Devices and process for high-pressure magic angle spinning nuclear magnetic resonance

Hoyt, David W; Sears, Jesse A; Turcu, Romulus V.F.; Rosso, Kevin M; Hu, Jian Zhi

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Title: Devices and process for high-pressure magic angle spinning nuclear magnetic resonance

Abstract

A high-pressure magic angle spinning (MAS) rotor is detailed that includes a high-pressure sample cell that maintains high pressures exceeding 150 bar. The sample cell design minimizes pressure losses due to penetration over an extended period of time.

Inventors:: Hoyt, David W; Sears, Jr., Jesse A; Turcu, Romulus V.F.; Rosso, Kevin M; Hu, Jian Zhi

Issue Date:: Tue Apr 08 00:00:00 EDT 2014

Research Org.:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1129164

Patent Number(s):: 8692548

Application Number:: 13/193,172

Assignee:: Battelle Memorial Institute (Richland, WA)

Patent Classifications (CPCs):: G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES

Show more

G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES
G01R33/305 - {specially adapted for high-pressure applications}
G01R33/307 - {specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer}
G01R33/34069 - {Saddle coils}

Show less

DOE Contract Number:: AC05-76RLO1830

Resource Type:: Patent

Resource Relation:: Patent File Date: 2011 Jul 28

Country of Publication:: United States

Language:: English

Subject:: 42 ENGINEERING

Citation Formats


                    Hoyt, David W, Sears, Jr., Jesse A, Turcu, Romulus V.F., Rosso, Kevin M, and Hu, Jian Zhi. Devices and process for high-pressure magic angle spinning nuclear magnetic resonance.  United States: N. p., 2014. 
        Web.

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                    Hoyt, David W, Sears, Jr., Jesse A, Turcu, Romulus V.F., Rosso, Kevin M, & Hu, Jian Zhi. Devices and process for high-pressure magic angle spinning nuclear magnetic resonance.  United States.

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                    Hoyt, David W, Sears, Jr., Jesse A, Turcu, Romulus V.F., Rosso, Kevin M, and Hu, Jian Zhi. Tue .  
        "Devices and process for high-pressure magic angle spinning nuclear magnetic resonance".  United States.  https://www.osti.gov/servlets/purl/1129164.

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@article{osti_1129164,

  title        = {Devices and process for high-pressure magic angle spinning nuclear magnetic resonance},

  author       = {Hoyt, David W and Sears, Jr., Jesse A and Turcu, Romulus V.F. and Rosso, Kevin M and Hu, Jian Zhi},

  abstractNote = {A high-pressure magic angle spinning (MAS) rotor is detailed that includes a high-pressure sample cell that maintains high pressures exceeding 150 bar. The sample cell design minimizes pressure losses due to penetration over an extended period of time.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Apr 08 00:00:00 EDT 2014},

  month        = {Tue Apr 08 00:00:00 EDT 2014}

}

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Works referenced in this record:

Radial Chamber Positive Displacement, Fluid Power Device
patent, June 1971

Klover, John
US Patent Document 3,585,973
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/3585973

Multiposition selector valve
patent, September 1985

Acker, Richard C.
US Patent Document 4,538,640
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4538640

Closed passage type equi-pressure combustion rotary engine
patent, April 1987

Zen, Sheng T.
US Patent Document 4,657,009
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4657009

Fuel distributing and injector pump with electronic control
patent, March 1992

Ament, Frank
US Patent Document 5,099,814
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5099814

Emulsion fuel feeding apparatus and method
patent, August 1996

Kessler, Alfred
US Patent Document 5,542,379
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5542379

Nuclear magnetic resonance spectrometer
patent, June 1998

Foerster, Hans; Zick, Klaus
US Patent Document 5,760,586
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5760586

NMR MAS sealing sample cells and methods
patent, April 2000

Doty, F. David
US Patent Document 6,054,857
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6054857

Closed-loop conveyance systems for well servicing
patent, March 2005

Vail, III, William Banning; Chitwood, James E.
US Patent Document 6,868,906
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6868906

Methods and apparatus to convey electrical pumping systems into wellbores to complete oil and gas wells
patent, February 2008

Vail, III, William Banning; Chitwood, James E.
US Patent Document 7,325,606
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7325606

Methods and apparatus to convey electrical pumping systems into wellbores to complete oil and gas wells
patent, November 2010

Vail, III, William Banning; Chitwood, James E.
US Patent Document 7,836,950
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7836950

Pressure release encoding system for communicating downhole information through a wellbore to a surface location
patent, February 2011

Close, David
US Patent Document 7,881,155
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7881155

Pressure release encoding system for communicating downhole information through a wellbore to a surface location
patent, June 2013

Close, David
US Patent Document 8,467,268
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8467268

NMR MAS Electret Spin Rate Detection
patent-application, October 2006

Doty, F. David
US Patent Application 11/276821; 20060220647
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20060220647

The use of supercritical fluids as solvents for NMR spectroscopy
journal, October 2005

Yonker, Clement R.; Linehan, John C.
Progress in Nuclear Magnetic Resonance Spectroscopy, Vol. 47, Issue 1-2, p. 95-109
https://doi.org/10.1016/j.pnmrs.2005.08.002

Design and performance of a high pressure insert for use in a standard magic angle spinning NMR probe
journal, December 2006

Deuchande, Teresa; Breton, Olivier; Haedelt, Josefin
Journal of Magnetic Resonance, Vol. 183, Issue 2, p. 178-182
https://doi.org/10.1016/j.jmr.2006.08.007

High-pressure magic angle spinning nuclear magnetic resonance
journal, October 2011

Hoyt, David W.; Turcu, Romulus V. F.; Sears, Jesse A.
Journal of Magnetic Resonance, Vol. 212, Issue 2, p. 378-385
https://doi.org/10.1016/j.jmr.2011.07.019

Nuclear Induction
journal, February 1946

Bloch, F.; Hansen, W. W.; Packard, Martin
Physical Review, Vol. 69, Issue 3-4, p. 127-127
https://doi.org/10.1103/PhysRev.69.127

Resonance Absorption by Nuclear Magnetic Moments in a Solid
journal, January 1946

Purcell, E. M.; Torrey, H. C.; Pound, R. V.
Physical Review, Vol. 69, Issue 1-2, p. 37-38
https://doi.org/10.1103/PhysRev.69.37

Free Induction Decays of Rotating Solids
journal, April 1959

Lowe, I. J.
Physical Review Letters, Vol. 2, Issue 7, p. 285-287
https://doi.org/10.1103/PhysRevLett.2.285

¹³C High-Pressure CPMAS NMR Characterization of the Molecular Motion of Polystyrene Plasticized by CO₂ Gas
journal, October 1997

Miyoshi, Toshikazu; Takegoshi, K.; Terao, Takehiko
Macromolecules, Vol. 30, Issue 21, p. 6582-6585
https://doi.org/10.1021/ma961891r

Effects of Xe Gas on Segmental Motion in a Polymer Blend As Studied by ¹³C and ¹²⁹Xe High-Pressure MAS NMR
journal, January 2002

Miyoshi, Toshikazu; Takegoshi, K.; Terao, Takehiko
Macromolecules, Vol. 35, Issue 1, p. 151-154
https://doi.org/10.1021/ma0115287

Chemistry in superacids. 12. Carbonic acid and its mono- and diprotonation: NMR, ab initio, and IGLO investigation
journal, March 1993

Rasul, Golam; Reddy, V. Prakash; Zdunek, Leszek Z.
Journal of the American Chemical Society, Vol. 115, Issue 6, p. 2236-2238
https://doi.org/10.1021/ja00059a020

Metal Carbonation of Forsterite in Supercritical CO₂ and H₂O Using Solid State ²⁹Si, ¹³C NMR Spectroscopy
journal, February 2010

Kwak, Ja Hun; Hu, Jian Zhi; Hoyt, David W.
The Journal of Physical Chemistry C, Vol. 114, Issue 9, p. 4126-4134
https://doi.org/10.1021/jp1001308

Microcoil High-Resolution Magic Angle Spinning NMR Spectroscop
June 2006

Janssen, Hans; Brinkmann, Andreas; van Eck, Ernst R. H.
Journal of the American Chemical Society, Vol. 128, Issue 27, p. 8722-8723
https://doi.org/10.1021/ja061350+

High-resolution, high-sensitivity NMR of nanolitre anisotropic samples by coil spinning
journal, June 2007

Sakellariou, D.; Goff, G. Le; Jacquinot, J.-F.
Nature, Vol. 447, Issue 7145, p. 694-697
https://doi.org/10.1038/nature05897

Nuclear Magnetic Resonance Spectra from a Crystal rotated at High Speed
journal, December 1958

Andrew, E. R.; Bradbury, A.; Eades, R. G.
Nature, Vol. 182, Issue 4650
https://doi.org/10.1038/1821659a0

¹²⁹Xe n.m.r. study of free volume and phase separation of the polystyrene/poly(vinyl methyl ether) blend
journal, October 1997

Miyoshi, Toshikazu; Takegoshi, K.; Terao, Takehiko
Polymer, Vol. 38, Issue 21, p. 5475-5480
https://doi.org/10.1016/S0032-3861(97)00086-4

A new high pressure sapphire nuclear magnetic resonance cell
journal, January 1996

Bai, Shi; Taylor, Craig M.; Mayne, Charles L.
Review of Scientific Instruments, Vol. 67, Issue 1, p. 240-243
https://doi.org/10.1063/1.1146578

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Similar Records

Title: Devices and process for high-pressure magic angle spinning nuclear magnetic resonance

Abstract

Citation Formats

Radial Chamber Positive Displacement, Fluid Power Device patent, June 1971

Multiposition selector valve patent, September 1985

Closed passage type equi-pressure combustion rotary engine patent, April 1987

Fuel distributing and injector pump with electronic control patent, March 1992

Emulsion fuel feeding apparatus and method patent, August 1996

Nuclear magnetic resonance spectrometer patent, June 1998

NMR MAS sealing sample cells and methods patent, April 2000

Closed-loop conveyance systems for well servicing patent, March 2005

Methods and apparatus to convey electrical pumping systems into wellbores to complete oil and gas wells patent, February 2008

Methods and apparatus to convey electrical pumping systems into wellbores to complete oil and gas wells patent, November 2010

Pressure release encoding system for communicating downhole information through a wellbore to a surface location patent, February 2011

Pressure release encoding system for communicating downhole information through a wellbore to a surface location patent, June 2013

NMR MAS Electret Spin Rate Detection patent-application, October 2006

The use of supercritical fluids as solvents for NMR spectroscopy journal, October 2005

Design and performance of a high pressure insert for use in a standard magic angle spinning NMR probe journal, December 2006

High-pressure magic angle spinning nuclear magnetic resonance journal, October 2011

Nuclear Induction journal, February 1946

Resonance Absorption by Nuclear Magnetic Moments in a Solid journal, January 1946

Free Induction Decays of Rotating Solids journal, April 1959

13C High-Pressure CPMAS NMR Characterization of the Molecular Motion of Polystyrene Plasticized by CO2 Gas journal, October 1997

Effects of Xe Gas on Segmental Motion in a Polymer Blend As Studied by 13C and 129Xe High-Pressure MAS NMR journal, January 2002

Chemistry in superacids. 12. Carbonic acid and its mono- and diprotonation: NMR, ab initio, and IGLO investigation journal, March 1993

Metal Carbonation of Forsterite in Supercritical CO2 and H2O Using Solid State 29Si, 13C NMR Spectroscopy journal, February 2010

Microcoil High-Resolution Magic Angle Spinning NMR Spectroscop June 2006

High-resolution, high-sensitivity NMR of nanolitre anisotropic samples by coil spinning journal, June 2007

Nuclear Magnetic Resonance Spectra from a Crystal rotated at High Speed journal, December 1958

129Xe n.m.r. study of free volume and phase separation of the polystyrene/poly(vinyl methyl ether) blend journal, October 1997

A new high pressure sapphire nuclear magnetic resonance cell journal, January 1996

Radial Chamber Positive Displacement, Fluid Power Device
patent, June 1971

Multiposition selector valve
patent, September 1985

Closed passage type equi-pressure combustion rotary engine
patent, April 1987

Fuel distributing and injector pump with electronic control
patent, March 1992

Emulsion fuel feeding apparatus and method
patent, August 1996

Nuclear magnetic resonance spectrometer
patent, June 1998

NMR MAS sealing sample cells and methods
patent, April 2000

Closed-loop conveyance systems for well servicing
patent, March 2005

Methods and apparatus to convey electrical pumping systems into wellbores to complete oil and gas wells
patent, February 2008

Methods and apparatus to convey electrical pumping systems into wellbores to complete oil and gas wells
patent, November 2010

Pressure release encoding system for communicating downhole information through a wellbore to a surface location
patent, February 2011

Pressure release encoding system for communicating downhole information through a wellbore to a surface location
patent, June 2013

NMR MAS Electret Spin Rate Detection
patent-application, October 2006

The use of supercritical fluids as solvents for NMR spectroscopy
journal, October 2005

Design and performance of a high pressure insert for use in a standard magic angle spinning NMR probe
journal, December 2006

High-pressure magic angle spinning nuclear magnetic resonance
journal, October 2011

Nuclear Induction
journal, February 1946

Resonance Absorption by Nuclear Magnetic Moments in a Solid
journal, January 1946

Free Induction Decays of Rotating Solids
journal, April 1959

¹³C High-Pressure CPMAS NMR Characterization of the Molecular Motion of Polystyrene Plasticized by CO₂ Gas
journal, October 1997

Effects of Xe Gas on Segmental Motion in a Polymer Blend As Studied by ¹³C and ¹²⁹Xe High-Pressure MAS NMR
journal, January 2002

Chemistry in superacids. 12. Carbonic acid and its mono- and diprotonation: NMR, ab initio, and IGLO investigation
journal, March 1993

Metal Carbonation of Forsterite in Supercritical CO₂ and H₂O Using Solid State ²⁹Si, ¹³C NMR Spectroscopy
journal, February 2010

Microcoil High-Resolution Magic Angle Spinning NMR Spectroscop
June 2006

High-resolution, high-sensitivity NMR of nanolitre anisotropic samples by coil spinning
journal, June 2007

Nuclear Magnetic Resonance Spectra from a Crystal rotated at High Speed
journal, December 1958

¹²⁹Xe n.m.r. study of free volume and phase separation of the polystyrene/poly(vinyl methyl ether) blend
journal, October 1997

A new high pressure sapphire nuclear magnetic resonance cell
journal, January 1996