Enhanced surface sampler and process for collection and release of analytes

Title: Enhanced surface sampler and process for collection and release of analytes

Abstract

An enhanced swipe sampler and method of making are described. The swipe sampler is made of a fabric containing selected glass, metal oxide, and/or oxide-coated glass or metal fibers. Fibers are modified with silane ligands that are directly attached to the surface of the fibers to functionalize the sampling surface of the fabric. The swipe sampler collects various target analytes including explosives and other threat agents on the surface of the sampler.

Inventors:: Addleman, Raymond S; Atkinson, David A; Bays, John T; Chouyyok, Wilaiwan; Cinson, Anthony D; Ewing, Robert G; Gerasimenko, Aleksandr A

Issue Date:: 2015-02-03

Research Org.:: Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1169122

Patent Number(s):: 8,943,910

Application Number:: 13/450,343

Assignee:: Battelle Memorial Institute (Richland, WA)

DOE Contract Number:: AC05-76RL01830

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Addleman, Raymond S, Atkinson, David A, Bays, John T, Chouyyok, Wilaiwan, Cinson, Anthony D, Ewing, Robert G, and Gerasimenko, Aleksandr A. Enhanced surface sampler and process for collection and release of analytes.  United States: N. p., 2015. 
        Web.

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                    Addleman, Raymond S, Atkinson, David A, Bays, John T, Chouyyok, Wilaiwan, Cinson, Anthony D, Ewing, Robert G, & Gerasimenko, Aleksandr A. Enhanced surface sampler and process for collection and release of analytes.  United States.

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                    Addleman, Raymond S, Atkinson, David A, Bays, John T, Chouyyok, Wilaiwan, Cinson, Anthony D, Ewing, Robert G, and Gerasimenko, Aleksandr A. Tue .  
        "Enhanced surface sampler and process for collection and release of analytes".  United States.  https://www.osti.gov/servlets/purl/1169122.

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@article{osti_1169122,

  title        = {Enhanced surface sampler and process for collection and release of analytes},

  author       = {Addleman, Raymond S and Atkinson, David A and Bays, John T and Chouyyok, Wilaiwan and Cinson, Anthony D and Ewing, Robert G and Gerasimenko, Aleksandr A},

  abstractNote = {An enhanced swipe sampler and method of making are described. The swipe sampler is made of a fabric containing selected glass, metal oxide, and/or oxide-coated glass or metal fibers. Fibers are modified with silane ligands that are directly attached to the surface of the fibers to functionalize the sampling surface of the fabric. The swipe sampler collects various target analytes including explosives and other threat agents on the surface of the sampler.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2015},

  month        = {2}

}

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Similar Records

Title: Enhanced surface sampler and process for collection and release of analytes

Abstract

Citation Formats

Formation and Structure of Self-Assembled Monolayers journal, January 1996

Design and synthesis of self-assembled monolayers on mesoporous supports (SAMMS): The importance of ligand posture in functional nanomaterials journal, January 2007

LC–MS–MS Determination of Stabilizers and Explosives Residues in Hand-Swabs journal, September 2008

A method to determine collection efficiency of particles by swipe sampling journal, September 2008

Trace analysis of explosives by thermospray high-performance liquid chromatography—mass spectrometry journal, January 1986

Using Gas Chromatography with Ion Mobility Spectrometry to Resolve Explosive Compounds in the Presence of Interferents*: EXPLOSIVES DETECTION BY IMS AND GC/IMS journal, August 2010

A NIST Standard Reference Material (SRM) to Support the Detection of Trace Explosives journal, September 2009

Detection of Explosives in Hair Using Ion Mobility Spectrometry journal, May 2008

A critical review of ion mobility spectrometry for the detection of explosives and explosive related compounds journal, May 2001

Separation of Ions from Explosives in Differential Mobility Spectrometry by Vapor-Modified Drift Gas journal, September 2004

Particle Characteristics of Trace High Explosives: RDX and PETN journal, March 2007

Rapid preseparation of interferences for ion mobility spectrometry journal, March 2008

Detection of Military Explosives by Atmospheric Pressure Chemical Ionization Mass Spectrometry with Counter-Flow Introduction journal, September 2002

Fabric analysis by ambient mass spectrometry for explosives and drugs journal, January 2008

Instrumentation for trace detection of high explosives journal, August 2004

Hierarchically Structured Nanocomposite Films as Highly Sensitive Chemosensory Materials for TNT Detection journal, September 2006

Effectiveness of contamination prevention procedures in a Trace Explosives Laboratory journal, November 2007

Detection of explosives on solid surfaces by thermal desorption and ambient ion/molecule reactions journal, January 2005

Direct detection of explosives on solid surfaces by mass spectrometry with an ambient ion source based on dielectric barrier discharge journal, August 2007

Direct detection of explosives on solid surfaces by mass spectrometry with an ambient ion source based on dielectric barrier discharge journal, August 2007

Determination of nitroaromatic and nitramine explosives from a PTFE wipe using thermal desorption-gas chromatography with electron-capture detection journal, January 2005

In-Injection Port Thermal Desorption for Explosives Trace Evidence Analysis journal, October 1999

Selective sampling with direct ion mobility spectrometric detection for explosives analysis journal, October 2009

Quantitative calibration of vapor levels of TNT, RDX, and PETN using a diffusion generator with gravimetry and ion mobility spectrometry journal, December 1997

Polyester Resin-Glass Fiber Laminates journal, August 1954

Electrochemical Sensor for Detecting Ultratrace Nitroaromatic Compounds Using Mesoporous SiO 2 -Modified Electrode journal, March 2006

Adsorption of 2,4,6-trinitrotoluene on a novel adsorption material PEI/SiO2 journal, July 2009

Adsorption mechanism and property of a novel adsorption material PAM/SiO2 towards 2,4,6-trinitrotoluene journal, August 2009

Importance of Structural and Chemical Heterogeneity of Activated Carbon Surfaces for Adsorption of Dibenzothiophene journal, August 2005

Adsorption of phenolic compounds by activated carbon—a critical review journal, February 2005

Catalytic oxidation of TNT by activated carbon journal, April 2002

Dynamic adsorption of trinitrotoluene on granular activated carbon journal, January 2005

Adsorption performance and mechanism of 2,4,6-trinitrotoluene on a novel adsorption material polyvinylbenzyl acid/SiO2 journal, February 2009

Conjugated polymer-grafted silica nanoparticles for the sensitive detection of TNT journal, March 2010

Resonance Energy Transfer-Amplifying Fluorescence Quenching at the Surface of Silica Nanoparticles toward Ultrasensitive Detection of TNT journal, November 2008

A Surface Functional Monomer-Directing Strategy for Highly Dense Imprinting of TNT at Surface of Silica Nanoparticles journal, June 2007

Molecular Imprinting at Walls of Silica Nanotubes for TNT Recognition journal, January 2008

Template-Free Synthesis of Organically Modified Silica Mesoporous Thin Films for TNT Sensing journal, September 2010

Computational screening of metal–organic frameworks for large-molecule chemical sensing journal, January 2010

Processible polyaniline complexes due to molecular recognition: Supramolecular structures based on hydrogen bonding and phenyl stacking journal, January 1997

Variable-Temperature Powder X-ray Diffraction of Aromatic Carboxylic Acid and Carboxamide Cocrystals journal, April 2007

Detection of explosives by positive corona discharge ion mobility spectrometry journal, April 2010

Chemical modification of self-assembled silane based monolayers by surface reactions journal, January 2010

Chemical modification of self-assembled silane based monolayers by surface reactions journal, January 2010

Formation and Structure of Self-Assembled Monolayers
journal, January 1996

Design and synthesis of self-assembled monolayers on mesoporous supports (SAMMS): The importance of ligand posture in functional nanomaterials
journal, January 2007

LC–MS–MS Determination of Stabilizers and Explosives Residues in Hand-Swabs
journal, September 2008

A method to determine collection efficiency of particles by swipe sampling
journal, September 2008

Trace analysis of explosives by thermospray high-performance liquid chromatography—mass spectrometry
journal, January 1986

Using Gas Chromatography with Ion Mobility Spectrometry to Resolve Explosive Compounds in the Presence of Interferents*: EXPLOSIVES DETECTION BY IMS AND GC/IMS
journal, August 2010

A NIST Standard Reference Material (SRM) to Support the Detection of Trace Explosives
journal, September 2009

Detection of Explosives in Hair Using Ion Mobility Spectrometry
journal, May 2008

A critical review of ion mobility spectrometry for the detection of explosives and explosive related compounds
journal, May 2001

Separation of Ions from Explosives in Differential Mobility Spectrometry by Vapor-Modified Drift Gas
journal, September 2004

Particle Characteristics of Trace High Explosives: RDX and PETN
journal, March 2007

Rapid preseparation of interferences for ion mobility spectrometry
journal, March 2008

Detection of Military Explosives by Atmospheric Pressure Chemical Ionization Mass Spectrometry with Counter-Flow Introduction
journal, September 2002

Fabric analysis by ambient mass spectrometry for explosives and drugs
journal, January 2008

Instrumentation for trace detection of high explosives
journal, August 2004

Hierarchically Structured Nanocomposite Films as Highly Sensitive Chemosensory Materials for TNT Detection
journal, September 2006

Effectiveness of contamination prevention procedures in a Trace Explosives Laboratory
journal, November 2007

Detection of explosives on solid surfaces by thermal desorption and ambient ion/molecule reactions
journal, January 2005

Direct detection of explosives on solid surfaces by mass spectrometry with an ambient ion source based on dielectric barrier discharge
journal, August 2007

Direct detection of explosives on solid surfaces by mass spectrometry with an ambient ion source based on dielectric barrier discharge
journal, August 2007

Determination of nitroaromatic and nitramine explosives from a PTFE wipe using thermal desorption-gas chromatography with electron-capture detection
journal, January 2005

In-Injection Port Thermal Desorption for Explosives Trace Evidence Analysis
journal, October 1999

Selective sampling with direct ion mobility spectrometric detection for explosives analysis
journal, October 2009

Quantitative calibration of vapor levels of TNT, RDX, and PETN using a diffusion generator with gravimetry and ion mobility spectrometry
journal, December 1997

Polyester Resin-Glass Fiber Laminates
journal, August 1954

Electrochemical Sensor for Detecting Ultratrace Nitroaromatic Compounds Using Mesoporous SiO ₂ -Modified Electrode
journal, March 2006

Adsorption of 2,4,6-trinitrotoluene on a novel adsorption material PEI/SiO₂
journal, July 2009

Adsorption mechanism and property of a novel adsorption material PAM/SiO₂ towards 2,4,6-trinitrotoluene
journal, August 2009

Importance of Structural and Chemical Heterogeneity of Activated Carbon Surfaces for Adsorption of Dibenzothiophene
journal, August 2005

Adsorption of phenolic compounds by activated carbon—a critical review
journal, February 2005

Catalytic oxidation of TNT by activated carbon
journal, April 2002

Dynamic adsorption of trinitrotoluene on granular activated carbon
journal, January 2005

Adsorption performance and mechanism of 2,4,6-trinitrotoluene on a novel adsorption material polyvinylbenzyl acid/SiO₂
journal, February 2009

Conjugated polymer-grafted silica nanoparticles for the sensitive detection of TNT
journal, March 2010

Resonance Energy Transfer-Amplifying Fluorescence Quenching at the Surface of Silica Nanoparticles toward Ultrasensitive Detection of TNT
journal, November 2008

A Surface Functional Monomer-Directing Strategy for Highly Dense Imprinting of TNT at Surface of Silica Nanoparticles
journal, June 2007

Molecular Imprinting at Walls of Silica Nanotubes for TNT Recognition
journal, January 2008

Template-Free Synthesis of Organically Modified Silica Mesoporous Thin Films for TNT Sensing
journal, September 2010

Computational screening of metal–organic frameworks for large-molecule chemical sensing
journal, January 2010

Processible polyaniline complexes due to molecular recognition: Supramolecular structures based on hydrogen bonding and phenyl stacking
journal, January 1997

Variable-Temperature Powder X-ray Diffraction of Aromatic Carboxylic Acid and Carboxamide Cocrystals
journal, April 2007

Detection of explosives by positive corona discharge ion mobility spectrometry
journal, April 2010

Chemical modification of self-assembled silane based monolayers by surface reactions
journal, January 2010

Chemical modification of self-assembled silane based monolayers by surface reactions
journal, January 2010