Reducing carbon dioxide to products

Cole, Emily Barton; Sivasankar, Narayanappa; Parajuli, Rishi; Keets, Kate A

Title: Reducing carbon dioxide to products

Abstract

A method reducing carbon dioxide to one or more products may include steps (A) to (C). Step (A) may bubble said carbon dioxide into a solution of an electrolyte and a catalyst in a divided electrochemical cell. The divided electrochemical cell may include an anode in a first cell compartment and a cathode in a second cell compartment. The cathode may reduce said carbon dioxide into said products. Step (B) may adjust one or more of (a) a cathode material, (b) a surface morphology of said cathode, (c) said electrolyte, (d) a manner in which said carbon dioxide is bubbled, (e), a pH level of said solution, and (f) an electrical potential of said divided electrochemical cell, to vary at least one of (i) which of said products is produced and (ii) a faradaic yield of said products. Step (C) may separate said products from said solution.

Inventors:: Cole, Emily Barton; Sivasankar, Narayanappa; Parajuli, Rishi; Keets, Kate A

Issue Date:: 2014-09-30

Research Org.:: Liquid Light, Inc., Monmouth Junction, NJ (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1159937

Patent Number(s):: 8845878

Application Number:: 13/787,304

Assignee:: Liquid Light, Inc. (Monmouth Junction, NJ)

Patent Classifications (CPCs):: Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02P - CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25B - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS

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Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02P - CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
Y02P20/133 - Renewable energy sources

C - CHEMISTRY C25 - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES C25B - ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS
C25B1/00 - Electrolytic production of inorganic compounds or non-metals

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DOE Contract Number:: SC0006201

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

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                    Cole, Emily Barton, Sivasankar, Narayanappa, Parajuli, Rishi, and Keets, Kate A. Reducing carbon dioxide to products.  United States: N. p., 2014. 
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                    Cole, Emily Barton, Sivasankar, Narayanappa, Parajuli, Rishi, & Keets, Kate A. Reducing carbon dioxide to products.  United States.

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                    Cole, Emily Barton, Sivasankar, Narayanappa, Parajuli, Rishi, and Keets, Kate A. Tue .  
        "Reducing carbon dioxide to products".  United States.  https://www.osti.gov/servlets/purl/1159937.

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@article{osti_1159937,

  title        = {Reducing carbon dioxide to products},

  author       = {Cole, Emily Barton and Sivasankar, Narayanappa and Parajuli, Rishi and Keets, Kate A},

  abstractNote = {A method reducing carbon dioxide to one or more products may include steps (A) to (C). Step (A) may bubble said carbon dioxide into a solution of an electrolyte and a catalyst in a divided electrochemical cell. The divided electrochemical cell may include an anode in a first cell compartment and a cathode in a second cell compartment. The cathode may reduce said carbon dioxide into said products. Step (B) may adjust one or more of (a) a cathode material, (b) a surface morphology of said cathode, (c) said electrolyte, (d) a manner in which said carbon dioxide is bubbled, (e), a pH level of said solution, and (f) an electrical potential of said divided electrochemical cell, to vary at least one of (i) which of said products is produced and (ii) a faradaic yield of said products. Step (C) may separate said products from said solution.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2014},

  month        = {9}

}

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Title: Reducing carbon dioxide to products

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Remarkable decrease in overpotential of oxalate formation in electrochemical CO 2 reduction by a metal–sulfide cluster journal, January 1995

Photochemical Reduction of Carbon Dioxide to Methanol Using ZnS Microcrystallite as a Photocatalyst in the Presence of Methanol Dehydrogenase journal, January 1994

Electrochemical Synthesis of Urea at Gas-Diffusion Electrodes journal, January 1998

Electrochemical Synthesis of Methanol from CO[sub 2] in High-Pressure Electrolyte journal, January 1997

Carbon dioxide reduction at low temperature on various metal electrodes journal, March 1989

Metal-Free Activation of CO2 by Mesoporous Graphitic Carbon Nitride journal, April 2007

Electroreduction of carbon dioxide: Part II. The mechanism of reduction in aprotic solvents journal, July 1985

Microfluidic Reactor for the Electrochemical Reduction of Carbon Dioxide: The Effect of pH journal, January 2010

Effect of Gaseous Impurities on the Electrochemical Reduction of CO conference, January 2009

Nitrogen-rich polymers for the electrocatalytic reduction of CO2 journal, December 2010

Electroreduction of carbon dioxide on platinum single crystal electrodes: electrochemical and in situ FTIR studies journal, November 1990

Pulsed Electroreduction of CO[sub 2] on Copper Electrodes journal, January 1993

Carbon Monoxide Adsorption on Copper and Silver Electrodes during Carbon Dioxide Electroreduction Studied by Infrared Reflection Absorption Spectroscopy and Surface-Enhanced Raman Spectroscopy journal, January 1996

Electrocatalytic generation of C2 and C3 compounds from carbon dioxide on a cobalt complex-immobilized dual-film electrode journal, January 1993

Electrochemical reduction of carbon dioxide on hydrogen-storing materials journal, March 1994

Electrochemical approaches to alleviation of the problem of carbon dioxide accumulation journal, January 2001

A study of the production of glyoxylic acid by the electrochemical reduction of oxalic acid solutions journal, February 1974

Photoelectrochemical pumping of enzymatic CO2 reduction journal, May 1984

Synthesis and Characterization of Rhodium Complexes Containing 2,4,6-Tris(2-pyridyl)-1,3,5-triazine and Its Metal-Promoted Hydrolytic Products: Potential Uses of the New Complexes in Electrocatalytic Reduction of Carbon Dioxide journal, November 1998

Molecular catalysts in photoelectrochemical cells: Study of an efficient system for the selective photoelectroreduction of CO2: p-GaP or p-GaAs/Ni(cyclam)2+, aqueous medium journal, September 1989

Reduction of carbon dioxide on ruthenium oxide and modified ruthenium oxide electrodes in 0.5 M NaHCO3 journal, January 1997

Prospects of CO2 Utilization via Direct Heterogeneous Electrochemical Reduction journal, December 2010

The electrochemical reduction of CO2 to oxalate at a Pt electrode immersed in acetonitrile and coated with polyvinylalcohol[Ni(dppm)2Cl2] journal, May 1995

Electrochemical reduction of CO2 on RuO2/TiO2 nanotubes composite modified Pt electrode journal, May 2005

High-yield reduction of carbon dioxide into formic acid by zero-valent metal/metal oxide redox cycles journal, January 2011

Electroreduction of carbon dioxide: Part III. Adsorption and reduction of CO2 on platinum journal, July 1985

CO2 Reduction on Rh single crystal electrodes and the structural effect journal, October 1995

Macrocyclic [N42-] Coordinated Nickel Complexes as Catalysts for the Formation of Oxalate by Electrochemical Reduction of Carbon Dioxide journal, November 2000

Electrochemical reduction of supercritical carbon dioxide in ionic liquid 1-n-butyl-3-methylimidazolium hexafluorophosphate journal, December 2004

Carbon Dioxide Reduction to Alcohols using Perovskite-Type Electrocatalysts journal, January 1993

Selective Formation of Formic Acid, Oxalic Acid, and Carbon Monoxide by Electrochemical Reduction of Carbon Dioxide journal, July 1987

Towards Solar Fuels from Water and CO 2 journal, February 2010

A new homogeneous electrocatalyst for the reduction of carbon dioxide to methanol at low overpotential
journal, July 1994

Electrochemical CO₂ Reduction on Metal Electrodes
book, January 2008

Adsorption Study of CO ₂ on Reticulated Vitreous Carbon (RVC) Covered with Platinum
journal, January 1985

Palladium and cobalt complexes of substituted quinoline, bipyridine and phenanthroline as catalysts for electrochemical reduction of carbon dioxide
journal, January 1997

Enhanced formation of ethylene and alcohols at ambient temperature and pressure in electrochemical reduction of carbon dioxide at a copper electrode
journal, January 1988

High Rate Gas Phase CO[sub 2] Reduction to Ethylene and Methane Using Gas Diffusion Electrodes
journal, January 1990

Electrode-confined catalyst systems for use in optical-to-chemical energy conversion
journal, May 1985

Electrochemical and Surface Studies of Carbon Dioxide Reduction to Methane and Ethylene at Copper Electrodes in Aqueous Solutions
journal, January 1989

Electrochemical reduction of CO and H₂ from carbon dioxide in aqua-solution
journal, March 2010

Electrochemical Reduction of CO ₂ in a Mixed Supercritical Fluid
journal, February 2000

The Electroreduction of Carbon Dioxide and Formic Acid on Tin and Indium Electrodes
journal, January 1983

Electrochemical hydrodimerization of formaldehyde to ethylene glycol
journal, October 1991

Effects of process conditions and electrode material on reaction pathways for carbon dioxide electroreduction with particular reference to formate formation
journal, December 2003

Use of gas-diffusion electrodes for high-rate electrochemical reduction of carbon dioxide. I. Reduction at lead, indium- and tin-impregnated electrodes
journal, November 1987

The electrochemical reduction of aqueous carbon dioxide to methanol at molybdenum electrodes with low overpotentials
journal, June 1986

Electrochemical Reduction of Carbon Dioxide to Methane, Methanol, and CO on Ru Electrodes
journal, January 1985

Reduction of CO[sub 2] on n-GaAs Electrodes and Selective Methanol Synthesis
journal, January 1984

Electrochemical synthesis of urea at gas-diffusion electrodes
journal, January 1998

Simultaneous reduction of carbon dioxide and nitrate ions at gas-diffusion electrodes with various metallophthalocyanine catalysts
journal, November 2003

A review of the aqueous electrochemical reduction of CO₂ to hydrocarbons at copper
journal, August 2006

Use of gas-diffusion electrodes for high-rate electrochemical reduction of carbon dioxide. II. Reduction at metal phthalocyanine-impregnated electrodes
journal, November 1987

Homogeneous Electron Transfer Catalysis of the Electrochemical Reduction of Carbon Dioxide. Do Aromatic Anion Radicals React in an Outer-Sphere Manner?
journal, January 1996

Electrochemical reduction of CO₂ on platinum electrodes in acid solutions
journal, November 1963

Photoelectrochemical reduction of aqueous carbon dioxide on p-type gallium phosphide in liquid junction solar cells
journal, September 1978

Hydrogen overpotential for transition metals and alloys, and its interpretation using an electronic model
journal, March 1993

The electrolytic reduction of carbon dioxide to formic acid
journal, September 1971

Temperature Dependence of the Probability of Chain Growth for Hydrocarbon Formation by Electrochemical Reduction of CO ₂
journal, November 2001

High performance RuPd catalysts for CO₂ reduction at gas-diffusion electrodes
journal, June 1997

An Approach to Ideal Semiconductor Electrodes for Efficient Photoelectrochemical Reduction of Carbon Dioxide by Modification with Small Metal Particles
journal, February 1998

Reversible interconversion of carbon dioxide and formate by an electroactive enzyme
journal, July 2008

Electrocatalytic process of CO selectivity in electrochemical reduction of CO₂ at metal electrodes in aqueous media
journal, August 1994

PRODUCTION OF CO AND CH ₄ IN ELECTROCHEMICAL REDUCTION OF CO ₂ AT METAL ELECTRODES IN AQUEOUS HYDROGENCARBONATE SOLUTION
journal, November 1985

Production of Methane and Ethylene in Electrochemical Reduction of Carbon Dioxide at Copper Electrode in Aqueous Hydrogencarbonate Solution
journal, June 1986

Step density dependence of co₂ reduction rate on Pt(S)-[n(111) × (111)] single crystal electrodes
journal, June 1996

Catalytic Activity of CO ₂ Reduction on Pt Single-Crystal Electrodes: Pt(S)-[ n (111)×(111)], Pt(S)-[ n (111)×(100)], and Pt(S)-[ n (100)×(111)]
journal, October 1997

Photoelectrochemical reduction products of carbon dioxide at metal coated p-GaP photocathodes in non-aqueous electrolytes
journal, March 1989

Electrochemical Reduction of Carbon Dioxide at Various Metal Electrodes in Aqueous Potassium Hydrogen Carbonate Solution
journal, September 1990

Electrochemical Conversion of Carbon Dioxide to Formate in Alkaline Polymer Electrolyte Membrane Cells
journal, January 2011

Photoelectrocatalytic reduction of carbon dioxide in aqueous suspensions of semiconductor powders
journal, February 1979

Long-term activation of the copper cathode in the course of CO₂ reduction
journal, August 1994

Photoelectrocatalytic reduction of CO₂ in LiOH/methanol at metal-modified p-InP electrodes
journal, April 2006

Reduction of CO₂ and CO to methane on Cu foil electrodes
journal, April 1988

Reduction of adsorbed Co on a Ni electrode in connection with the electrochemical reduction of CO₂
journal, July 1993

A photoelectrochemical approach to splitting carbon dioxide for a manned mission to Mars
journal, October 2001

Dinuclear Nickel Complexes as Catalysts for Electrochemical Reduction of Carbon Dioxide
journal, January 2005

Remarkable decrease in overpotential of oxalate formation in electrochemical CO ₂ reduction by a metal–sulfide cluster
journal, January 1995

Photochemical Reduction of Carbon Dioxide to Methanol Using ZnS Microcrystallite as a Photocatalyst in the Presence of Methanol Dehydrogenase
journal, January 1994

Electrochemical Synthesis of Urea at Gas-Diffusion Electrodes
journal, January 1998

Electrochemical Synthesis of Methanol from CO[sub 2] in High-Pressure Electrolyte
journal, January 1997

Carbon dioxide reduction at low temperature on various metal electrodes
journal, March 1989

Metal-Free Activation of CO₂ by Mesoporous Graphitic Carbon Nitride
journal, April 2007

Electroreduction of carbon dioxide: Part II. The mechanism of reduction in aprotic solvents
journal, July 1985

Microfluidic Reactor for the Electrochemical Reduction of Carbon Dioxide: The Effect of pH
journal, January 2010

Effect of Gaseous Impurities on the Electrochemical Reduction of CO
conference, January 2009

Nitrogen-rich polymers for the electrocatalytic reduction of CO₂
journal, December 2010

Electroreduction of carbon dioxide on platinum single crystal electrodes: electrochemical and in situ FTIR studies
journal, November 1990

Pulsed Electroreduction of CO[sub 2] on Copper Electrodes
journal, January 1993

Carbon Monoxide Adsorption on Copper and Silver Electrodes during Carbon Dioxide Electroreduction Studied by Infrared Reflection Absorption Spectroscopy and Surface-Enhanced Raman Spectroscopy
journal, January 1996

Electrocatalytic generation of C2 and C3 compounds from carbon dioxide on a cobalt complex-immobilized dual-film electrode
journal, January 1993

Electrochemical reduction of carbon dioxide on hydrogen-storing materials
journal, March 1994

Electrochemical approaches to alleviation of the problem of carbon dioxide accumulation
journal, January 2001

A study of the production of glyoxylic acid by the electrochemical reduction of oxalic acid solutions
journal, February 1974

Photoelectrochemical pumping of enzymatic CO2 reduction
journal, May 1984

Synthesis and Characterization of Rhodium Complexes Containing 2,4,6-Tris(2-pyridyl)-1,3,5-triazine and Its Metal-Promoted Hydrolytic Products: Potential Uses of the New Complexes in Electrocatalytic Reduction of Carbon Dioxide
journal, November 1998

Molecular catalysts in photoelectrochemical cells: Study of an efficient system for the selective photoelectroreduction of CO₂: p-GaP or p-GaAs/Ni(cyclam)²⁺, aqueous medium
journal, September 1989

Reduction of carbon dioxide on ruthenium oxide and modified ruthenium oxide electrodes in 0.5 M NaHCO₃
journal, January 1997

Prospects of CO₂ Utilization via Direct Heterogeneous Electrochemical Reduction
journal, December 2010

The electrochemical reduction of CO₂ to oxalate at a Pt electrode immersed in acetonitrile and coated with $polyvinylalcohol [Ni(dppm)_{2} Cl_{2}]$
journal, May 1995

Electrochemical reduction of CO₂ on RuO₂/TiO₂ nanotubes composite modified Pt electrode
journal, May 2005

High-yield reduction of carbon dioxide into formic acid by zero-valent metal/metal oxide redox cycles
journal, January 2011

Electroreduction of carbon dioxide: Part III. Adsorption and reduction of CO₂ on platinum
journal, July 1985

CO₂ Reduction on Rh single crystal electrodes and the structural effect
journal, October 1995

Macrocyclic [N₄^2-] Coordinated Nickel Complexes as Catalysts for the Formation of Oxalate by Electrochemical Reduction of Carbon Dioxide
journal, November 2000

Electrochemical reduction of supercritical carbon dioxide in ionic liquid 1-n-butyl-3-methylimidazolium hexafluorophosphate
journal, December 2004

Carbon Dioxide Reduction to Alcohols using Perovskite-Type Electrocatalysts
journal, January 1993

Selective Formation of Formic Acid, Oxalic Acid, and Carbon Monoxide by Electrochemical Reduction of Carbon Dioxide
journal, July 1987

Towards Solar Fuels from Water and CO ₂
journal, February 2010

Photo-aided reduction of carbon dioxide to carbon monoxide
journal, October 1983

The mediation of the photoelectrochemical reduction of carbon dioxide by ammonium ions
journal, February 1984

Effects of electrolytes on the photoelectrochemical reduction of carbon dioxide at illuminated p-type cadmium telluride and p-type indium phosphide electrodes in aqueous solutions
journal, July 1988