skip to main content
DOE Patents title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Microwave-assisted synthesis of transition metal phosphide

Abstract

A method of synthesizing transition metal phosphide. In one embodiment, the method has the steps of preparing a transition metal lignosulfonate, mixing the transition metal lignosulfonate with phosphoric acid to form a mixture, and subjecting the mixture to a microwave radiation for a duration of time effective to obtain a transition metal phosphide.

Inventors:
Issue Date:
Research Org.:
Board of Trustees of the University of Arkansas, Little Rock, AR (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1166767
Patent Number(s):
8,920,688
Application Number:
12/754,336
Assignee:
Board of Trustees of the University of Arkansas (Little Rock, AR)
DOE Contract Number:  
FG36-06GO86072
Resource Type:
Patent
Resource Relation:
Patent File Date: 2010 Apr 05
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats

Viswanathan, Tito. Microwave-assisted synthesis of transition metal phosphide. United States: N. p., 2014. Web.
Viswanathan, Tito. Microwave-assisted synthesis of transition metal phosphide. United States.
Viswanathan, Tito. Tue . "Microwave-assisted synthesis of transition metal phosphide". United States. https://www.osti.gov/servlets/purl/1166767.
@article{osti_1166767,
title = {Microwave-assisted synthesis of transition metal phosphide},
author = {Viswanathan, Tito},
abstractNote = {A method of synthesizing transition metal phosphide. In one embodiment, the method has the steps of preparing a transition metal lignosulfonate, mixing the transition metal lignosulfonate with phosphoric acid to form a mixture, and subjecting the mixture to a microwave radiation for a duration of time effective to obtain a transition metal phosphide.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2014},
month = {12}
}

Patent:

Save / Share:

Works referenced in this record:

The effect of nanocrystalline magnetite size on arsenic removal
journal, January 2007

  • Mayo, J. T.; Yavuz, C.; Yean, S.
  • Science and Technology of Advanced Materials, Vol. 8, Issue 1-2, p. 71-75
  • DOI: 10.1016/j.stam.2006.10.005

Novel catalysts for advanced hydroprocessing: transition metal phosphides
journal, May 2003


Adsorption of arsenic to magnetite nanoparticles: Effect of particle concentration, pH, ionic strength, and temperature
journal, December 2009

  • Shipley, Heather J.; Yean, Sujin; Kan, Amy T.
  • Environmental Toxicology and Chemistry, Vol. 28, Issue 3, p. 509-515
  • DOI: 10.1897/08-155.1

Microwave-Assisted Synthesis of a Superparamagnetic Surface-Functionalized Porous Fe3O4/C Nanocomposite
journal, October 2006

  • Hu, Xianluo; Yu, Jimmy C.
  • Chemistry – An Asian Journal, Vol. 1, Issue 4, p. 605-610
  • DOI: 10.1002/asia.200600111

Copper-doped mesoporous activated carbons as electrode material for electrochemical capacitors
journal, October 2005

  • Qinghan, Meng; Ling, Liu; Huaihe, Song
  • Journal of Applied Electrochemistry, Vol. 36, Issue 1, p. 63-67
  • DOI: 10.1007/s10800-005-9023-9

Flash Carbonization of Biomass
journal, August 2003

  • Antal, Michael Jerry; Mochidzuki, Kazuhiro; Paredes, Lloyd S.
  • Industrial & Engineering Chemistry Research, Vol. 42, Issue 16, p. 3690-3699
  • DOI: 10.1021/ie0301839

A Novel Carbothermal Method for the Preparation of Nano-sized WC on High Surface Area Carbon
journal, October 2006

  • Liu, Wei; Soneda, Yasushi; Hatori, Hiroaki
  • Chemistry Letters, Vol. 35, Issue 10, p. 1148-1149
  • DOI: 10.1246/cl.2006.1148

Removal of arsenic from water streams: an overview of available techniques
journal, July 2007

  • Vaclavikova, Miroslava; Gallios, George P.; Hredzak, Slavomir
  • Clean Technologies and Environmental Policy, Vol. 10, Issue 1, p. 89-95
  • DOI: 10.1007/s10098-007-0098-3

A novel nanostructure of nickel nanotubes encapsulated in carbon nanotubes
journal, December 2002

  • Bao, Jianchun; Wang, Keyu; Xu, Zheng
  • Chemical Communications, Issue 2, p. 208-209
  • DOI: 10.1039/B208539A

Microwave-assisted route for synthesis of nanosized metal oxides
journal, January 2007

  • Lagashetty, Arunkumar; Havanoor, Vijayanand; Basavaraja, S.
  • Science and Technology of Advanced Materials, Vol. 8, Issue 6, p. 484-493
  • DOI: 10.1016/j.stam.2007.07.001

Fabrication of novel copper phosphide (Cu3P) hollow spheres by a simple solvothermal method
journal, September 2007


Microwave-assisted synthesis of carbon supported Pt nanoparticles for fuel cell applications
journal, October 2002

  • Chen, Wei Xiang; Lee, Jim Yang; Liu, Zhaolin
  • Chemical Communications, Issue 21, p. 2588-2589
  • DOI: 10.1039/B208600J

Microwave-assisted synthesis and in-situ self-assembly of coaxial Ag/C nanocables
journal, April 2005

  • Yu, Jimmy C.; Hu, Xianluo; Li, Quan
  • Chemical Communications, Issue 21, p. 2704-2706
  • DOI: 10.1039/B502493E

Obtaining carbon nanotubes from grass
journal, May 2005


Mechanism of Hydrodenitrogenation on Phosphides and Sulfides
journal, February 2005

  • Oyama, S. Ted; Lee, Yong-Kul
  • The Journal of Physical Chemistry B, Vol. 109, Issue 6, p. 2109-2119
  • DOI: 10.1021/jp049194l

Preparation and characterization of NiO nanorods by thermal decomposition of NiC2O4 precursor
journal, February 2003

  • Xu, Congkang; Xu, Guoding; Wang, Guanghou
  • Journal of Materials Science, Vol. 38, Issue 4, p. 779-782
  • DOI: 10.1023/A:1021856930632

Controlled Synthesis, Characterization, and Crystallization of Ni−P Nanospheres
journal, December 2005

  • Xie, Songhai; Qiao, Minghua; Zhou, Wuzong
  • The Journal of Physical Chemistry B, Vol. 109, Issue 51
  • DOI: 10.1021/jp055068l

Enhanced field emission from O2 and CF4 plasma-treated CuO nanowires
journal, February 2006


A synergistic assembly of nanoscale lamellar photoconductor hybrids
journal, December 2008

  • Sofos, Marina; Goldberger, Joshua; Stone, David A.
  • Nature Materials, Vol. 8, Issue 1, p. 68-75
  • DOI: 10.1038/nmat2336

Controlled synthesis and characterization of nickel phosphide nanocrystal
journal, June 2007


Control of sp2/sp3 Carbon Ratio and Surface Chemistry of Nanodiamond Powders by Selective Oxidation in Air
journal, September 2006

  • Osswald, Sebastian; Yushin, Gleb; Mochalin, Vadym
  • Journal of the American Chemical Society, Vol. 128, Issue 35, p. 11635-11642
  • DOI: 10.1021/ja063303n

Synthesis of Inorganic Solids Using Microwaves
journal, April 1999

  • Rao, K. J.; Vaidhyanathan, B.; Ganguli, M.
  • Chemistry of Materials, Vol. 11, Issue 4, p. 882-895
  • DOI: 10.1021/cm9803859

Hydrodesulfurization of Petroleum Feedstocks with a New Type of Nonsulfide Hydrotreating Catalyst
journal, July 2002

  • Oyama, S. T.; Wang, X.; Requejo, F. G.
  • Journal of Catalysis, Vol. 209, Issue 1, p. 1-5
  • DOI: 10.1006/jcat.2002.3613

Determination of the Composition of Commercial Tannin Extracts by Liquid Secondary Ion Mass Spectrometry (LSIMS)
journal, November 1996