Thin-layer chromatography and colorimetric analysis of multi-component explosive mixtures
Abstract
A thin-layer chromatography method for detection and identification of common military and peroxide explosives in samples includes the steps of provide a reverse-phase thin-layer chromatography plate; prepare the plate by marking spots on which to deposit the samples by touching the plate with a marker; spot one micro liter of a first standard onto one of the spots, spot one micro liter of a second standard onto another of the spots, and spot samples onto other of spots producing a spotted plate; add eluent to a developing chamber; add the spotted plate to the developing chamber; remove the spotted plate from the developing chamber producing a developed plate; place the developed plate in an ultraviolet light box; add a visualization agent to a dip tank; dip the developed plate in the dip tank and remove the developed plate quickly; and detect explosives by viewing said developed plate.
- Inventors:
- Issue Date:
- Research Org.:
- Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1151765
- Patent Number(s):
- 8815606
- Application Number:
- 12/106,400
- Assignee:
- Lawrence Livermore National Security, LLC (Livermore, CA)
- Patent Classifications (CPCs):
-
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y10 - TECHNICAL SUBJECTS COVERED BY FORMER USPC Y10T - TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- DOE Contract Number:
- AC52-07NA27344
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Pagoria, Philip F., Mitchell, Alexander R., Whipple, Richard E., and Carman, M. Leslie. Thin-layer chromatography and colorimetric analysis of multi-component explosive mixtures. United States: N. p., 2014.
Web.
Pagoria, Philip F., Mitchell, Alexander R., Whipple, Richard E., & Carman, M. Leslie. Thin-layer chromatography and colorimetric analysis of multi-component explosive mixtures. United States.
Pagoria, Philip F., Mitchell, Alexander R., Whipple, Richard E., and Carman, M. Leslie. Tue .
"Thin-layer chromatography and colorimetric analysis of multi-component explosive mixtures". United States. https://www.osti.gov/servlets/purl/1151765.
@article{osti_1151765,
title = {Thin-layer chromatography and colorimetric analysis of multi-component explosive mixtures},
author = {Pagoria, Philip F. and Mitchell, Alexander R. and Whipple, Richard E. and Carman, M. Leslie},
abstractNote = {A thin-layer chromatography method for detection and identification of common military and peroxide explosives in samples includes the steps of provide a reverse-phase thin-layer chromatography plate; prepare the plate by marking spots on which to deposit the samples by touching the plate with a marker; spot one micro liter of a first standard onto one of the spots, spot one micro liter of a second standard onto another of the spots, and spot samples onto other of spots producing a spotted plate; add eluent to a developing chamber; add the spotted plate to the developing chamber; remove the spotted plate from the developing chamber producing a developed plate; place the developed plate in an ultraviolet light box; add a visualization agent to a dip tank; dip the developed plate in the dip tank and remove the developed plate quickly; and detect explosives by viewing said developed plate.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Aug 26 00:00:00 EDT 2014},
month = {Tue Aug 26 00:00:00 EDT 2014}
}
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