Silicon carbide fibers and articles including same

Garnier, John E; Griffith, George W

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Title: Silicon carbide fibers and articles including same

Abstract

Methods of producing silicon carbide fibers. The method comprises reacting a continuous carbon fiber material and a silicon-containing gas in a reaction chamber at a temperature ranging from approximately 1500.degree. C. to approximately 2000.degree. C. A partial pressure of oxygen in the reaction chamber is maintained at less than approximately 1.01.times.10.sup.2 Pascal to produce continuous alpha silicon carbide fibers. Continuous alpha silicon carbide fibers and articles formed from the continuous alpha silicon carbide fibers are also disclosed.

Inventors:: Garnier, John E; Griffith, George W

Issue Date:: 2015-01-27

Research Org.:: Idaho National Laboratory (INL), Idaho Falls, ID (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1168687

Patent Number(s):: 8940391

Application Number:: 12/901,309

Assignee:: Advanced Ceramic Fibers, LLC (Idaho Falls, ID)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS

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B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
B82Y30/00 - Nanotechnology for materials or surface science, e.g. nanocomposites

C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
C01B32/956 - Silicon carbide
C01B32/97 - Preparation from SiO or SiO2

C - CHEMISTRY C04 - CEMENTS C04B - LIME, MAGNESIA
C04B2235/428 - Silicon
C04B2235/46 - Gases other than oxygen used as reactant, e.g. nitrogen used to make a nitride phase
C04B2235/48 - Organic compounds becoming part of a ceramic after heat treatment, e.g. carbonising phenol resins
C04B2235/5244 - Silicon carbide
C04B2235/5248 - Carbon, e.g. graphite
C04B2235/526 - characterised by the length of the fibers
C04B2235/5264 - characterised by the diameter of the fibers
C04B2235/5284 - Hollow fibers, e.g. nanotubes
C04B2235/5445 - submicron sized, i.e. from 0,1 to 1 micron
C04B2235/616 - Liquid infiltration of green bodies or pre-forms
C04B2235/72 - Products characterised by the absence or the low content of specific components, e.g. alkali metal free alumina ceramics
C04B2235/767 - Hexagonal symmetry, e.g. beta-Si3N4, beta-Sialon, alpha-SiC or hexa-ferrites
C04B35/565 - based on silicon carbide
C04B35/571 - obtained from {Si-containing} polymer precursors {or organosilicon monomers}
C04B35/573 - obtained by reaction sintering {or recrystallisation}
C04B35/62281 - {based on silicon carbide
C04B35/80 - Fibres, filaments, whiskers, platelets, or the like {

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
Y10T428/249924 - Noninterengaged fiber-containing paper-free web or sheet which is not of specified porosity
Y10T428/249928 - Fiber embedded in a ceramic, glass, or carbon matrix
Y10T428/24993 - Fiber is precoated
Y10T428/249974 - Metal- or silicon-containing element
Y10T428/2918 - including free carbon or carbide or therewith [not as steel]
Y10T428/292 - In coating or impregnation
Y10T428/2933 - Coated or with bond, impregnation or core
Y10T428/2958 - Metal or metal compound in coating
Y10T428/2964 - Artificial fiber or filament
Y10T428/2967 - Synthetic resin or polymer
Y10T428/2975 - Tubular or cellular

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DOE Contract Number:: AC07-051D14517

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Garnier, John E, and Griffith, George W. Silicon carbide fibers and articles including same.  United States: N. p., 2015. 
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                    Garnier, John E, & Griffith, George W. Silicon carbide fibers and articles including same.  United States.

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                    Garnier, John E, and Griffith, George W. Tue .  
        "Silicon carbide fibers and articles including same".  United States.  https://www.osti.gov/servlets/purl/1168687.

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@article{osti_1168687,

  title        = {Silicon carbide fibers and articles including same},

  author       = {Garnier, John E and Griffith, George W},

  abstractNote = {Methods of producing silicon carbide fibers. The method comprises reacting a continuous carbon fiber material and a silicon-containing gas in a reaction chamber at a temperature ranging from approximately 1500.degree. C. to approximately 2000.degree. C. A partial pressure of oxygen in the reaction chamber is maintained at less than approximately 1.01.times.10.sup.2 Pascal to produce continuous alpha silicon carbide fibers. Continuous alpha silicon carbide fibers and articles formed from the continuous alpha silicon carbide fibers are also disclosed.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2015},

  month        = {1}

}

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Works referencing / citing this record:

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URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/9272913

Methods of producing continuous boron carbide fibers
patent, December 2015

Garnier, John E.; Griffith, George W.
US Patent Document 9,199,227
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/9199227

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Similar Records

Title: Silicon carbide fibers and articles including same

Abstract

Citation Formats

Method of Making Silicon Carbide-Bonded Refractory Bodies and Coated Metal Articles patent, March 1957

Process for Making Nuclear Fuel Element patent, January 1965

Process for Producing Coatings on Carbon and Graphite Filaments patent, February 1968

Article Containing Silicon Carbon Fibers patent, June 1968

Nuclear Fuel Elements patent, February 1969

Manufacture of Silicon Carbide patent, July 1970

Surface-Treated Lamination Structures patent, April 1974

Method of Producing Crystalline Silicon Carbide Whiskers patent, May 1974

Nuclear fuel element patent, December 1975

Filamentary silicon carbide crystals by VLS growth in molten iron patent, March 1977

Nuclear fuel element having a metal liner and a diffusion barrier patent, May 1977

Preparation of SiC whiskers patent, August 1981

Nuclear fuel elements having a composite cladding patent, September 1983

Method for forming nuclear fuel containers of a composite construction and the product thereof patent, May 1984

Nuclear fuel element having a composite coating patent, September 1984

Zirconium metal matrix-silicon carbide composite nuclear reactor components patent, November 1987

Hexagonal silicon carbide platelets and preforms and methods for making and using same patent, July 1988

Single crystal whisker electric light filament patent, September 1989

Nuclear fuel element having oxidation resistant cladding patent, January 1990

Non-oxide sintered ceramic fibers patent, March 1990

Preparation of hollow ceramic fibers patent, August 1990

Coating fibers with a layer of silicon patent, November 1990

Silicon carbide fibre and production thereof patent, November 1991

Method for providing a silicon carbide matrix in carbon-fiber reinforced composites patent, November 1991

Non-oxide sintered ceramic fibers patent, August 1992

Water cooled nuclear reactor and fuel elements therefor patent, January 1993

High yield manufacturing process for silicon carbide patent, March 1993

Method of thermochemically treating silicon carbide fibers derived from polymers patent, July 1993

Method of coating carbon fibers with a carbide patent, August 1993

Wear resistant coating for fuel cladding patent, December 1993

Process for preparing silicon carbide by carbothermal reduction patent, August 1994

Process for making silicon carbide ceramic fibers patent, October 1994

Polycrystalline silicon carbide fibers patent, November 1994

Method for making fuel cladding having zirconium barrier layers and inner liners patent, January 1995

Hydride damage resistant fuel elements patent, July 1995

Ceramic fiber-reinforced composite articles and their production patent, July 1995

Aluminum alloy composite material with intermetallic compound finely dispersed in matrix among reinforcing elements patent, September 1995

Process for producing silicon carbide material patent, April 1997

Method of producing silicon carbide fibers patent, October 1997

Incandescent light energy conversion with reduced infrared emission patent, September 1998

Process for producing silicon carbide fibers patent, July 1999

Process for producing silicon carbide patent, February 2000

Method of producing single-crystal silicon carbide patent, August 2000

Composite bodies and methods for making same patent, September 2000

Process for producing silicon carbide fiber patent, November 2001

Silicon carbide fibers essentially devoid of whiskers and products made therefrom patent, May 2006

Process for producing silicon carbide fibers essentially devoid of whiskers patent, August 2006

Process for producing reinforcing SiC fiber for SiC composite material patent, October 2006

Methods for producing silicon carbide architectural preforms patent, March 2010

Controlled Atmosphere Sintering Process for Urania Containing Silica Additive patent-application, March 2002

Composite Materials and Methods for Making the Same patent-application, May 2002

Multi-layered ceramic tube for fuel containment barrier and other applications in nuclear and fossil power plants patent-application, February 2006

High Heat Flux Rate Nuclear Fuel Cladding and other Nuclear Reactor Components patent-application, October 2006

High-density, Solid Solution Nuclear Fuel and Fuel Block Utilizing Same patent-application, March 2007

Multi-layered ceramic tube for fuel containment barrier and other applications in nuclear and fossil power plants patent-application, February 2009

Silicon Carbide Material for Nuclear Applications, Precursor and Method for Forming Same, and Structures Including the Material patent-application, May 2010

Cladding Material, Tube including Such Cladding Material and Methodds of Forming the Same patent-application, April 2012

The effect of Zircaloy-4 substrate surface condition on the adhesion strength and corrosion of SiC coatings journal, November 2005

An Innovative Ceramic Corrosion Protection System for Zircaloy Cladding report, February 2003

Occurrence of airborne silicon carbide fibers during industrial production of silicon carbide. journal, April 1985

Synthesis of a silicon carbide coating on carbon fibers by deposition of a layer of pyrolytic carbon and reacting it with silicon monoxide journal, August 2008

In Situ Formation of Silicon Carbide Nanofibers on Cordierite Substrates journal, May 2007

Growth of beta-silicon carbide whiskers by the VLS process journal, April 1985

Preparation of Silicon Carbide Fiber from Activated Carbon Fiber and Gaseous Silicon Monoxide journal, June 1994

Cladding material, tube including such cladding material and methods of forming the same patent, March 2016

Methods for producing silicon carbide fibers patent, March 2016

Methods of producing continuous boron carbide fibers patent, December 2015

Method of Making Silicon Carbide-Bonded Refractory Bodies and Coated Metal Articles
patent, March 1957

Process for Making Nuclear Fuel Element
patent, January 1965

Process for Producing Coatings on Carbon and Graphite Filaments
patent, February 1968

Article Containing Silicon Carbon Fibers
patent, June 1968

Nuclear Fuel Elements
patent, February 1969

Manufacture of Silicon Carbide
patent, July 1970

Surface-Treated Lamination Structures
patent, April 1974

Method of Producing Crystalline Silicon Carbide Whiskers
patent, May 1974

Nuclear fuel element
patent, December 1975

Filamentary silicon carbide crystals by VLS growth in molten iron
patent, March 1977

Nuclear fuel element having a metal liner and a diffusion barrier
patent, May 1977

Preparation of SiC whiskers
patent, August 1981

Nuclear fuel elements having a composite cladding
patent, September 1983

Method for forming nuclear fuel containers of a composite construction and the product thereof
patent, May 1984

Nuclear fuel element having a composite coating
patent, September 1984

Zirconium metal matrix-silicon carbide composite nuclear reactor components
patent, November 1987

Hexagonal silicon carbide platelets and preforms and methods for making and using same
patent, July 1988

Single crystal whisker electric light filament
patent, September 1989

Nuclear fuel element having oxidation resistant cladding
patent, January 1990

Non-oxide sintered ceramic fibers
patent, March 1990

Preparation of hollow ceramic fibers
patent, August 1990

Coating fibers with a layer of silicon
patent, November 1990

Silicon carbide fibre and production thereof
patent, November 1991

Method for providing a silicon carbide matrix in carbon-fiber reinforced composites
patent, November 1991

Non-oxide sintered ceramic fibers
patent, August 1992

Water cooled nuclear reactor and fuel elements therefor
patent, January 1993

High yield manufacturing process for silicon carbide
patent, March 1993

Method of thermochemically treating silicon carbide fibers derived from polymers
patent, July 1993

Method of coating carbon fibers with a carbide
patent, August 1993

Wear resistant coating for fuel cladding
patent, December 1993

Process for preparing silicon carbide by carbothermal reduction
patent, August 1994

Process for making silicon carbide ceramic fibers
patent, October 1994

Polycrystalline silicon carbide fibers
patent, November 1994

Method for making fuel cladding having zirconium barrier layers and inner liners
patent, January 1995

Hydride damage resistant fuel elements
patent, July 1995

Ceramic fiber-reinforced composite articles and their production
patent, July 1995

Aluminum alloy composite material with intermetallic compound finely dispersed in matrix among reinforcing elements
patent, September 1995

Process for producing silicon carbide material
patent, April 1997

Method of producing silicon carbide fibers
patent, October 1997

Incandescent light energy conversion with reduced infrared emission
patent, September 1998

Process for producing silicon carbide fibers
patent, July 1999

Process for producing silicon carbide
patent, February 2000

Method of producing single-crystal silicon carbide
patent, August 2000

Composite bodies and methods for making same
patent, September 2000

Process for producing silicon carbide fiber
patent, November 2001

Silicon carbide fibers essentially devoid of whiskers and products made therefrom
patent, May 2006

Process for producing silicon carbide fibers essentially devoid of whiskers
patent, August 2006

Process for producing reinforcing SiC fiber for SiC composite material
patent, October 2006

Methods for producing silicon carbide architectural preforms
patent, March 2010

Controlled Atmosphere Sintering Process for Urania Containing Silica Additive
patent-application, March 2002

Composite Materials and Methods for Making the Same
patent-application, May 2002

Multi-layered ceramic tube for fuel containment barrier and other applications in nuclear and fossil power plants
patent-application, February 2006

High Heat Flux Rate Nuclear Fuel Cladding and other Nuclear Reactor Components
patent-application, October 2006

High-density, Solid Solution Nuclear Fuel and Fuel Block Utilizing Same
patent-application, March 2007

Multi-layered ceramic tube for fuel containment barrier and other applications in nuclear and fossil power plants
patent-application, February 2009

Silicon Carbide Material for Nuclear Applications, Precursor and Method for Forming Same, and Structures Including the Material
patent-application, May 2010

Cladding Material, Tube including Such Cladding Material and Methodds of Forming the Same
patent-application, April 2012

The effect of Zircaloy-4 substrate surface condition on the adhesion strength and corrosion of SiC coatings
journal, November 2005

An Innovative Ceramic Corrosion Protection System for Zircaloy Cladding
report, February 2003

Occurrence of airborne silicon carbide fibers during industrial production of silicon carbide.
journal, April 1985

Synthesis of a silicon carbide coating on carbon fibers by deposition of a layer of pyrolytic carbon and reacting it with silicon monoxide
journal, August 2008

In Situ Formation of Silicon Carbide Nanofibers on Cordierite Substrates
journal, May 2007

Growth of beta-silicon carbide whiskers by the VLS process
journal, April 1985

Preparation of Silicon Carbide Fiber from Activated Carbon Fiber and Gaseous Silicon Monoxide
journal, June 1994

Cladding material, tube including such cladding material and methods of forming the same
patent, March 2016

Methods for producing silicon carbide fibers
patent, March 2016

Methods of producing continuous boron carbide fibers
patent, December 2015