from gas mixture by adsorption
patent, January 1991

Uno, Masaru; Ueda, Kanji; Inoue, Masahiro
US Patent Document 4,986,835
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4986835

Separation of gas from solvent by membrane technology
patent, February 1991

Beaupre, Richard F.; Jung, Dick Y.
US Patent Document 4,995,888
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4995888

Continuous constant pressure staging of solid-vapor compound reactors
patent, June 1991

Rockenfeller, Uwe; Kirol, Lance D.
US Patent Document 5,025,635
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5025635

Process for increasing the reactivity of cellulose-containing materials
patent, August 1991

Dale, Bruce E.
US Patent Document 5,037,663
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5037663

Integrated process for the production of food, feed and fuel from biomass
patent, September 1991

Chahal, Devinder S.
US Patent Document 5,047,332
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5047332

Ammonia recovery from purge gas
patent, May 1992

Grotz, Bernard J.
US Patent Document 5,114,694
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5114694

Biomass refining process
patent, December 1992

Holtzapple, Mark T.; Davison, Richard; Stuart, Earnest
US Patent Document 5,171,592
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5171592

Treatment of fibrous lignocellulosic biomass by high shear forces in a turbulent couette flow to make the biomass more susceptible to hydrolysis
patent, December 1994

Stuart, Earnest
US Patent Document 5,370,999
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5370999

Process for the treatment of cellulose
patent, December 1995

Bredereck, Karl; Karstens, Ties; Lentz, Harro
US Patent Document 5,473,061
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5473061

Process for separating selected components from multi-component natural gas streams
patent, August 1997

Elliot, Douglas G.; Chen, Jong Juh
US Patent Document 5,660,603
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5660603

Stabilization of biowastes
patent, April 1998

Cox, James P.; Cox, Robert W. Duffy
US Patent Document 5,736,032
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Methods of biomass pretreatment
patent, February 1999

Holtzapple, Mark T.; Davison, Richard
US Patent Document 5,865,898
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5865898

Process for activating polysaccharides, polysaccharides produced by this process, and use thereof
patent, August 1999

Karstens, Ties; Steinmeier, Hans
US Patent Document 5,939,544
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5939544

Method for removing ammonia and carbon dioxide gases from a steam
patent, February 2000

Ruck, Donald Neal; Lines, James Richard; Athey, Roderick E.
US Patent Document 6,027,552
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Process for Recovering Carbon Dioxide from a Gas Mixture
patent, October 1935

Vosburgh, Charles H.
US Patent Document 2,017,779
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Process for treating cellulosic materials
patent, August 2000

Dale, Bruce E.; Weaver, Justin K.
US Patent Document 6,106,888
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Adsorption Process and Apparatus
patent, April 1951

Berg, Clyde H. O.
US Patent Document 2,548,192
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Separation of Gas Mixtures Utilizing Plural Sorbent Zones in Series and Parallel
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Urban, Peter
US Patent Document 3,306,006
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Recovery method of ammonia from gaseous mixture
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Umino, Hiroshi; Chikamatsu, Nobuyasu; Ito, Hirofumi
US Patent Document 6,585,807
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Cellulose production from lignocellulosic biomass
patent, September 2003

Wingerson, Richard C.
US Patent Document 6,620,292
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Apparatus for treating cellulosic materials
patent, January 2001

Dale, Bruce E.; Weaver, Justin K.
US Patent Document 6,176,176
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Microbial polyunsaturated fatty acid containing oil from pasteurised biomass
patent, July 2001

Bijl, Hendrik Louis; Wolf, Johannes Hendrik; Schaap, Albert
US Patent Document 6,255,505
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Apparatus, process and pressure reactor for the treatment of solids with pressurized liquid gases
patent, July 2002

Karstens, Ties
US Patent Document 6,416,621
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6416621

Process for the production of hydrogen using a carbonated adsorbent with selected dubinin parameters
patent, July 2002

Moreau, Serge; Polster, Bernd
US Patent Document 6,425,939
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6425939

Process for the production of nutritional products with microorganisms using sequential solid substrate and liquid fermentation
patent, September 2002

Sporleder, Robert A.; Linden, James C.; Schroeder, Herbert A.
US Patent Document 6,444,437
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Recirculating composting system
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McNelly, James J.
US Patent Document 6,524,848
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Diode energy converter for chemical kinetic electron energy transfer
patent, May 2008

Zuppero, Anthony C.; Gidwani, Jawahar M.
US Patent Document 7,371,962
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7371962

Process for the production of animal feed and ethanol and novel animal feed
patent, February 2009

Abbas, Charles; Binder, Thomas P.; Beery, Kyle
US Patent Document 7,494,675
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Process for the production of cellulolytic and hemicellulolytic enzymes using distillation residues from the ethanolic fermentation of enzymatic hydrolyzates of (ligno)cellulosic materials
patent, February 2009

Warzywoda, Michel; Ballerini, Daniel; Monot, Frederic
US Patent Document 7,494,792
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7494792

Process for ammonia recovery
patent, May 2009

Benderly, Abraham; Briegel, Keith Frederick; DeCourcy, Michael Stanley
US Patent Document 7,537,744
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7537744

Recovery of inorganic salt during processing of lignocellulosic feedstocks
patent, September 2009

Foody, Brian; Tolan, Jeffrey S.; Rahme, Ziyad
US Patent Document 7,585,652
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7585652

Method of pre-treating woodchips prior to mechanical pulping
patent, August 2010

Kirov, Ventzislav H.; Sethy, Anil; Sorensen, Bryan L.
US Patent Document 7,771,565
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7771565

Integration of alternative feedstreams for biomass treatment and utilization
patent, March 2011

Hennessey, Susan Marie; Friend, Julie; Dunson, Jr., James B.
US Patent Document 7,910,338
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7910338

Method for producing water-absorbing polymer particles
patent, March 2011

Funk, Rüdiger; Schröder, Jürgen
US Patent Document 7,910,675
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7910675

Process for the treatment of lignocellulosic biomass
patent, March 2011

Dale, Bruce E.
US Patent Document 7,915,017
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7915017

Process for treatment of biomass feedstocks
patent, May 2011

Rajagopalan, Srinivasan; Tiedje, Tonya; McCalla, Darold
US Patent Document 7,937,851
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7937851

AG-wafer product and method of making same
patent, September 2011

Karpik, Joseph
US Patent Document 8,020,342
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8020342

Biomass pretreatment
patent, October 2011

Varanasi, Sasidhar; Schall, Constance Ann; Dadi, Anantharam Prasad
US Patent Document 8,030,030
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8030030

Process for producing sugars and ethanol using corn stillage
patent, February 2013

Balan, Venkatesh; Chundawat, Shishir; Sousa, Leonardo
US Patent Document 8,367,378
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8367378

Method of separating components from a gas stream
patent, March 2013

Campbell, Timothy; Teymouri, Farzaneh; Jones, David K.
US Patent Document 8,394,177
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8394177

Process for the treatment of lignocellulosic biomass
patent, March 2013

Dale, Bruce E.; Lynd, Lee R.; Laser, Mark
US Patent Document 8,394,611
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8394611

Apparatus for pretreatment for saccharification of lignocellulose biomass
patent, April 2013

Baba, Tsuyoshi; Mitsuzawa, Shigenobu
US Patent Document 8,419,900
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8419900

Lignocellulosic biomass saccharification pre-treatment device
patent, May 2013

Baba, Tsuyoshi
US Patent Document 8,444,925
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8444925

Process using agriculture residue biomass for producing feed pellets
patent, October 2013

Zeeck, James Russell
US Patent Document 8,551,549
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8551549

Anhydrous ammonia treatment for improved milling of biomass
patent, February 2014

Camp, Carl E.; Cirakovic, Jelena; Diner, Bruce A.
US Patent Document 8,651,403
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8651403

Pretreated densified biomass products
patent, March 2014

Dale, Bruce E.; Ritchie, Bryan; Marshall, Derek
US Patent Document 8,673,031
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8673031

Process for the treatment of lignocellulosic biomass
patent, July 2014

Dale, Bruce E.
US Patent Document 8,771,425
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8771425

Biomass pelletizing process
patent, September 2014

Zeeck, James Russell
US Patent Document 8,846,123
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8846123

Transgenic plants containing ligninase and cellulase which degrade lignin and cellulose to fermentable sugars
patent, May 2006

Sticklen, Masomeh B.; Dale, Bruce E.; Maqbool, Shahina B.
US Patent Document 7,049,485
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7049485

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Methods for producing and using densified biomass products containing pretreated biomass fibers

Patent Dale, Bruce E.; Ritchie, Bryan; Marshall, Derek

A process is provided comprising subjecting a quantity of plant biomass fibers to a pretreatment to cause at least a portion of lignin contained within each fiber to move to an outer surface of said fiber, wherein a quantity of pretreated tacky plant biomass fibers is produced; and densifying the quantity of pretreated tacky plant biomass fibers to produce one or more densified biomass particulates, wherein said biomass fibers are densified without using added binder.
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Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto

Patent Bals, Bryan; Teymouri, Farzaneh; Campbell, Tim; ...

A method is provided in which pretreated and densified cellulosic biomass particulates can be hydrolyzed at a high solids loading rate as compared with the solids loading rate of loose hydrolysable cellulosic biomass fibers. The resulting high concentration sugar-containing stream can be easily converted to biofuels or an entire suite of other useful bioproducts.
Full Text Available
Method for pretreating lignocellulosic biomass

Patent Kuzhiyil, Najeeb M.; Brown, Robert C.; Dalluge, Dustin Lee

The present invention relates to a method for pretreating lignocellulosic biomass containing alkali and/or alkaline earth metal (AAEM). The method comprises providing a lignocellulosic biomass containing AAEM; determining the amount of the AAEM present in the lignocellulosic biomass; identifying, based on said determining, the amount of a mineral acid sufficient to completely convert the AAEM in the lignocellulosic biomass to thermally-stable, catalytically-inert salts; and treating the lignocellulosic biomass with the identified amount of the mineral acid, wherein the treated lignocellulosic biomass contains thermally-stable, catalytically inert AAEM salts.
Full Text Available
Methods for pretreating biomass

Patent Balan, Venkatesh; Dale, Bruce E; Chundawat, Shishir; ...

A method for pretreating biomass is provided, which includes, in a reactor, allowing gaseous ammonia to condense on the biomass and react with water present in the biomass to produce pretreated biomass, wherein reactivity of polysaccharides in the biomass is increased during subsequent biological conversion as compared to the reactivity of polysaccharides in biomass which has not been pretreated. A method for pretreating biomass with a liquid ammonia and recovering the liquid ammonia is also provided. Related systems which include a biochemical or biofuel production facility are also disclosed.
Full Text Available
Methods for producing extracted and digested products from pretreated lignocellulosic biomass

Patent Chundawat, Shishir; Sousa, Leonardo Da Costa; Cheh, Albert M.; ...

Methods for producing extracted and digested products from pretreated lignocellulosic biomass are provided. The methods include converting native cellulose I.sub..beta. to cellulose III.sub.I by pretreating the lignocellulosic biomass with liquid ammonia under certain conditions, and performing extracting or digesting steps on the pretreated/converted lignocellulosic biomass.
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Title: Methods for pretreating biomass

Abstract

Citation Formats

Cocurrent downflow circulating fluidized bed (downer) reactors - A state of the art review journal, October 1995

Pretreatment of Switchgrass by Ammonia Fiber Explosion (AFEX) journal, January 2005

Process and economic analysis of pretreatment technologies journal, December 2005

In vitro and in vivo digestibility of soya-bean straw treated with various alkalis journal, August 1990

Features of promising technologies for pretreatment of lignocellulosic biomass journal, April 2005

Improving Digestibility of Straws for Ruminant Feed by Aqueous Ammonia journal, July 1972

The World Mushroom Industry: Trends and Technological Development journal, January 2006

Roll Press Briquetting and Pelleting of Corn Stover and Switchgrass journal, January 2009

Biological waste air treatment in biofilters journal, June 1997

Assessment of the influence of media particle size on the biofiltration of odorous exhaust ventilation air from a piggery facility journal, September 2002

The effect of different treatment conditions on biomass binder preparation for lignite briquette journal, November 2001

Production of Cellulase by Solid-State Fermentation book, January 1999

Production of Cellulase in Solid-State Fermentation with Trichoderma reesei MCG 80 on Wheat Straw book, January 1996

Methods for Pretreatment of Lignocellulosic Biomass for Efficient Hydrolysis and Biofuel Production journal, April 2009

Microbial Cellulose Utilization: Fundamentals and Biotechnology journal, September 2002

Advancement and comparative profiles in the production technologies using solid-state and submerged fermentation for microbial cellulases journal, June 2010

Production and characterization of cellulolytic enzymes from Trichoderma reesei grown on various carbon sources journal, January 1992

Technical and Financial Feasibility Analysis of Distributed Bioprocessing Using Regional Biomass Pre-Processing Centers journal, January 2007

Complete Rations for Dairy Cattle. II. Sugarcane Bagasse Pellets as Roughage in Blended Rations for Lactating Cows journal, June 1975

Complete Rations for Dairy Cattle. V. Interaction of Sugarcane Bagasse Quantity and Form with Soybean Meal, Urea, and Starea journal, September 1975

Replacement of fish meal in diets for Australian silver perch, Bidyanus bidyanus: I. Digestibility of alternative ingredients journal, June 2000

Lignocellulosic Biomass Pretreatment Using AFEX book, January 2009

Mushroom spent straw: a potential substrate for an ethanol-based biorefinery journal, January 2008

Variability of laccase activity in the white-rot basidiomycetePleurotus ostreatus journal, August 2002

Enzymatic Hydrolysis of Distiller's Dry Grain and Solubles (DDGS) Using Ammonia Fiber Expansion Pretreatment journal, November 2006

Leaf photosynthesis in the C 4 -grass Miscanthus x giganteus , growing in the cool temperate climate of southern England journal, January 1996

Element Concentrations of Dry-Grind Corn-Processing Streams journal, January 2006

Extractability and solubility of leaf protein journal, January 1973

Acid–base interactions and swelling of cellulose fibers in organic liquids journal, July 2005

Biotechnological processes for conversion of corn into ethanol journal, December 2004

Effect of particle size based separation of milled corn stover on AFEX pretreatment and enzymatic digestibility journal, January 2006

Multi-scale visualization and characterization of lignocellulosic plant cell wall deconstruction during thermochemical pretreatment journal, January 2011

Biotechnological applications and potential of wood-degrading mushrooms of the genus Pleurotus journal, April 2002

Deodorization of Ammonia by Coffee Grounds journal, January 2006

Evaluating the impact of ammonia fiber expansion (AFEX) pretreatment conditions on the cost of ethanol production journal, January 2011

Recent process improvements for the ammonia fiber expansion (AFEX) process and resulting reductions in minimum ethanol selling price journal, November 2008

Optimization of pH controlled liquid hot water pretreatment of corn stover journal, December 2005

Comparative study on the growth and yield of Pleurotus ostreatus mushroom on different lignocellulosic by-products journal, February 2003

Biorefinery journal, October 2003

Obtaining a protein concentrate from integral defatted sunflower flour journal, June 2001

Splitting tendency of cellulosic fibers. Part 2: Effects of fiber swelling in alkali solutions journal, March 2006

Investigation and Optimization of the Factors Influencing Sorghum Protein Extraction journal, November 2003

Liquid-vapor interfacial properties of water-ammonia mixtures: Dependence on ammonia concentration journal, November 2005

Detoxification methods of aflatoxins. A review journal, May 1995

Development of a pilot process for the production of alfalfa peptide isolate: Production of alfalfa peptide isolate journal, April 2003

The Path Forward for Biofuels and Biomaterials journal, January 2006

Enhancing Profitability of Dry Mill Ethanol Plants: Process Modeling and Economics of Conversion of Degermed Defibered Corn to Ethanol journal, January 2005

The Future of Coproducts From Corn Processing journal, January 2006

Combined effect of pelleting and pretreatment on enzymatic hydrolysis of switchgrass journal, July 2012

Increasing cellulose accessibility is more important than removing lignin: A comparison of cellulose solvent-based lignocellulose fractionation and soaking in aqueous ammonia journal, September 2010

Integrated production of ethanol fuel and protein from Coastal Bermudagrass journal, March 1994

Hemicellulose bioconversion journal, May 2003

Biodegradation of Viticulture Wastes by Pleurotus : A Source of Microbial and Human Food and Its Potential Use in Animal Feeding journal, April 2002

Switchgrass as a sustainable bioenergy crop journal, April 1996

Solid-State Fermentation of Lignocellulosic Plant Residues from Brassica napus by Pleurotus ostreatus journal, January 1999

Composting of a crop residue through treatment with microorganisms and subsequent vermicomposting journal, November 2002

Biomass Densification â€“ Cubing Operations and Costs for corn Stover journal, January 2004

Toward a Systems Approach to Understanding Plant Cell Walls journal, December 2004

Enzyme Recovery and Recycling Following Hydrolysis of Ammonia Fiber Explosion–Treated Corn Stover journal, January 2005

Cellulase production using biomass feed stock and its application in lignocellulose saccharification for bio-ethanol production journal, February 2009

Hydrolysis of lignocellulosic materials for ethanol production: a review journal, May 2002

Induction and catabolite repression mechanisms of cellulase in fungi journal, January 2001

Evaluation of pretreatment with Pleurotus ostreatus for enzymatic hydrolysis of rice straw journal, December 2005

Effects of the pelleting conditions on chemical composition and sugar yield of corn stover, big bluestem, wheat straw, and sorghum stalk pellets journal, October 2011

Leaf Protein from Ammonia-Treated Dwarf Elephant Grass (<I>Pennisetum purpureum</I> Schum cv. Mott) journal, January 2005

Complete Rations for Growing Dairy Replacements Utilizing By-Product Feedstuffs journal, September 1980

Pretreatment of Miscanthus for hydrogen production by Thermotoga elfii journal, November 2002

Cost estimates and sensitivity analyses for the ammonia fiber explosion process journal, March 1998

Fuel ethanol after 25 years journal, December 1999

An initial assessment of spent mushroom compost as a potential energy feedstock journal, September 2001

Comparative sugar recovery data from laboratory scale application of leading pretreatment technologies to corn stover journal, December 2005

Coordinated development of leading biomass pretreatment technologies journal, December 2005

Improving Accessibility and Reactivity of Celluloses of Annual Plants for the Synthesis of Methylcellulose journal, October 2005

A Transition from Cellulose Swelling to Cellulose Dissolution by o -Phosphoric Acid: Evidence from Enzymatic Hydrolysis and Supramolecular Structure journal, February 2006

Oyster mushroom cultivation with rice and wheat straw journal, May 2002

Toward an aggregated understanding of enzymatic hydrolysis of cellulose: Noncomplexed cellulase systems journal, November 2004

Optimization of enzymatic hydrolysis and ethanol fermentation from AFEX-treated rice straw journal, April 2009

Cocurrent downflow circulating fluidized bed (downer) reactors - A state of the art review
journal, October 1995

Pretreatment of Switchgrass by Ammonia Fiber Explosion (AFEX)
journal, January 2005

Process and economic analysis of pretreatment technologies
journal, December 2005

In vitro and in vivo digestibility of soya-bean straw treated with various alkalis
journal, August 1990

Features of promising technologies for pretreatment of lignocellulosic biomass
journal, April 2005

Improving Digestibility of Straws for Ruminant Feed by Aqueous Ammonia
journal, July 1972

The World Mushroom Industry: Trends and Technological Development
journal, January 2006

Roll Press Briquetting and Pelleting of Corn Stover and Switchgrass
journal, January 2009

Biological waste air treatment in biofilters
journal, June 1997

Assessment of the influence of media particle size on the biofiltration of odorous exhaust ventilation air from a piggery facility
journal, September 2002

The effect of different treatment conditions on biomass binder preparation for lignite briquette
journal, November 2001

Production of Cellulase by Solid-State Fermentation
book, January 1999

Production of Cellulase in Solid-State Fermentation with Trichoderma reesei MCG 80 on Wheat Straw
book, January 1996

Methods for Pretreatment of Lignocellulosic Biomass for Efficient Hydrolysis and Biofuel Production
journal, April 2009

Microbial Cellulose Utilization: Fundamentals and Biotechnology
journal, September 2002

Advancement and comparative profiles in the production technologies using solid-state and submerged fermentation for microbial cellulases
journal, June 2010

Production and characterization of cellulolytic enzymes from Trichoderma reesei grown on various carbon sources
journal, January 1992

Technical and Financial Feasibility Analysis of Distributed Bioprocessing Using Regional Biomass Pre-Processing Centers
journal, January 2007

Complete Rations for Dairy Cattle. II. Sugarcane Bagasse Pellets as Roughage in Blended Rations for Lactating Cows
journal, June 1975

Complete Rations for Dairy Cattle. V. Interaction of Sugarcane Bagasse Quantity and Form with Soybean Meal, Urea, and Starea
journal, September 1975

Replacement of fish meal in diets for Australian silver perch, Bidyanus bidyanus: I. Digestibility of alternative ingredients
journal, June 2000

Lignocellulosic Biomass Pretreatment Using AFEX
book, January 2009

Mushroom spent straw: a potential substrate for an ethanol-based biorefinery
journal, January 2008

Variability of laccase activity in the white-rot basidiomycetePleurotus ostreatus
journal, August 2002

Enzymatic Hydrolysis of Distiller's Dry Grain and Solubles (DDGS) Using Ammonia Fiber Expansion Pretreatment
journal, November 2006

Leaf photosynthesis in the C ₄ -grass Miscanthus x giganteus , growing in the cool temperate climate of southern England
journal, January 1996

Element Concentrations of Dry-Grind Corn-Processing Streams
journal, January 2006

Extractability and solubility of leaf protein
journal, January 1973

Acid–base interactions and swelling of cellulose fibers in organic liquids
journal, July 2005

Biotechnological processes for conversion of corn into ethanol
journal, December 2004

Effect of particle size based separation of milled corn stover on AFEX pretreatment and enzymatic digestibility
journal, January 2006

Multi-scale visualization and characterization of lignocellulosic plant cell wall deconstruction during thermochemical pretreatment
journal, January 2011

Biotechnological applications and potential of wood-degrading mushrooms of the genus Pleurotus
journal, April 2002

Deodorization of Ammonia by Coffee Grounds
journal, January 2006

Evaluating the impact of ammonia fiber expansion (AFEX) pretreatment conditions on the cost of ethanol production
journal, January 2011

Recent process improvements for the ammonia fiber expansion (AFEX) process and resulting reductions in minimum ethanol selling price
journal, November 2008

Optimization of pH controlled liquid hot water pretreatment of corn stover
journal, December 2005

Comparative study on the growth and yield of Pleurotus ostreatus mushroom on different lignocellulosic by-products
journal, February 2003

Biorefinery
journal, October 2003

Obtaining a protein concentrate from integral defatted sunflower flour
journal, June 2001

Splitting tendency of cellulosic fibers. Part 2: Effects of fiber swelling in alkali solutions
journal, March 2006

Investigation and Optimization of the Factors Influencing Sorghum Protein Extraction
journal, November 2003

Liquid-vapor interfacial properties of water-ammonia mixtures: Dependence on ammonia concentration
journal, November 2005

Detoxification methods of aflatoxins. A review
journal, May 1995

Development of a pilot process for the production of alfalfa peptide isolate: Production of alfalfa peptide isolate
journal, April 2003

The Path Forward for Biofuels and Biomaterials
journal, January 2006

Enhancing Profitability of Dry Mill Ethanol Plants: Process Modeling and Economics of Conversion of Degermed Defibered Corn to Ethanol
journal, January 2005

The Future of Coproducts From Corn Processing
journal, January 2006

Combined effect of pelleting and pretreatment on enzymatic hydrolysis of switchgrass
journal, July 2012

Increasing cellulose accessibility is more important than removing lignin: A comparison of cellulose solvent-based lignocellulose fractionation and soaking in aqueous ammonia
journal, September 2010

Integrated production of ethanol fuel and protein from Coastal Bermudagrass
journal, March 1994

Hemicellulose bioconversion
journal, May 2003

Biodegradation of Viticulture Wastes by Pleurotus : A Source of Microbial and Human Food and Its Potential Use in Animal Feeding
journal, April 2002

Switchgrass as a sustainable bioenergy crop
journal, April 1996

Solid-State Fermentation of Lignocellulosic Plant Residues from Brassica napus by Pleurotus ostreatus
journal, January 1999

Composting of a crop residue through treatment with microorganisms and subsequent vermicomposting
journal, November 2002

Biomass Densification â€“ Cubing Operations and Costs for corn Stover
journal, January 2004

Toward a Systems Approach to Understanding Plant Cell Walls
journal, December 2004

Enzyme Recovery and Recycling Following Hydrolysis of Ammonia Fiber Explosion–Treated Corn Stover
journal, January 2005

Cellulase production using biomass feed stock and its application in lignocellulose saccharification for bio-ethanol production
journal, February 2009

Hydrolysis of lignocellulosic materials for ethanol production: a review
journal, May 2002

Induction and catabolite repression mechanisms of cellulase in fungi
journal, January 2001

Evaluation of pretreatment with Pleurotus ostreatus for enzymatic hydrolysis of rice straw
journal, December 2005

Effects of the pelleting conditions on chemical composition and sugar yield of corn stover, big bluestem, wheat straw, and sorghum stalk pellets
journal, October 2011

Leaf Protein from Ammonia-Treated Dwarf Elephant Grass (<I>Pennisetum purpureum</I> Schum cv. Mott)
journal, January 2005

Complete Rations for Growing Dairy Replacements Utilizing By-Product Feedstuffs
journal, September 1980

Pretreatment of Miscanthus for hydrogen production by Thermotoga elfii
journal, November 2002

Cost estimates and sensitivity analyses for the ammonia fiber explosion process
journal, March 1998

Fuel ethanol after 25 years
journal, December 1999

An initial assessment of spent mushroom compost as a potential energy feedstock
journal, September 2001

Comparative sugar recovery data from laboratory scale application of leading pretreatment technologies to corn stover
journal, December 2005

Coordinated development of leading biomass pretreatment technologies
journal, December 2005

Improving Accessibility and Reactivity of Celluloses of Annual Plants for the Synthesis of Methylcellulose
journal, October 2005

A Transition from Cellulose Swelling to Cellulose Dissolution by o -Phosphoric Acid: Evidence from Enzymatic Hydrolysis and Supramolecular Structure
journal, February 2006

Oyster mushroom cultivation with rice and wheat straw
journal, May 2002

Toward an aggregated understanding of enzymatic hydrolysis of cellulose: Noncomplexed cellulase systems
journal, November 2004

Optimization of enzymatic hydrolysis and ethanol fermentation from AFEX-treated rice straw
journal, April 2009

Gene Integration and Expression and Extracellular Secretion of Erwinia chrysanthemi Endoglucanase CelY (celY) and CelZ (celZ) in Ethanologenic Klebsiella oxytoca P2
journal, January 2001

Growth of the plant cell wall
journal, November 2005

Extrusion Processing for Ammonia Fiber Explosion (AFEX)
journal, January 1999