Composite media for fluid stream processing, a method of forming the composite media, and a related method of processing a fluid stream

Garn, Troy G; Law, Jack D; Greenhalgh, Mitchell R; Tranter, Rhonda

Title: Composite media for fluid stream processing, a method of forming the composite media, and a related method of processing a fluid stream

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Abstract

A composite media including at least one crystalline aluminosilicate material in polyacrylonitrile. A method of forming a composite media is also disclosed. The method comprises dissolving polyacrylonitrile in an organic solvent to form a matrix solution. At least one crystalline aluminosilicate material is combined with the matrix solution to form a composite media solution. The organic solvent present in the composite media solution is diluted. The composite media solution is solidified. In addition, a method of processing a fluid stream is disclosed. The method comprises providing a beads of a composite media comprising at least one crystalline aluminosilicate material dispersed in a polyacrylonitrile matrix. The beads of the composite media are contacted with a fluid stream comprising at least one constituent. The at least one constituent is substantially removed from the fluid stream.

Inventors:: Garn, Troy G; Law, Jack D; Greenhalgh, Mitchell R; Tranter, Rhonda

Issue Date:: 2014-04-01

Research Org.:: Idaho National Lab. (INL), Idaho Falls, ID (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1128708

Patent Number(s):: 8686083

Application Number:: 13/291,214

Assignee:: Battelle Energy Alliance, LLC (Idaho Falls, ID)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION

G - PHYSICS G21 - NUCLEAR PHYSICS G21F - PROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT

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B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D2257/202 - Single element halogens
B01D2257/11 - Noble gases
B01D2259/40088 - by heating

G - PHYSICS G21 - NUCLEAR PHYSICS G21F - PROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT
G21F9/02 - Treating gases

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J2220/46 - Materials comprising a mixture of inorganic and organic materials

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D2253/108 - Zeolites

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J20/28019 - {Spherical, ellipsoidal or cylindrical}
B01J20/28061 - {being in the range 100-500 m2/g}
B01J20/3085 - {Chemical treatments not covered by groups B01J20/3007 - B01J20/3078}

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D53/685 - {by treating the gases with solids}
B01D53/02 - by adsorption, e.g. preparative gas chromatography {

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J20/3028 - {Granulating, agglomerating or aggregating}
B01J20/18 - Synthetic zeolitic molecular sieves

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D2253/306 - Surface area, e.g. BET-specific surface
B01D2253/202 - Polymeric adsorbents
B01D2253/34 - Specific shapes

B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B01J20/261 - {obtained by reactions only involving carbon to carbon unsaturated bonds
B01J20/186 - {Chemical treatments in view of modifying the properties of the sieve, e.g. increasing the stability or the activity, also decreasing the activity}

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DOE Contract Number:: AC07-05ID14517

Resource Type:: Patent

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats


                    Garn, Troy G, Law, Jack D, Greenhalgh, Mitchell R, and Tranter, Rhonda. Composite media for fluid stream processing, a method of forming the composite media, and a related method of processing a fluid stream.  United States: N. p., 2014. 
        Web.

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                    Garn, Troy G, Law, Jack D, Greenhalgh, Mitchell R, & Tranter, Rhonda. Composite media for fluid stream processing, a method of forming the composite media, and a related method of processing a fluid stream.  United States.

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                    Garn, Troy G, Law, Jack D, Greenhalgh, Mitchell R, and Tranter, Rhonda. Tue .  
        "Composite media for fluid stream processing, a method of forming the composite media, and a related method of processing a fluid stream".  United States.  https://www.osti.gov/servlets/purl/1128708.

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@article{osti_1128708,

  title        = {Composite media for fluid stream processing, a method of forming the composite media, and a related method of processing a fluid stream},

  author       = {Garn, Troy G and Law, Jack D and Greenhalgh, Mitchell R and Tranter, Rhonda},

  abstractNote = {A composite media including at least one crystalline aluminosilicate material in polyacrylonitrile. A method of forming a composite media is also disclosed. The method comprises dissolving polyacrylonitrile in an organic solvent to form a matrix solution. At least one crystalline aluminosilicate material is combined with the matrix solution to form a composite media solution. The organic solvent present in the composite media solution is diluted. The composite media solution is solidified. In addition, a method of processing a fluid stream is disclosed. The method comprises providing a beads of a composite media comprising at least one crystalline aluminosilicate material dispersed in a polyacrylonitrile matrix. The beads of the composite media are contacted with a fluid stream comprising at least one constituent. The at least one constituent is substantially removed from the fluid stream.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2014},

  month        = {4}

}

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