Compositions, devices and methods for SERS and LSPR

Van Duyne, Richard P; Zhang, Xiaoyu; Zhao, Jing; Whitney, Alyson V; Elam, Jeffrey W; Schatz, George C; Stair, Peter C; Zou, Shengli; Young, Matthew; Lyandres, Olga

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Title: Compositions, devices and methods for SERS and LSPR

Abstract

The present invention relates to compositions, devices and methods for detecting microorganisms (e.g., anthrax). In particular, the present invention provides portable, surface-enhanced Raman biosensors, and associated substrates, and methods of using the same, for use in rapidly detecting and identifying microorganisms (e.g., anthrax).

Inventors:: Van Duyne, Richard P; Zhang, Xiaoyu; Zhao, Jing; Whitney, Alyson V; Elam, Jeffrey W; Schatz, George C; Stair, Peter C; Zou, Shengli; Young, Matthew; Lyandres, Olga

Issue Date:: 2014-01-14

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1117699

Patent Number(s):: 8628727

Application Number:: 11/846,352

Assignee:: Northwestern University (Evanston, IL)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES

C - CHEMISTRY C12 - BIOCHEMISTRY C12Q - MEASURING OR TESTING PROCESSES INVOLVING ENZYMES, NUCLEIC ACIDS OR MICROORGANISMS

Show more

B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
B82Y15/00 - Nanotechnology for interacting, sensing or actuating, e.g. quantum dots as markers in protein assays or molecular motors
B82Y30/00 - Nanotechnology for materials or surface science, e.g. nanocomposites

C - CHEMISTRY C12 - BIOCHEMISTRY C12Q - MEASURING OR TESTING PROCESSES INVOLVING ENZYMES, NUCLEIC ACIDS OR MICROORGANISMS
C12Q1/04 - Determining presence or kind of microorganism

G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N21/658 - {enhancement Raman, e.g. surface plasmons}

Show less

DOE Contract Number:: FG02-03ER15457; W-31-109-ENG-38; AC02-06CH11357

Resource Type:: Patent

Resource Relation:: Patent File Date: 2007 Aug 28

Country of Publication:: United States

Language:: English

Subject:: 47 OTHER INSTRUMENTATION

Citation Formats


                    Van Duyne, Richard P, Zhang, Xiaoyu, Zhao, Jing, Whitney, Alyson V, Elam, Jeffrey W, Schatz, George C, Stair, Peter C, Zou, Shengli, Young, Matthew, and Lyandres, Olga. Compositions, devices and methods for SERS and LSPR.  United States: N. p., 2014. 
        Web.

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                    Van Duyne, Richard P, Zhang, Xiaoyu, Zhao, Jing, Whitney, Alyson V, Elam, Jeffrey W, Schatz, George C, Stair, Peter C, Zou, Shengli, Young, Matthew, & Lyandres, Olga. Compositions, devices and methods for SERS and LSPR.  United States.

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                    Van Duyne, Richard P, Zhang, Xiaoyu, Zhao, Jing, Whitney, Alyson V, Elam, Jeffrey W, Schatz, George C, Stair, Peter C, Zou, Shengli, Young, Matthew, and Lyandres, Olga. Tue .  
        "Compositions, devices and methods for SERS and LSPR".  United States.  https://www.osti.gov/servlets/purl/1117699.

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@article{osti_1117699,

  title        = {Compositions, devices and methods for SERS and LSPR},

  author       = {Van Duyne, Richard P and Zhang, Xiaoyu and Zhao, Jing and Whitney, Alyson V and Elam, Jeffrey W and Schatz, George C and Stair, Peter C and Zou, Shengli and Young, Matthew and Lyandres, Olga},

  abstractNote = {The present invention relates to compositions, devices and methods for detecting microorganisms (e.g., anthrax). In particular, the present invention provides portable, surface-enhanced Raman biosensors, and associated substrates, and methods of using the same, for use in rapidly detecting and identifying microorganisms (e.g., anthrax).},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2014},

  month        = {1}

}

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Works referenced in this record:

Surface-enhanced raman nanobiosensor
patent-application, September 2004

Van Duyne, Richard P.; Glucksberg, Matthew R.; Shafer-Peltier, Karen
US Patent Application 10/652280; 20040180379
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20040180379

Adaptive metal films for detection of biomolecules
patent-application, November 2005

Drachev, Vladimir P.; Thoreson, Mark D.; Nashine, Vishal C.
US Patent Application 11/087262; 20050244977
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20050244977

Atomic force microscopy and surface‐enhanced Raman spectroscopy. I. Ag island films and Ag film over polymer nanosphere surfaces supported on glass
journal, August 1993

Van Duyne, R. P.; Hulteen, J. C.; Treichel, D. A.
The Journal of Chemical Physics, Vol. 99, Issue 3
https://doi.org/10.1063/1.465276

Localized Surface Plasmon Resonance Nanosensor: A High-Resolution Distance-Dependence Study Using Atomic Layer Deposition
journal, November 2005

Whitney, Alyson V.; Elam, Jeffrey W.; Zou, Shengli
The Journal of Physical Chemistry B, Vol. 109, Issue 43
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Vibrational spectra and structure of crystalline dipicolinic acid and calcium dipicolinate trihydrate
journal, January 1980

Carmona, P.
Spectrochimica Acta Part A: Molecular Spectroscopy, Vol. 36, Issue 7, p. 705-712
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Octadecylthiol-modified surface-enhanced Raman spectroscopy substrates: a new method for the detection of aromatic compounds
journal, October 1992

Carron, Keith; Peitersen, Laura; Lewis, Mary
Environmental Science & Technology, Vol. 26, Issue 10
https://doi.org/10.1021/es00034a011

Reagentless Identification of Single Bacterial Spores in Aqueous Solution by Confocal Laser Tweezers Raman Spectroscopy
journal, February 2004

Chan, J. W.; Esposito, A. P.; Talley, C. E.
Analytical Chemistry, Vol. 76, Issue 3
https://doi.org/10.1021/ac0350155

Metal Film over Nanosphere (MFON) Electrodes for Surface-Enhanced Raman Spectroscopy (SERS): Improvements in Surface Nanostructure Stability and Suppression of Irreversible Loss
journal, January 2002

Dick, Lisa A.; McFarland, Adam D.; Haynes, Christy L.
The Journal of Physical Chemistry B, Vol. 106, Issue 4
https://doi.org/10.1021/jp013638l

Introductory Lecture : Surface enhanced Raman spectroscopy: new materials, concepts, characterization tools, and applications
journal, January 2006

Dieringer, Jon A.; McFarland, Adam D.; Shah, Nilam C.
Faraday Discuss., Vol. 132
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Low-Level Detection of Viral Pathogens by a Surface-Enhanced Raman Scattering Based Immunoassay
journal, October 2005

Driskell, Jeremy D.; Kwarta, Karen M.; Lipert, Robert J.
Analytical Chemistry, Vol. 77, Issue 19
https://doi.org/10.1021/ac0504159

Viscous flow reactor with quartz crystal microbalance for thin film growth by atomic layer deposition
journal, August 2002

Elam, J. W.; Groner, M. D.; George, S. M.
Review of Scientific Instruments, Vol. 73, Issue 8, p. 2981-2987
https://doi.org/10.1063/1.1490410

Rapid Dipicolinic Acid Extraction from Bacillus Spores Detected by Surface-Enhanced Raman Spectroscopy
journal, March 2004

Farquharson, Stuart; Gift, Alan D.; Maksymiuk, Paul
Applied Spectroscopy, Vol. 58, Issue 3
https://doi.org/10.1366/000370204322886735

Detection of the Dipicolinic Acid Biomarker in Bacillus Spores Using Curie-Point Pyrolysis Mass Spectrometry and Fourier Transform Infrared Spectroscopy
journal, January 2000

Goodacre, Royston; Shann, Beverley; Gilbert, Richard J.
Analytical Chemistry, Vol. 72, Issue 1
https://doi.org/10.1021/ac990661i

Plasmon-Sampled Surface-Enhanced Raman Excitation Spectroscopy ^†
journal, July 2003

Haynes, Christy L.; Van Duyne, Richard P.
The Journal of Physical Chemistry B, Vol. 107, Issue 30
https://doi.org/10.1021/jp027749b

Nanosphere lithography: A materials general fabrication process for periodic particle array surfaces
journal, May 1995

Hulteen, John C.; Van Duyne, Richard P.
Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films, Vol. 13, Issue 3, p. 1553-1558
https://doi.org/10.1116/1.579726

Discrimination of Bacteria Using Surface-Enhanced Raman Spectroscopy
journal, January 2004

Jarvis, Roger M.; Goodacre, Royston
Analytical Chemistry, Vol. 76, Issue 1
https://doi.org/10.1021/ac034689c

Sticking Probabilities in Adsorption of Alkanethiols from Liquid Ethanol Solution onto Gold
journal, November 2000

Jung, Linda S.; Campbell, Charles. T.
The Journal of Physical Chemistry B, Vol. 104, Issue 47
https://doi.org/10.1021/jp001649t

Sticking Probabilities in Adsorption from Liquid Solutions: Alkylthiols on Gold
journal, May 2000

Jung, Linda S.; Campbell, Charles T.
Physical Review Letters, Vol. 84, Issue 22
https://doi.org/10.1103/PhysRevLett.84.5164

Performance Assessment of Three Commercial Assays for Direct Detection of Bacillus anthracis Spores
journal, July 2003

King, D.; Luna, V.; Cannons, A.
Journal of Clinical Microbiology, Vol. 41, Issue 7
https://doi.org/10.1128/JCM.41.7.3454-3455.2003

Surface-Enhanced Raman Scattering Detected Temperature Programmed Desorption: Optical Properties, Nanostructure, and Stability of Silver Film over SiO ₂ Nanosphere Surfaces
journal, July 2001

Litorja, Maritoni; Haynes, Christy L.; Haes, Amanda J.
The Journal of Physical Chemistry B, Vol. 105, Issue 29
https://doi.org/10.1021/jp010333y

Wavelength-Scanned Surface-Enhanced Raman Excitation Spectroscopy
journal, June 2005

McFarland, Adam D.; Young, Matthew A.; Dieringer, Jon A.
The Journal of Physical Chemistry B, Vol. 109, Issue 22
https://doi.org/10.1021/jp050508u

Detection of Nitrate and Sulfate Anions by Normal Raman Spectroscopy and SERS of Cationic-Coated, Silver Substrates
journal, August 2000

Mosier-Boss, P. A.; Lieberman, S. H.
Applied Spectroscopy, Vol. 54, Issue 8
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Enhanced spore detection using dipicolinate extraction techniques
journal, March 2002

Pellegrino, Paul M.; Fell, Nicholas F.; Gillespie, James B.
Analytica Chimica Acta, Vol. 455, Issue 2, p. 167-177
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Electromagnetic Mechanism of Surface-Enhanced Spectroscopy
book, June 2006

Schatz, George C.; Van Duyne, Richard P.; Chalmers, John M.
Handbook of Vibrational Spectroscopy
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Identification of Bacterial Spores Using Statistical Analysis of Fourier Transform Infrared Photoacoustic Spectroscopy Data
journal, August 2003

Thompson, Sandra E.; Foster, Nancy S.; Johnson, Timothy J.
Applied Spectroscopy, Vol. 57, Issue 8
https://doi.org/10.1366/000370203322258832

A Glucose Biosensor Based on Surface-Enhanced Raman Scattering: Improved Partition Layer, Temporal Stability, Reversibility, and Resistance to Serum Protein Interference
journal, January 2004

Yonzon, Chanda Ranjit; Haynes, Christy L.; Zhang, Xiaoyu
Analytical Chemistry, Vol. 76, Issue 1
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An electrochemical surface-enhanced Raman spectroscopy approach to anthrax detection
conference, November 2003

Zhang, Xiaoyu; Yonzon, Chanda R.; Van Duyne, Richard P.
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Rapid Detection of an Anthrax Biomarker by Surface-Enhanced Raman Spectroscopy
journal, March 2005

Zhang, Xiaoyu; Young, Matthew A.; Lyandres, Olga
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Similar Records

Title: Compositions, devices and methods for SERS and LSPR

Abstract

Citation Formats

Surface-enhanced raman nanobiosensor patent-application, September 2004

Adaptive metal films for detection of biomolecules patent-application, November 2005

Atomic force microscopy and surface‐enhanced Raman spectroscopy. I. Ag island films and Ag film over polymer nanosphere surfaces supported on glass journal, August 1993

Localized Surface Plasmon Resonance Nanosensor: A High-Resolution Distance-Dependence Study Using Atomic Layer Deposition journal, November 2005

Vibrational spectra and structure of crystalline dipicolinic acid and calcium dipicolinate trihydrate journal, January 1980

Octadecylthiol-modified surface-enhanced Raman spectroscopy substrates: a new method for the detection of aromatic compounds journal, October 1992

Reagentless Identification of Single Bacterial Spores in Aqueous Solution by Confocal Laser Tweezers Raman Spectroscopy journal, February 2004

Metal Film over Nanosphere (MFON) Electrodes for Surface-Enhanced Raman Spectroscopy (SERS): Improvements in Surface Nanostructure Stability and Suppression of Irreversible Loss journal, January 2002

Introductory Lecture : Surface enhanced Raman spectroscopy: new materials, concepts, characterization tools, and applications journal, January 2006

Low-Level Detection of Viral Pathogens by a Surface-Enhanced Raman Scattering Based Immunoassay journal, October 2005

Viscous flow reactor with quartz crystal microbalance for thin film growth by atomic layer deposition journal, August 2002

Rapid Dipicolinic Acid Extraction from Bacillus Spores Detected by Surface-Enhanced Raman Spectroscopy journal, March 2004

Detection of the Dipicolinic Acid Biomarker in Bacillus Spores Using Curie-Point Pyrolysis Mass Spectrometry and Fourier Transform Infrared Spectroscopy journal, January 2000

Plasmon-Sampled Surface-Enhanced Raman Excitation Spectroscopy † journal, July 2003

Nanosphere lithography: A materials general fabrication process for periodic particle array surfaces journal, May 1995

Discrimination of Bacteria Using Surface-Enhanced Raman Spectroscopy journal, January 2004

Sticking Probabilities in Adsorption of Alkanethiols from Liquid Ethanol Solution onto Gold journal, November 2000

Sticking Probabilities in Adsorption from Liquid Solutions: Alkylthiols on Gold journal, May 2000

Performance Assessment of Three Commercial Assays for Direct Detection of Bacillus anthracis Spores journal, July 2003

Surface-Enhanced Raman Scattering Detected Temperature Programmed Desorption: Optical Properties, Nanostructure, and Stability of Silver Film over SiO 2 Nanosphere Surfaces journal, July 2001

Wavelength-Scanned Surface-Enhanced Raman Excitation Spectroscopy journal, June 2005

Detection of Nitrate and Sulfate Anions by Normal Raman Spectroscopy and SERS of Cationic-Coated, Silver Substrates journal, August 2000

Enhanced spore detection using dipicolinate extraction techniques journal, March 2002

Electromagnetic Mechanism of Surface-Enhanced Spectroscopy book, June 2006

Identification of Bacterial Spores Using Statistical Analysis of Fourier Transform Infrared Photoacoustic Spectroscopy Data journal, August 2003

A Glucose Biosensor Based on Surface-Enhanced Raman Scattering: Improved Partition Layer, Temporal Stability, Reversibility, and Resistance to Serum Protein Interference journal, January 2004

An electrochemical surface-enhanced Raman spectroscopy approach to anthrax detection conference, November 2003

Rapid Detection of an Anthrax Biomarker by Surface-Enhanced Raman Spectroscopy journal, March 2005

Surface-enhanced raman nanobiosensor
patent-application, September 2004

Adaptive metal films for detection of biomolecules
patent-application, November 2005

Atomic force microscopy and surface‐enhanced Raman spectroscopy. I. Ag island films and Ag film over polymer nanosphere surfaces supported on glass
journal, August 1993

Localized Surface Plasmon Resonance Nanosensor: A High-Resolution Distance-Dependence Study Using Atomic Layer Deposition
journal, November 2005

Vibrational spectra and structure of crystalline dipicolinic acid and calcium dipicolinate trihydrate
journal, January 1980

Octadecylthiol-modified surface-enhanced Raman spectroscopy substrates: a new method for the detection of aromatic compounds
journal, October 1992

Reagentless Identification of Single Bacterial Spores in Aqueous Solution by Confocal Laser Tweezers Raman Spectroscopy
journal, February 2004

Metal Film over Nanosphere (MFON) Electrodes for Surface-Enhanced Raman Spectroscopy (SERS): Improvements in Surface Nanostructure Stability and Suppression of Irreversible Loss
journal, January 2002

Introductory Lecture : Surface enhanced Raman spectroscopy: new materials, concepts, characterization tools, and applications
journal, January 2006

Low-Level Detection of Viral Pathogens by a Surface-Enhanced Raman Scattering Based Immunoassay
journal, October 2005

Viscous flow reactor with quartz crystal microbalance for thin film growth by atomic layer deposition
journal, August 2002

Rapid Dipicolinic Acid Extraction from Bacillus Spores Detected by Surface-Enhanced Raman Spectroscopy
journal, March 2004

Detection of the Dipicolinic Acid Biomarker in Bacillus Spores Using Curie-Point Pyrolysis Mass Spectrometry and Fourier Transform Infrared Spectroscopy
journal, January 2000

Plasmon-Sampled Surface-Enhanced Raman Excitation Spectroscopy ^†
journal, July 2003

Nanosphere lithography: A materials general fabrication process for periodic particle array surfaces
journal, May 1995

Discrimination of Bacteria Using Surface-Enhanced Raman Spectroscopy
journal, January 2004

Sticking Probabilities in Adsorption of Alkanethiols from Liquid Ethanol Solution onto Gold
journal, November 2000

Sticking Probabilities in Adsorption from Liquid Solutions: Alkylthiols on Gold
journal, May 2000

Performance Assessment of Three Commercial Assays for Direct Detection of Bacillus anthracis Spores
journal, July 2003

Surface-Enhanced Raman Scattering Detected Temperature Programmed Desorption: Optical Properties, Nanostructure, and Stability of Silver Film over SiO ₂ Nanosphere Surfaces
journal, July 2001

Wavelength-Scanned Surface-Enhanced Raman Excitation Spectroscopy
journal, June 2005

Detection of Nitrate and Sulfate Anions by Normal Raman Spectroscopy and SERS of Cationic-Coated, Silver Substrates
journal, August 2000

Enhanced spore detection using dipicolinate extraction techniques
journal, March 2002

Electromagnetic Mechanism of Surface-Enhanced Spectroscopy
book, June 2006

Identification of Bacterial Spores Using Statistical Analysis of Fourier Transform Infrared Photoacoustic Spectroscopy Data
journal, August 2003

A Glucose Biosensor Based on Surface-Enhanced Raman Scattering: Improved Partition Layer, Temporal Stability, Reversibility, and Resistance to Serum Protein Interference
journal, January 2004

An electrochemical surface-enhanced Raman spectroscopy approach to anthrax detection
conference, November 2003

Rapid Detection of an Anthrax Biomarker by Surface-Enhanced Raman Spectroscopy
journal, March 2005